Metallurgical and Materials Transactions A

, Volume 43, Issue 5, pp 1413–1422 | Cite as

Stress Annealing Induced Diffuse Scattering from Ni3 (Al, Si) Precipitates

  • R. I. Barabash
  • G. E. Ice
  • E. A. Karapetrova
  • P. Zschack
Symposium: Neutron and X-Ray Studies of Advanced Materials IV

Abstract

Diffuse scattering caused by L12 type Ni3 (Al, Si) precipitates after stress annealing of Ni-Al-Si alloys is studied. Peculiarities of diffuse scattering in the asymptotic region as compared to the Huang scattering region are discussed. Coupling between the stress annealing direction and the precipitate shape is demonstrated. Experimental reciprocal space maps (RSMs) are compared to theoretical ones. Oscillations of diffuse scattering due to Ni3 (Al, Sc) precipitates are observed. The strengths of the precipitates are estimated from the analysis of the diffuse scattering oscillations.

References

  1. 1.
    M.A. Krivoglaz: X-ray and Neutron Diffraction in Nonideal Crystals, Springer, Berlin, 1996; Theory of X-ray and Thermal Neutron Scattering by Real Crystals, Plenum Press, New York, NY, 1969.Google Scholar
  2. 2.
    R.I. Barabash and M.A. Krivoglaz: Phys. Met. Metallogr., 1978, vol. 45 (1), pp. 7–18.Google Scholar
  3. 3.
    R.I. Barabash and M.A. Krivoglaz: Phys. Met. Metallogr., 1981, vol. 51 (5), pp. 903–16.Google Scholar
  4. 4.
    R.I. Barabash: J. Chim. Phys., 1997, vol. 94, pp. 1121–32.Google Scholar
  5. 5.
    R.I. Barabash: in Local Structure and Diffraction, S.J.L. Billinge and M.F. Thorpe, eds., Plenum Press, New York, NY, 1998, pp. 233–51.Google Scholar
  6. 6.
    R.I. Barabash, J.S. Chung, and M.F. Thorpe: J. Phys.: Condens. Matter., 1999, vol. 11, pp. 3075–90.CrossRefGoogle Scholar
  7. 7.
    S. Iida, B.C. Larson, and J.Z. Tischler: J. Mater. Res., 1988, vol. 3 (2), pp. 267–73.CrossRefGoogle Scholar
  8. 8.
    B.C. Larson: J. Appl. Cryst., 1975, vol. 8 (2), pp. 150–60.CrossRefGoogle Scholar
  9. 9.
    B.C. Larson and W. Schmatz: Phys. Rev. B, 1974, vol. 10 (6), pp. 2307–14.CrossRefGoogle Scholar
  10. 10.
    P.H. Dederichs: Phys. Rev. B, 1971, vol. 4 (4), pp. 1041–50.CrossRefGoogle Scholar
  11. 11.
    H. Trinkaus: Phys. Stat. Sol. (b), 1972, vol. 51, pp. 307–19.CrossRefGoogle Scholar
  12. 12.
    C.R. Houska: Acta Cryst. A, 1993, vol. 49, pp. 771–81.CrossRefGoogle Scholar
  13. 13.
    O. Lyon, I. Guillon, and C. Servant: J. Appl. Cryst., 2001, vol. 34, pp. 484–92.CrossRefGoogle Scholar
  14. 14.
    C. Servant, I. Guillon, and O. Lyon: J. Appl. Cryst., 2003, vol. 36, pp. 454–58.CrossRefGoogle Scholar
  15. 15.
    A.G. Khachaturyan: Theory of Structural Transformations in Solids, Wiley & Sons, New York, NY, 1983.Google Scholar
  16. 16.
    C. Wolverton: Acta Mater., 2001, vol. 49, pp. 3129–42.CrossRefGoogle Scholar
  17. 17.
    C. Wolverton and A. Zunger: Phys. Rev. B, 1994, vol. 49 (22), pp. 16058–61.CrossRefGoogle Scholar
  18. 18.
    C. Wolverton and A. Zunger: Phys. Rev. B, 1995, vol. 52 pp. 8813–28.CrossRefGoogle Scholar
  19. 19.
    L.-M. Stadler, B. Sepiol, R. Weinkamer, M. Hartmann, P. Fratzl, J.W. Kantelhardt, F. Zontone, G. Grubel, and G. Vogl: Phys. Rev. B, 2003, vol. 68, p. 18010.CrossRefGoogle Scholar
  20. 20.
    L. Reinhardt, J.L. Robertson, S.C. Moss, G.E. Ice, P. Zschack, and C.J. Sparks: Phys. Rev. B, 1992, vol. 45 (6), pp. 2662–76.CrossRefGoogle Scholar
  21. 21.
