Zusammenfassung
Der Einfluss von betrieblichen Bedingungen, Katalysatoreigenschaften und Reaktorabmessungen auf das Verhalten von Rieselbettreaktoren für heterogen-katalysierte Gas-Flüssig-Reaktionen wird illustriert. Dabei liegt der Schwerpunkt auf der Beschreibung der komplexen Hydrodynamik und der Transportprozesse sowie deren Berücksichtigung bei der Reaktormodellierung. Zusätzlich werden Aspekte der Prozessentwicklung auf Basis von Laborexperimenten beleuchtet und Kriterien zur Bewertung der Abweichung vom idealen Rohrreaktor diskutiert. Zur Überwindung von Stofftransportlimitierungen werden Intensivierungskonzepte für Rieselbettreaktoren vorgestellt.
Der Beitrag wurde in einer vorigen Version versehentlich vorab veröffentlicht und wurde korrigiert.
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Notes
- 1.
Die Korrelationen zu Hydrodynamik und Stofftransport basierend auf dem neuronalen Netz von der Gruppe um Prof. Larachi (Universität Laval, Kanada) sind in einem Simulator implementiert (http://www2.gch.ulaval.ca/flarachi/pbrsimul/).
Literatur
Al-Dahhan, M.H., Dudukovic, M.P.: Catalyst bed dilution for improving catalyst wetting in laboratory trickle-bed reactors. AIChE J. 42, 2594–2606 (1996)
Al-Dahhan, M.H., Highfill, W.: Liquid holdup measurement techniques in laboratory high pressure trickle bed reactors. Can. J. Chem. Eng. 77, 759–765 (1999)
Al-Dahhan, M.H., Larachi, F., Dudukovic, M.P., Laurent, A.: High-pressure trickle-bed reactors: a review. Ind. Eng. Chem. Res. 36, 3292–3314 (1997)
Al-Dahhan, M.H., Wu, Y., Dudukovic, M.P.: Reproducible technique for packing laboratory-scale trickle-bed reactors. Ind. Eng. Chem. Res. 34, 741–747 (1995)
Alicilar, A., Bicer, A., Murathan, A.: The relation between wetting efficiency and liquid holdup in packed columns. Chem. Eng. Commun. 128, 95–107 (1994)
Anadon, L.D., Sederman, A.J., Gladden, F.L.: Rationalising MRI, conductance and pressure drop measurements of the trickle-to-pulse transition in trickle beds. Chem. Eng. Sci. 63, 4640–4648 (2008)
Ancheyta, J., Marroquin, G., Angeles, M.J., Macias, M.J., Pitault, I., Forisser, M., Morales, R.D.: Some experimental observation of mass transfer limitation in a trickle-bed hydrotreating pilot reactor. Energy Fuel 16, 1059–1067 (2002)
Anderson, J.B.: A criterion for isothermal behavior of catalyst pellet. Chem. Eng. Sci. 18, 147–148 (1963)
Aris, R.: Notes on the diffusion-type model for longitudinal mixing in flows. Chem. Eng. Sci. 9, 266–267 (1959)
Atta, A., Hamidipour, M., Roy, S., Nigam, K.D.P., Larachi, F.: Propagation of slow/fast-mode solitary liquid waves in trickle beds via electrical capacitance tomography and computational fluid dynamics. Chem. Eng. Sci. 65, 1144–1150 (2010a)
Atta, A., Schubert, M., Nigam, K.D.P., Roy, S., Larachi, F.: Co-current descending two-phase flow in inclined packed beds: experiments versus simulations. Can. J. Chem. Eng. 88, 742–750 (2010b)
Atta, A., Roy, S., Larachi, F., Nigam, K.D.P.: Cyclic operation of trickle bed reactors: a review. Chem. Eng. Sci. 115, 205–214 (2014)
