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Stress Annealing Induced Diffuse Scattering from Ni3 (Al, Si) Precipitates

  • Symposium: Neutron and X-Ray Studies of Advanced Materials IV
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Abstract

Diffuse scattering caused by L12 type Ni3 (Al, Si) precipitates after stress annealing of Ni-Al-Si alloys is studied. Peculiarities of diffuse scattering in the asymptotic region as compared to the Huang scattering region are discussed. Coupling between the stress annealing direction and the precipitate shape is demonstrated. Experimental reciprocal space maps (RSMs) are compared to theoretical ones. Oscillations of diffuse scattering due to Ni3 (Al, Sc) precipitates are observed. The strengths of the precipitates are estimated from the analysis of the diffuse scattering oscillations.

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References

  1. M.A. Krivoglaz: X-ray and Neutron Diffraction in Nonideal Crystals, Springer, Berlin, 1996; Theory of X-ray and Thermal Neutron Scattering by Real Crystals, Plenum Press, New York, NY, 1969.

  2. R.I. Barabash and M.A. Krivoglaz: Phys. Met. Metallogr., 1978, vol. 45 (1), pp. 7–18.

    CAS  Google Scholar 

  3. R.I. Barabash and M.A. Krivoglaz: Phys. Met. Metallogr., 1981, vol. 51 (5), pp. 903–16.

    CAS  Google Scholar 

  4. R.I. Barabash: J. Chim. Phys., 1997, vol. 94, pp. 1121–32.

    CAS  Google Scholar 

  5. R.I. Barabash: in Local Structure and Diffraction, S.J.L. Billinge and M.F. Thorpe, eds., Plenum Press, New York, NY, 1998, pp. 233–51.

  6. R.I. Barabash, J.S. Chung, and M.F. Thorpe: J. Phys.: Condens. Matter., 1999, vol. 11, pp. 3075–90.

    Article  CAS  Google Scholar 

  7. S. Iida, B.C. Larson, and J.Z. Tischler: J. Mater. Res., 1988, vol. 3 (2), pp. 267–73.

    Article  Google Scholar 

  8. B.C. Larson: J. Appl. Cryst., 1975, vol. 8 (2), pp. 150–60.

    Article  Google Scholar 

  9. B.C. Larson and W. Schmatz: Phys. Rev. B, 1974, vol. 10 (6), pp. 2307–14.

    Article  CAS  Google Scholar 

  10. P.H. Dederichs: Phys. Rev. B, 1971, vol. 4 (4), pp. 1041–50.

    Article  Google Scholar 

  11. H. Trinkaus: Phys. Stat. Sol. (b), 1972, vol. 51, pp. 307–19.

    Article  CAS  Google Scholar 

  12. C.R. Houska: Acta Cryst. A, 1993, vol. 49, pp. 771–81.

    Article  Google Scholar 

  13. O. Lyon, I. Guillon, and C. Servant: J. Appl. Cryst., 2001, vol. 34, pp. 484–92.

    Article  CAS  Google Scholar 

  14. C. Servant, I. Guillon, and O. Lyon: J. Appl. Cryst., 2003, vol. 36, pp. 454–58.

    Article  Google Scholar 

  15. A.G. Khachaturyan: Theory of Structural Transformations in Solids, Wiley & Sons, New York, NY, 1983.

    Google Scholar 

  16. C. Wolverton: Acta Mater., 2001, vol. 49, pp. 3129–42.

    Article  CAS  Google Scholar 

  17. C. Wolverton and A. Zunger: Phys. Rev. B, 1994, vol. 49 (22), pp. 16058–61.

    Article  CAS  Google Scholar 

  18. C. Wolverton and A. Zunger: Phys. Rev. B, 1995, vol. 52 pp. 8813–28.

    Article  CAS  Google Scholar 

  19. L.-M. Stadler, B. Sepiol, R. Weinkamer, M. Hartmann, P. Fratzl, J.W. Kantelhardt, F. Zontone, G. Grubel, and G. Vogl: Phys. Rev. B, 2003, vol. 68, p. 18010.

    Article  Google Scholar 

  20. L. Reinhardt, J.L. Robertson, S.C. Moss, G.E. Ice, P. Zschack, and C.J. Sparks: Phys. Rev. B, 1992, vol. 45 (6), pp. 2662–76.

    Article  Google Scholar 

  21. A.R. Stokes and A.J.C. Wilson: Proc. Phys. Soc., 1944, vol. 56 (3), pp. 174–81.

    Article  CAS  Google Scholar 

  22. H. Trinkaus: Z. Angew. Phys., 1971, vol. 31 (5–6), pp. 229–35.

    CAS  Google Scholar 

  23. M.A. Krivoglaz: Fiz. Met. Metallov., 1960, vol. 9 (5), pp. 641–56.

    CAS  Google Scholar 

  24. H. Trinkaus, H. Spalt, and H. Peisl: Phys. Status Solidi (a), 1970, vol. 2, pp. 97–100.

    Article  Google Scholar 

  25. R. Drautz, H. Reihert, M. Fahnle, and H. Dosch: PRL, 2001, vol. 87 (23), p. 236102.

    Article  CAS  Google Scholar 

  26. B.C. Larson: in Diffuse Scattering and the Fundamental Properties of Materials, R.I. Barabash, G.E. Ice, and P.E.A. Turchi, eds., Momentum Press, New York, NY, 2009, pp. 139–60.

