Abstract
A fundamental principle in materials science and engineering is that the microstructure controls material properties. The use of three-dimensional techniques has gained popularity in establishing structure-property relationships in a variety of material systems. In particular, X-ray microtomography is being widely used as it requires minimal sample preparation and is nondestructive in nature. Moreover, being a nondestructive technique, it is very well suited to perform 4D studies (the fourth dimension being time) where the evolution of microstructure can be captured over time. This chapter describes the fundamentals of X-ray microtomography followed by applications of the use of X-ray microtomography to understand the mechanical properties of materials under a variety of loading conditions, such as tensile loading, fatigue loading, corrosion fatigue, and stress corrosion cracking.
References
Williams JJ, Chapman NC, Jakkali V, Tanna VA, Chawla N, Xiao X, De Carlo F. Characterization of damage evolution in SiC particle reinforced Al alloy matrix composites by in-situ X-ray synchrotron tomography. Metall Mater Trans A. 2011;42:2999–3005.
Stock SR. Microcomputed tomography: methodology and applications. Boca Raton: CRC Press; 2008.
Maire E, Zhou SX, Adrien J, Dimichiel M. Damage quantification in aluminium alloys using in situ tensile tests in X-ray tomography. Eng Fract Mech. 2011;78(15):2679–90.
Maire E, Carmona V, Courbon J, Ludwig W. Fast X-ray tomography and acoustic emission study of damage in metals during continuous tensile tests. Acta Mater. 2007;55:6806–15.
Patterson BM, Cordes NL, Henderson K, Williams JJ, Stannard T, Singh SS, Ovejero AR, Xiao X, Robinson M, Chawla N. In situ X-ray synchrotron tomographic imaging during the compression of hyper-elastic polymeric materials. J Mater Sci. 2016;51:171–87.
Cordes NL, Henderson K, Stannard T, Williams JJ, Xiao X, Robinson MWC, Schaedler TA, Chawla N, Patterson BM. Synchrotron-based X-ray computed tomography during compression loading of cellular materials. Microscopy Today. 2015;23:12–9.
Guvenilir A, Breunig TM, Kinney JH, Stock SR. Direct observation of crack opening as a function of applied load in the interior of a notched tensile sample of Al-Li 2090. Acta Mater. 1997;45(5):1977–87.
Chapman NC, Silva J, Williams JJ, Chawla N, Xiao X. Characterization of thermal cycling induced cavitation in particle reinforced metal matrix composites by three-dimensional (3D) X-ray synchrotron tomography. Mater Sci Technol. 2014;31(5):573–8.
Williams JJ, Yazzie KE, Padilla E, Chawla N, Xiao X, De Carlo F. Understanding fatigue crack growth in aluminum alloys by in situ X-ray synchrotron tomography. Int J Fatigue. 2013;57:79–85.
Khor KH, Buffiere JY, Ludwig W, Toda H, Ubhi HS, Gregson PJ, Sinclair I. In situ high resolution synchrotron X-ray tomography of fatigue crack closure micromechanisms. J Phys Condens Matter. 2004;16:S3511–5.
Toda H, Sinclair I, Buffiere JY, Maire E, Connolley T, Joyce M, Khor KH, Gregson P. Assessment of the fatigue crack closure phenomenon in damage-tolerant aluminium alloy by in-situ high-resolution synchrotron X-ray microtomography. Philos Mag. 2003;83(21): 2429–48.
Babout L, Marrow TJ, Engelberg D, Withers PJ. X-ray microtomographic observation ofintergranular stress corrosion cracking in sensitized austenitic stainless steel. Mater Sci Technol. 2006;22:1068–75.
Marrow TJ, Babout L, Jivkov AP, Wood P, Engelberg D, Stevens N, Withers PJ, Newman RC. Three dimensional observations and modelling of intergranular stress corrosion cracking in austenitic stainless steel. J Nucl Mater. 2006;352:62–74.
King A, Johnson G, Engelberg D, Ludwig W, Marrow TJ. Observations of intergranular stress corrosion cracking in a grain- mapped polycrystal. Science. 2008;321(5887):382–5.
Singh SS, Williams JJ, Stannard TJ, Xiao X, De Carlo F, Chawla N. Measurement of localized corrosion rates at inclusion particles in AA7075 by in situ three dimensional (3D) X-ray synchrotron tomography. Corros Sci. 2016;104:330–5.
Singh SS, Williams JJ, Xiao X, De Carlo F, Chawla N. In Situ three dimensional (3D) X-ray synchrotron tomography of corrosion fatigue in Al7075 alloy. In: Srivatsan TS, Imam AM, Srinivasan R, editors. Fatigue of materials II: advances and emergences in understanding. Pittsburgh: Materials Science and Technology; 2012.
Isaac A, Sket F, Reimers W, Camin B, Sauthoff G, Pyzalla AR. In situ 3D quantification of the evolution of creep cavity size, shape, and spatial orientation using synchrotron X-ray tomography. Mater Sci Eng A. 2008;478:108–18.
Stock SR. Recent advances in X-ray microtomography applied to materials. Int Mater Rev. 2008;53:129–81.
Marone F, Stampanoni M. Regridding reconstruction algorithm for real-time tomographic imaging. J Synchrotron Radiat. 2012;19:1029–37.