Atta, A., Roy, S., Nigam, K.D.P.: Prediction of pressure drop and liquid holdup in trickle bed reactor using relative permeability concept in CFD. Chem. Eng. Sci. 62, 5870–5879 (2007a)
Atta, A., Roy, S., Nigam, K.D.P.: Investigation of liquid maldistribution in trickle-bed reactors using porous media concept in CFD. Chem. Eng. Sci. 62, 7033–7044 (2007b)
Attou, A., Boyer, C.: Hydrodynamics of gas-liquid-solid trickle-bed reactors: a critical review. Oil Gas Sci. Technol. 54, 29–66 (1999)
Attou, A., Boyer, C., Ferschneider, G.: Modelling of the hydrodynamics of the cocurrent gas-liquid trickle flow through a trickle-bed reactor. Chem. Eng. Sci. 54, 785–802 (1999)
Attou, A., Ferschneider, G.: A two-fluid hydrodynamic model for the transition between trickle and pulse flow in a cocurrent gas-liquid packed-bed reactor. Chem. Eng. Sci. 55, 491–511 (2000)
Aydin, B., Bilodeau, S., Hamidipour, M., Larachi, F., Kleitz, F.: Polymer-filled composite porous catalytic particles for hydrodynamic studies in trickle-bed reactors. Ind. Eng. Chem. Res. 47, 2569–2578 (2008)
Babcock, B.D., Mejdell, G.T., Hougen, O.A.: Catalyzed gas-liquid reactions in trickling-bed reactors. 1. Hydrogenation of α-methylstyrene catalyzed by palladium. AIChE J. 3, 366–369 (1957)
Banchero, M., Manna, L., Sicardi, S., Ferri, A.: Experimental investigation of fast-mode liquid modulation in a trickle-bed reactor. Chem. Eng. Sci. 59, 4149–4154 (2004)
Battsengel, B., Datsevich, L.B., Jess, A., Munnich, C., Peter, S., Turek, T.: Use of a two-phase reactor with pre-saturator for multiphase reactions. Chem. Ing. Tech. 75, 553–558 (2003)
Baussaron, L., Julcour-Lebigue, C., Wilhelm, A.-M., Boyer, C., Delmas, H.: Partial wetting in trickle bed reactors: measurement techniques and global wetting efficiency. Ind. Eng. Chem. Res. 46, 8397–8405 (2007)
Bej, S.K., Dabral, R.P., Gupta, P.C., Mittal, K.K., Sen, G.S., Kapoor, V.K., Dalai, A.K.: Studies on the performance of a microscale trickle bed reactor using different size of diluent. Energy Fuel 14, 701–705 (2000)
Bellussi, G., Pazzuconi, G., Perego, C., Girotti, G., Terzoni, G.: Liquid-phase alkylation of benzene with light olefins catalyzed by β-zeolites. J. Catal. 157, 227–234 (1995)
Beziat, J.-C., Besson, M., Gallezot, P., Durecu, S.: Catalytic wet air oxidation on a Ru/TiO2 catalyst in a trickle-bed reactor. Ind. Eng. Chem. Res. 38, 1310–1315 (1999)
Bieberle, A., Schubert, M., da Silva, M.J., Hampel, U.: Measurement of liquid distributions in particle packings using wire-mesh sensor versus transmission tomographic imaging. Ind. Eng. Chem. Res. 49, 9445–9453 (2010)
Blok, J.R., Varkevisser, J., Drinkenburg, A.A.H.: Transition to pulsing flow, holdup and pressure drop in packed columns with cocurrent gas-liquid downflow. Chem. Eng. Sci. 38, 687–699 (1983)
Boelhouwer, J.G., Piepers, H.W., Drinkenburg, A.A.H.: Particle–liquid heat transfer in trickle-bed reactors. Chem. Eng. Sci. 56, 1181–1187 (2001a)
Boelhouwer, J.G., Piepers, H.W., Drinkenburg, A.A.H.: The induction of pulses in trickle-bed reactors by cycling the liquid feed. Chem. Eng. Sci. 56, 2605–2614 (2001b)