    A.R. Stokes and A.J.C. Wilson: Proc. Phys. Soc., 1944, vol. 56 (3), pp. 174–81.CrossRefGoogle Scholar
  22. 22.
    H. Trinkaus: Z. Angew. Phys., 1971, vol. 31 (5–6), pp. 229–35.Google Scholar
  23. 23.
    M.A. Krivoglaz: Fiz. Met. Metallov., 1960, vol. 9 (5), pp. 641–56.Google Scholar
  24. 24.
    H. Trinkaus, H. Spalt, and H. Peisl: Phys. Status Solidi (a), 1970, vol. 2, pp. 97–100.CrossRefGoogle Scholar
  25. 25.
    R. Drautz, H. Reihert, M. Fahnle, and H. Dosch: PRL, 2001, vol. 87 (23), p. 236102.CrossRefGoogle Scholar
  26. 26.
    B.C. Larson: in Diffuse Scattering and the Fundamental Properties of Materials, R.I. Barabash, G.E. Ice, and P.E.A. Turchi, eds., Momentum Press, New York, NY, 2009, pp. 139–60.Google Scholar
  27. 27.
    N.A. Zarkevich, D.D. Johnson, and A.V. Smirnov: Acta Mater., 2002, vol. 50, pp. 2443–59.CrossRefGoogle Scholar
  28. 28.
    B. Schonfeld and G. Kostorz: in Diffuse Scattering and the Fundamental Properties of Materials, R.I. Barabash, G.E. Ice, and P.E.A. Turchi, eds., Momentum Press, New York, NY, 2009, pp. 119–37.Google Scholar
  29. 29.
    J.M. Schneider, B. Schonfeld, B. Deme, and G. Kostorz: J. Appl. Cryst., 2000, vol. 33, pp. 465–68.CrossRefGoogle Scholar
  30. 30.
    M. Mezger, H. Reichert, I.B. Ramsteiner, A. Udyansky, O. Shchyglo, V.N. Bugaev, H. Dosch, and V. Honkimäki: Phys. Rev. B, 2006, vol. 73, p. 184206.CrossRefGoogle Scholar
  31. 31.
    B.J. Campbell: Metall. Mater. Trans. A, 2010, vol. 41A, pp. 1130–36.CrossRefGoogle Scholar
  32. 32.
    J.D. Brock, J.D. Ferguson, and A.R. Woll: Metall. Mater. Trans. A, 2010, vol. 41A, pp. 1162–66.CrossRefGoogle Scholar
  33. 33.
    C.I. Del Genio, K.E. Bassler, A.L. Korzenevskii, R.I. Barabash, J. Trenkler, G.F. Reiter, and S.C. Moss: Phys. Rev. B, 2010, vol. 81, p. 144111.CrossRefGoogle Scholar
  34. 34.
    P. Wochner, C. Gutt, T. Autenrieth, T. Demmer, V. Bugaev, A. Díaz Ortiz, A. Duri, F. Zontone, G. Grubel, and H. Dosch: PNAS, 2009, vol. 106 (28), pp. 11511–14.CrossRefGoogle Scholar
  35. 35.
    C. Mocuta, H. Reichert, K. Mecke, H. Dosch, and M. Drakopoulos: Science, 2005, vol. 308, pp. 1287–91.CrossRefGoogle Scholar
  36. 36.
    T.R. Welberry and M. Pasciaik: Metall. Mater. Trans. A, 2011, vol. 42A, pp. 6–13.CrossRefGoogle Scholar
  37. 37.
    D.J. Goossens, A.P. Heerdegen, E.J. Chan, and T.R. Welberry: Metall. Mater. Trans. A, 2011, vol. 42A, pp. 23–31.CrossRefGoogle Scholar
  38. 38.
    H. Abe, Y. Imai, T. Goto, Y. Yoshimura, M. Aono, T. Takekiyo, H. Matsumoto, and T. Arai: Metall. Mater. Trans. A, 2010, vol. 41A, pp. 1137–43.CrossRefGoogle Scholar
  39. 39.
    T. Egami: in Diffuse Scattering and the Fundamental Properties of Materials, R.I. Barabash, G.E. Ice, and P.E.A. Turchi, eds., Momentum Press, New York, NY, 2009, pp. 317–28.Google Scholar
  40. 40.
    R.I. Barabash, O.M. Barabash, and G. Mansurov: Metallofizika, 1988, vol. 10 (1), pp. 56–59.Google Scholar
  41. 41.
    B.E. Warren: X-Ray Diffraction, Dover Publications, Inc., New York, NY, 1969.Google Scholar

Copyright information

© The Minerals, Metals & Materials Society and ASM International (outside the USA) 2011

Authors and Affiliations

  • R. I. Barabash
    • 1
  • G. E. Ice
    • 1
  • E. A. Karapetrova
    • 2
  • P. Zschack
    • 2
  1. 1.Oak Ridge National LaboratoryOak RidgeUSA
  2. 2.Materials Science and Technology DivisionAdvanced Photon SourceArgonneUSA

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