Baruchel J, Buffiere JY, Maire E, Merle P, Peix G. X-ray tomography in material science. Paris: HERMES Science Publications; 2000.
Mertens JCE, Williams JJ, Chawla N. Development of a lab-scale, high-resolution, tube-generated X-ray computed-tomography system for three-dimensional (3D) materials characterization. Mater Charact. 2014;92:36–48.
Mertens JCE, Williams JJ, Chawla N. A study of Pb-rich dendrites in a near-eutectic 63Sn-37Pb solder microstructure via laboratory-scale micro X-ray computed tomography (μXCT). J Electron Mater. 2014;43:4442–56.
Stock SR. X-ray computed tomography, X-ray techniques, characterization of materials. Hoboken: Wiley; 2012.
Maire E, Withers PJ. Quantitative X-ray tomography. Int Mater Rev. 2014;59:1–43.
Singh SS, Schwartzstein C, Williams JJ, Xiao X, De Carlo F, Chawla N. 3D microstructural characterization and mechanical properties of constituent particles in Al 7075 alloys using X-ray synchrotron tomography and nanoindentation. J Alloys Compd. 2014;602:163–74.
Silva FA, Williams JJ, Mueller BR, Hentschel MP, Portella PD, Chawla N. 3D microstructure visualization of inclusions and porosity in SiC particle reinforced Al matrix composites by X-ray synchrotron tomography. Metall Mater Trans A. 2010;41:2121–8.
Williams JJ, Flom Z, Amell AA, Chawla N, Xiao X, De Carlo F. Damage evolution in SiC particle reinforced Al alloy matrix composites by X-ray synchrotron tomography. Acta Mater. 2010;58:6194–205.
Wang M, Xu Y, Zheng Q, Wu S, Jing T, Chawla N. Dendritic growth in Mg-based alloys: phase-field simulations and experimental verification by X-ray synchrotron tomography. Metall Mater Trans A. 2014;45:2562–74.
Singh SS, Loza JJ, Merkle AP, Chawla N. Three dimensional microstructural characterization of nanoscale precipitates in AA7075-T651 by focused ion beam (FIB) tomography. Mater Charact. 2016;118:102–11.
Singh SS, Guo E, Xie H, Chawla N. Mechanical properties of intermetallic inclusions in Al 7075 alloys by micropillar compression. Intermetallics. 2015;62:69–75.
Merkle AP, Lechner L, Steinbach A, Gelb J, Kienle M, Phaneuf MW, Unrau D, Singh SS, Chawla N. Automated correlative tomography using XRM and FIB-SEM to span length scales and modalities in 3D materials. Microsc Microanal. 2014;28:S10–3.
Withers PJ, Preuss M. Fatigue and damage in structural materials studied by X-ray tomography. Annu Rev Mater Res. 2012;42:81–103.
Buffiere JY, Maire E, Adrien J, Masse JP, Boller E. In situ experiments with X-ray tomography: an attractive tool for experimental mechanics. Exp Mech. 2010;50:289–305.
Beckmann F, Grupp R, Haibel A, Huppmann M, Nöthe M, Pyzalla A, Reimers W, Schreyer A, Zettler R. In-situ synchrotron X-ray microtomography studies of microstructure and damage evolution in engineering materials. Adv Eng Mater. 2007;9:939–50.
Salvo L, Suery M, Marmottant A, Limodin N, Bernard D. 3D imaging in material science: application of X-ray tomography. C R Phys. 2010;11:641–9.
Maire E, Buffiere J-Y, Salvo L, Blandin JJ, Ludwig W, Letang JM. On the application of X-ray microtomography in the field of materials science. Adv Eng Mater. 2001;3:539–46.
Singh SS, Williams JJ, Hruby P, Xiao X, De Carlo F, Chawla N. In situ experimental techniques to study the mechanical behavior of materials using X-ray synchrotron tomography. Integr Mater Manuf Innov. 2014;3:1–14.
Hruby P, Singh SS, Williams JJ, Xiao X, De Carlo F, Chawla N. Fatigue crack growth in SiC particle reinforced Al alloy matrix composites at high and low R-ratios by in situ X-ray synchrotron tomography. Int J Fatigue. 2014;68:136–43.
Singh SS, Williams JJ, Lin MF, Xiao X, De Carlo F, Chawla N. In situ investigation of high humidity stress corrosion cracking of 7075 aluminum alloy by three-dimensional (3D) X-ray synchrotron tomography. Mater Res Lett. 2014;2(4):217–20.
Singh SS, Stannard TJ, Xiao X, Chawla N. In situ X-ray microtomography of stress corrosion cracking and corrosion fatigue in aluminum alloys. JOM. 2017;69(8):1404–14.
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Singh, S.S., Chawla, N. (2018). 3D/4D X-Ray Microtomography: Probing the Mechanical Behavior of Materials. In: Schmauder, S., Chen, CS., Chawla, K., Chawla, N., Chen, W., Kagawa, Y. (eds) Handbook of Mechanics of Materials. Springer, Singapore. https://doi.org/10.1007/978-981-10-6855-3_47-1
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DOI: https://doi.org/10.1007/978-981-10-6855-3_47-1
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