Borremans, D., Rode, S., Wild, G.: Liquid flow distribution and particle-fluid heat transfer in trickle-bed reactors: the influence of periodic operation. Chem. Eng. Process. 43, 1403–1410 (2004)
Boyer, C, Duquenne, A.M., Wild, G.: Measuring techniques in gas-liquid and gas-liquid-solid reactors. Chem. Eng. Sci. 57, 3185–3215 (2002)
Boyer, C., Koudil, A., Chen, P., Dudukovic, M.P.: Study of liquid spreading from a point source in a trickle bed via gamma-ray tomography and CFD simulation. Chem. Eng. Sci. 60, 6279–6288 (2005)
Buffham, B.A., Gibilaro, L.G., Rathor, M.N.: A probabilistic time delay description of flow in packed beds. AIChE J. 16, 218–223 (1970)
Bukur, D.B., Patel, S.A., Lang, X.S.: Fixed-bed and slurry reactor studies of Fischer-Tropsch synthesis on precipitated iron catalyst. Appl. Catal. 61, 329–349 (1990)
Burghardt, A., Kolodziej, A.S.: Dynamic method for determining of liquid-solid contacting efficiency in trickle-bed reactors. Chem. Process. Eng-Inz. 11, 553–573 (1990)
Burghardt, A., Kolodziej, A.S., Jaroszynski, M.: Experimental studies of liquid solid wetting efficiency in trickle-bed cocurrent reactors. Chem. Eng. Process. 28, 35–49 (1990)
Burghardt, A., Zaleski, T.: Longitudinal dispersion at small and large Péclet numbers in chemical flow reactors. Chem. Eng. Sci. 23, 575–591 (1968)
Cassanello, M., Larachi, F., Laurent, A., Wild, G., Midoux, N.: Gas-liquid mass transfer in high pressure trickle-bed reactors: experiments and modelling. In: von Rohr, P.R., Trepp, C. (Hrsg.) High Pressure Chemical Engineering, Bd. 12, S. 493–498. Elsevier, Amsterdam (1996)
Castellari, A.T., Haure, P.M.: Experimental study of the periodic operation of a trickle-bed reactor. AIChE J. 41, 1593–1597 (1995)
Chan, J.-C., Tan, C.-S.: Hydrogenation of tetralin over Pt/γ-Al2O3 in trickle-bed reactor in the presence of compressed CO2. Energy Fuel 20, 771–777 (2006)
Charpentier, J.C., Favier, M.: Some liquid holdup experimental data in trickle-bed reactors for foaming and nonfoaming hydrocarbons. AIChE J. 21, 1213–1218 (1975)
Chaudhari, R.V., Jaganathan, R., Mathew, S.P., Julcour, C., Delmas, H.: Hydrogenation of 1,5,9-cyclododecatriene in fixed-bed reactors: down- vs. upflow modes. AIChE J. 48, 110–125 (2002)
Chaudhari, R.V., Ramachandran, P.A.: Three-phase slurry reactors. AIChE J. 26, 177–201 (1980)
Colombo, A.J., Baldi, G., Sicardi, S.: Solid-liquid contacting effectiveness in trickle bed reactors. Chem. Eng. Sci. 31, 1101–1108 (1976)
Couto, C.S., Madeira, L.M., Nunes, C.P., Araújo, P.: Liquid-phase hydrogenation of nitrobenzene in a tubular reactor: parametric study of the operating conditions influence. Ind. Eng. Chem. Res. 56, 3231–3242 (2017)
Crine, M.: Heat-transfer phenomena in trickle-bed reactors. Chem. Eng. Commun. 19, 99–114 (1982)
Crine, M., Marchot, P.: Measuring dynamic liquid holdup in trickle-bed reactors under actual operating conditions. Chem. Eng. Commun. 8, 365–371 (1981)
Cybulski, A., Moulijn, J.A.: Structured Catalysts and Reactors, 2. Aufl. Taylor & Francis, Boca Raton (2006)