  27. N.A. Zarkevich, D.D. Johnson, and A.V. Smirnov: Acta Mater., 2002, vol. 50, pp. 2443–59.

    Article  CAS  Google Scholar 

  28. B. Schonfeld and G. Kostorz: in Diffuse Scattering and the Fundamental Properties of Materials, R.I. Barabash, G.E. Ice, and P.E.A. Turchi, eds., Momentum Press, New York, NY, 2009, pp. 119–37.

  29. J.M. Schneider, B. Schonfeld, B. Deme, and G. Kostorz: J. Appl. Cryst., 2000, vol. 33, pp. 465–68.

    Article  CAS  Google Scholar 

  30. M. Mezger, H. Reichert, I.B. Ramsteiner, A. Udyansky, O. Shchyglo, V.N. Bugaev, H. Dosch, and V. Honkimäki: Phys. Rev. B, 2006, vol. 73, p. 184206.

    Article  Google Scholar 

  31. B.J. Campbell: Metall. Mater. Trans. A, 2010, vol. 41A, pp. 1130–36.

    Article  CAS  Google Scholar 

  32. J.D. Brock, J.D. Ferguson, and A.R. Woll: Metall. Mater. Trans. A, 2010, vol. 41A, pp. 1162–66.

    Article  CAS  Google Scholar 

  33. C.I. Del Genio, K.E. Bassler, A.L. Korzenevskii, R.I. Barabash, J. Trenkler, G.F. Reiter, and S.C. Moss: Phys. Rev. B, 2010, vol. 81, p. 144111.

    Article  Google Scholar 

  34. P. Wochner, C. Gutt, T. Autenrieth, T. Demmer, V. Bugaev, A. Díaz Ortiz, A. Duri, F. Zontone, G. Grubel, and H. Dosch: PNAS, 2009, vol. 106 (28), pp. 11511–14.

    Article  CAS  Google Scholar 

  35. C. Mocuta, H. Reichert, K. Mecke, H. Dosch, and M. Drakopoulos: Science, 2005, vol. 308, pp. 1287–91.

    Article  CAS  Google Scholar 

  36. T.R. Welberry and M. Pasciaik: Metall. Mater. Trans. A, 2011, vol. 42A, pp. 6–13.

    Article  Google Scholar 

  37. D.J. Goossens, A.P. Heerdegen, E.J. Chan, and T.R. Welberry: Metall. Mater. Trans. A, 2011, vol. 42A, pp. 23–31.

    Article  Google Scholar 

  38. H. Abe, Y. Imai, T. Goto, Y. Yoshimura, M. Aono, T. Takekiyo, H. Matsumoto, and T. Arai: Metall. Mater. Trans. A, 2010, vol. 41A, pp. 1137–43.

    Article  CAS  Google Scholar 

  39. T. Egami: in Diffuse Scattering and the Fundamental Properties of Materials, R.I. Barabash, G.E. Ice, and P.E.A. Turchi, eds., Momentum Press, New York, NY, 2009, pp. 317–28.

  40. R.I. Barabash, O.M. Barabash, and G. Mansurov: Metallofizika, 1988, vol. 10 (1), pp. 56–59.

    CAS  Google Scholar 

  41. B.E. Warren: X-Ray Diffraction, Dover Publications, Inc., New York, NY, 1969.

    Google Scholar 

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Acknowledgments

Research supported by the Materials Sciences and Engineering Division, Office of Basic Energy Sciences, United States Department of Energy. X-ray microbeam measurements were performed at 33-ID at the Advanced Photon Source (APS). The use of the APS was supported by the Scientific Users Facilities Division, Office of Basic Energy Sciences, United States Department of Energy.

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Authors and Affiliations

  1. Oak Ridge National Laboratory, Oak Ridge, TN, 37831, USA

    R. I. Barabash (Research Staff Member) & G. E. Ice (Division Director)

  2. Materials Science and Technology Division, Advanced Photon Source, Argonne, IL, 60439, USA

    E. A. Karapetrova (Senior Scientific Associate) & P. Zschack (Senior Research Staff Member)

Authors
  1. R. I. Barabash
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  2. G. E. Ice
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  3. E. A. Karapetrova
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  4. P. Zschack
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Correspondence to R. I. Barabash.

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Manuscript submitted March 21, 2011.

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Barabash, R.I., Ice, G.E., Karapetrova, E.A. et al. Stress Annealing Induced Diffuse Scattering from Ni3 (Al, Si) Precipitates. Metall Mater Trans A 43, 1413–1422 (2012). https://doi.org/10.1007/s11661-011-0937-z

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