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Pesticide Protocols

  • Book
  • © 2006

Overview

Editors:
  1. José L. Martínez Vidal

    1. Department of Analytical Chemistry, Faculty of Sciences, University of Almería, Almería, Spain

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    You can also search for this editor in PubMed   Google Scholar

  2. Antonia Garrido Frenich

    1. Department of Analytical Chemistry, Faculty of Sciences, University of Almería, Almería, Spain

    View editor publications

    You can also search for this editor in PubMed   Google Scholar

Part of the book series: Methods in Biotechnology (MIBT, volume 19)

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Table of contents (35 protocols)

  1. Front Matter

    Pages i-xiv
    Download chapter PDF

  2. Analytical Methodologies to Determine Pesticides and Metabolites in Human Fat Tissues and Body Fluids

    1. Front Matter

      Pages 1-1
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    2. Analysis of Endocrine Disruptor Pesticides in Adipose Tissue Using Gas Chromatography-Tandem Mass Spectrometry

      • José L. Martínez Vidal, Antonia Garrido Frenich, Francisco J. Egea González, Francisco J. Arrebola Liébanas
      Pages 3-15

    3. Determination of Pyrethroids in Blood Plasma and Pyrethroid/Pyrethrin Metabolites in Urine by Gas Chromatography-Mass Spectrometry and High-Resolution GC-MS

      • Gabriele Leng, Wolfgang Gries
      Pages 17-33

    4. A Multianalyte Method for the Quantification of Current-Use Pesticides in Human Serum or Plasma Using Isotope Dilution Gas Chromatography-High-Resolution Mass Spectrometry

      • Dana B. Barr, Roberto Bravo, John R. Barr, Larry L. Needham
      Pages 35-47

    5. Application of Solid-Phase Disk Extraction Combined With Gas Chromatographic Techniques for Determination of Organochlorine Pesticides in Human Body Fluids

      • Adrian Covaci
      Pages 49-59

    6. Comprehensive Approach for Biological Monitoring of Pesticides in Urine Using HPLC-MS/MS and GC-MS/MS

      • Dana B. Barr, Anders O. Olsson, Roberto Bravo, Larry L. Needham
      Pages 61-78

    7. Urinary Ethylenethiourea as a Biomarker of Exposure to Ethylenebisdithiocarbamates

      • Silvia Fustinoni, Laura Campo, Sarah Birindelli, Claudio Colosio
      Pages 79-89

    8. Analysis of 2,4-Dichlorophenoxyacetic Acid and 2-Methyl-4-Chloro-Phenoxyacetic Acid in Human Urine

      • Cristina Aprea, Gianfranco Sciarra, Nanda Bozzi, Liana Lunghini
      Pages 91-103

    9. Determination of Herbicides in Human Urine by Liquid Chromatography-Mass Spectrometry With Electrospray Ionization

      • Isabel C. S. F. Jardim, Joseane M. Pozzebon, Sonia C. N. Queiroz
      Pages 105-110

    10. Analysis of Pentachlorophenol and Other Chlorinated Phenols in Biological Samples by Gas Chromatography or Liquid Chromatography-Mass Spectrometry

      • Ji Y. Zhang
      Pages 111-118

    11. Analysis of 2,4-Dichlorophenoxyacetic Acid in Body Fluids of Exposed Subjects Using Radioimmunoassay

      • Dietmar Knopp
      Pages 119-131

    12. A High-Throughput Screening Immunochemical Protocol for Biological Exposure Assessment of Chlorophenols in Urine Samples

      • Mikaela Nichkova, M.-Pilar Marco
      Pages 133-145

  3. Assessment of Inhalatory and Potential Dermal Exposure

    1. Front Matter

      Pages 147-147
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    2. Assessment of Postapplication Exposure to Pesticides in Agriculture

      • Joop J. van Hemmen, Katinka E. van der Jagt, Derk H. Brouwer
      Pages 149-164

    3. Field Study Methods for the Determination of Bystander Exposure to Pesticides

      • C. Richard Glass
      Pages 165-177

    4. Determination of Household Insecticides in Indoor Air by Gas Chromatography-Mass Spectrometry

      • Edith Berger-Preiss, Lutz Elflein
      Pages 179-190

    5. Assessment of Dermal and Inhalatory Exposure of Agricultural Workers to Malathion Using Gas Chromatography-Tandem Mass Spectrometry

      • Francisco J. Egea González, Francisco J. Arrebola Liébanas, A. Marín
      Pages 191-205

    6. Pesticides in Human Fat and Serum Samples vs Total Effective Xenoestrogen Burden

      • Patricia Araque, Ana M. Soto, M. Fátima Olea-Serrano, Carlos Sonnenschein, Nicolas Olea
      Pages 207-215

  4. Pesticide Analysis in Food

    1. Front Matter

      Pages 217-217
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Keywords

About this book

A comprehensive collection of robust methods for the detection of pesticide compounds or their metabolites useful in food, environmental, and biological monitoring, and in studies of exposure via food, water, air, and the skin or lungs. The readily reproducible methods range from gas and liquid chromatography coupled to mass spectrometry detection and other classic detectors, to capillary electrophoresis and immunochemical or radioimmunoassay methods. The authors have focused on extraction and cleanup procedures, in order to develop and optimize more fullyautomated and miniaturized methods, including solid-phase extraction, solid-phase microextraction, microwave-assisted extraction, and on-line tandem liquid chromatography (LC/LC) trace enrichment, among others. The protocols offer step-by-step laboratory instructions, an introduction outlining the principles behind the technique, lists of the necessary equipment and reagents, and tips on troubleshooting and avoiding known pitfalls.

Editors and Affiliations

  • Department of Analytical Chemistry, Faculty of Sciences, University of Almería, Almería, Spain

    José L. Martínez Vidal, Antonia Garrido Frenich

Bibliographic Information

  • Book Title: Pesticide Protocols

  • Editors: José L. Martínez Vidal, Antonia Garrido Frenich

  • Series Title: Methods in Biotechnology

  • DOI: https://doi.org/10.1385/159259929X

  • Publisher: Humana Totowa, NJ

  • eBook Packages: Springer Protocols

  • Copyright Information: Humana Press 2006

  • Hardcover ISBN: 978-1-58829-410-4Published: 01 September 2005

  • Softcover ISBN: 978-1-61737-548-4Published: 09 December 2010

  • eBook ISBN: 978-1-59259-929-5Published: 26 October 2007

  • Series ISSN: 1940-6061

  • Series E-ISSN: 1940-607X

  • Edition Number: 1

  • Number of Pages: XIV, 504

  • Number of Illustrations: 103 b/w illustrations

  • Topics: Biochemistry, general

  • Industry Sectors: Biotechnology, Consumer Packaged Goods, Pharma

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