Dashliborun, A.M., Härting, H.-U., Schubert, M., Larachi, F.: Process intensification of gas-liquid downflow and upflow packed beds by a new low-shear rotating reactor concept. AIChE J. 63, 283–294 (2017)
Dashliborun, A.M., Larachi, F.: CFD study and experimental validation of multiphase packed bed hydrodynamics in the context of rolling sea conditions. AIChE J. 65, 385–397 (2019)
Datsevich, L.B., Mukhortov, D.A.: Pre-saturation in multiphase fixed-bed reactors as a method for process intensification/reactor minimization. Catal. Today 120, 71–77 (2007)
Dhiman, S.K., Verma, V., Rao, D.P., Rao, M.S.: Process intensification in a trickle-bed reactor: experimental studies. AIChE J. 51, 3186–3192 (2005)
Dietrich, W., Grünewald, M., Agar, D.W.: Dynamic modelling of periodically wetted catalyst particles. Chem. Eng. Sci. 60, 6254–6261 (2005)
Dixon, A.G., Nijemaisland, M., Stitt, E.H.: Packed tubular reactor modelling and catalyst design using computational fluid dynamics. Adv. Chem. Eng. 31, 307–389 (2006)
Dudas, J., Hanika, J., Lepuru, J., Barkhuysen, M.: Thymol hydrogenation in bench scale trickle bed reactor. Chem. Biochem. Eng. Q. 19, 255–262 (2005)
Dudukovic, M.P., Larachi, F., Mill, P.L.: Multiphase catalytic reactors: a perspective on current knowledge and future trends. Catal. Rev. 44, 123–246 (2002)
Dudukovic, M.P., Mills, P.L.: Contacting and hydrodynamics in trickle-bed reactors. In: Cheremisinoff, N.P. (Hrsg.) Encyclopedia of Fluid Mechanics, Bd. 3, S. 969–1017. Gulf Publishing, Houston (1986)
Edvinsson, A.R., Nyström, M., Siverström, M., Sellin, A., Dellve, A.-C., Andersson, U., Herrmann, W., Berglin, T.: Development of a monolith-based process for H2O2 production: from idea to large-scale implementation. Catal. Today 69, 247–252 (2001)
El-Hisnawi, A.A., Dudukovic, M.P., Mills, P.L.: Trickle-bed reactors – dynamic tracer tests, reaction studies, and modeling of reactor performance. ACS Symp. Ser. 196, 421–440 (1982)
Ellman, M.J., Midoux, N., Laurent, A., Charpentier, J.C.: A new, improved pressure-drop correlation for trickle-bed reactors. Chem. Eng. Sci. 43, 2201–2206 (1988)
Ellman, M.J., Midoux, N., Wild, G., Laurent, A., Charpentier, J.C.: A new, improved liquid hold-up correlation for trickle-bed reactors. Chem. Eng. Sci. 45, 1677–1684 (1990)
Enache, D.I., Landon, P., Lok, C.M., Pollington, S.D., Stitt, E.H.: Direct comparison of a trickle bed and a monolith for hydrogenation of pyrolysis gasoline. Ind. Eng. Chem. Res. 44, 9431–9439 (2005)
Fahien, R.W., Stankovic, I.M.: An equation for the velocity profile in packed columns. Chem. Eng. Sci. 34, 1350–1354 (1979)
Fordham, P., Besson, M., Gallezot, P.: Selective catalytic oxidation with air of glycerol and oxygenated derivatives on platinum metals. In: Hightower, J., Delgass, W.N., Iglesia, E., Bell, A.T. (Hrsg.) Studies in Surface Science and Catalysis, Bd. 101, S. 161–170. Elsevier, Amsterdam (1996)
Fortuny, A., Font, J., Fabregat, A.: Wet air oxidation of phenol using active carbon as catalyst. Appl Catal B. 19, 165–173 (1998)
Freund, H., Lämmermann, M., Busse, C., Schwieger, W.: Additive manufacturing of tailor-made catalytic reactors for single phase and multiphase reaction systems. 25th international symposium on chemical reaction engineering, Florence (2018)
Fu, M.S., Tan, C.S.: Liquid holdup and axial dispersion in trickle-bed reactors. Chem. Eng. Sci. 51, 5357–5361 (1996)
Fukushima, S., Kusaka, K.: Interfacial area and boundary of hydrodynamic flow region in packed column with concurrent downward flow. J. Chem. Eng. Jpn. 10, 461–467 (1977a)
Fukushima, S., Kusaka, K.: Liquid-phase volumentric and mass-transfer coefficient and boundary of hydrodynamic flow region in packed-column with concurrent downward flow. J. Chem. Eng. Jpn. 10, 468–474 (1977b)
Gallezot, P., Nicolaus, N., Flèche, G., Fuertes, P., Perrard, A.: Glucose hydrogenation on ruthenium catalysts in a trickle-bed reactor. J. Catal. 180, 51–55 (1998)
Garcia, G.E.C., van der Schaaf, J., Kiss, A.A.: A review on process intensification in HiGee distillation. J. Chem. Eng. Technol. Biotechnol. 92, 1136–1156 (2017)
Garcia-Serna, J., Gallina, G., Biasi, P., Salmi, T.: Liquid holdup by gravimetric recirculation continuous measurement method. Application to trickle bed reactors under pressure at laboratory scale. Ind. Eng. Chem. Res. 56, 13.295–13.301 (2017)
Gascon, J., van Ommen, J.R., Moulijn, J.A., Kapteijn, F.: Structuring catalyst and reactor – an inviting avenue to process intensification. Cat. Sci. Technol. 5, 807–817 (2015)
Gelhausen, M.G., Yang, S.Q., Cegla, M., Agar, D.W.: Cyclic mass transport phenomena in a novel reactor for gas-liquid-solid contacting. AIChE J. 63, 208–215 (2017)
Germain, A.H., LeFebvre, A.G., L’Homme, G.A.: Experimental study of a catalytic trickle bed reactor. Adv. Chem. Ser. 133, 164–180 (1974)
Gianetto, A., Berruti, F.: Modelling of trickle bed reactors. In: de Lasa, H.I. (Hrsg.) Chemical Reactor Design and Technology NATO ASI Series 110, S. 631–685. Springer, Dordrecht (1986)
Gianetto, A., Specchia, V.: Trickle-bed reactors – state of art and perspectives. Chem. Eng. Sci. 47, 3197–3213 (1992)
Gianetto, A., Specchia, V., Baldi, G.: Absorption in packed towers with concurrent downward high-velocity flows. 2. Mass-transfer. AIChE J. 19, 916–922 (1973)
Gierman, H.: Design of laboratory hydrotreating reactors – scaling down of trickle-flow reactors. Appl. Catal. 43, 277–286 (1988)
Gladden, L.F., Lim, M.H.M., Mantle, M.D., Sederman, A.J., Stitt, E.H.: MRI visualisation of two-phase flow in structured supports and trickle-bed reactors. Catal. Today 79, 203–210 (2003)
Goto, S., Chatani, T., Matouq, M.H.: Hydration of 2-methyl-2-butene in gas-liquid cocurrent upflow and downflow reactors. Can. J. Chem. Eng. 71, 821–823 (1993)
Goto, S., Levec, J., Smith, J.M.: Mass-transfer in packed-beds with two-phase flow. Ind. Eng. Chem. Proc. Des. Dev. 14, 473–478 (1975)
Goto, S., Smith, J.M.: Trickle-bed reactor performance. 1. Holdup and mass-transfer effects. AIChE J. 21, 706–713 (1975)
Govindarao, V.M.H., Fromet, G.F.: Voidage profiles in packed beds of spheres. Chem. Eng. Sci. 41, 553–539 (1986)
Govindarao, V.M.H., Murthy, K.V.R.: Liquid-phase hydrogenation of aniline in a trickle bed reactor. J. Appl. Chem. Biotechnol. 25, 169–181 (1975)
Grosser, K., Carbonell, R.G., Sundaresan, S.: Onset of pulsing in two-phase concurrent downflow through a packed-bed. AIChE J. 34, 1850–1860 (1988)
Gunjal, P.R., Kashid, M.N., Ranade, V.V., Chaudhari, R.V.: Hydrodynamics of trickle-bed reactors: experiments and CFD modeling. Ind. Eng. Chem. Res. 44(16), 6278–6294 (2005)
Gunjal, P.R., Ranade, V.V.: Modeling of laboratory and commercial scale hydro-processing reactors using CFD. Chem. Eng. Sci. 62, 5512–5526 (2007)
Gupta, R.: Pulsed flow vapor-liquid reactors. U.S. Patent 4,526,757 (1985)
Hamidipour, M., Larachi, F., Ring, Z.: Monitoring filtration in trickle beds using electrical capacitance tomography. Ind. Eng. Chem. Res. 48, 1140–1153 (2009)
Hampel, U., Dittmeyer, R., Patyk, A., Wetzel, T., Lange, R., Freund, H., Schwieger, W., Grünewald, M., Schlüter, M., Petasch, U.: The Helmholtz Energy Alliance „Energy efficient multiphase chemical processes“. Chem. Ing. Tech. 85, 992–996 (2013)
Hanika, J., Kucharova, M., Kolena, J., Smejkal, Q.: Multi-functional trickle bed reactor for butylacetate synthesis. Catal. Today 79, 83–87 (2002)
Härting, H.-U., Berger, R., Lange, R., Larachi, F., Schubert, M.: Liquid backmixing in an inclined rotating tubular fixed bed reactor – augmenting liquid residence time via flow regime adjustment. Chem. Eng. Process. 94, 2–10 (2015c)
Härting, H.-U., Bieberle, A., Lange, R., Larachi, F., Schubert, M.: Hydrodynamics of co-current two-phase flow in an inclined rotating tubular fixed bed reactor – wetting intermittency via periodic catalyst immersion. Chem. Eng. Sci. 128, 147–158 (2015b)
Härting, H.-U., Lange, R., Larachi, F., Schubert, M.: A novel inclined rotating tubular fixed bed reactor concept for enhancement of reaction rates and adjustment of flow regimes. Chem. Eng. J. 281, 931–944 (2015a)
Hashimoto, K., Muroyama, K., Fujiyoshi, K., Nagata, S.: Effective radial thermal conductivity in concurrent flow of a gas and liquid through a packed bed. Int. Chem. Eng. 16, 720–727 (1976)
Haure, P., Silveston, P.L., Hudgins, R.R., Bellut, M.: Conversion efficiency in trickle bed reactors. U.S. Patent 5,011,675 (1988)
Hochman, J.M., Efron, E.: Two-phase cocurrent downflow in packed beds. Ind. Eng. Chem. Fundam. 8, 63–71 (1969)
Hofmann, H.: Hydrodynamics, transport phenomena, and mathematical models in trickle-bed reactors. Int. Chem. Eng. 17, 19–28 (1977)
Holub, R.A., Dudukovic, M.P., Ramachandran, P.A.: A phenomenological model of pressure drop, liquid hold-up and flow regime transition in gas-liquid trickle flow. Chem. Eng. Sci. 47, 2343–2348 (1992)
Honda, G.S., Lehmann, E., Hickman, D.A., Varma, A.: Effects of prewetting on bubbly- and pulsing-flow regime transitions in trickle-bed reactors. Ind. Eng. Chem. Res. 54, 10.253–10.259 (2015)
Houwelingen, A.J. van, Nicol, W.: Parallel hydrogenation for the quantification of wetting efficiency and liquid-solid mass transfer in a trickle-bed reactor. AIChE J. 57, 1310–1319 (2011)
Houwelingen, A. J. van, Sandrock, C., Nicol, W.: Particle wetting distribution in trickle-bed reactors. AIChE J. 52, 3532–3542 (2006)
Huang, T.-C., Kang, B.-C.: Kinetic study of naphthalene hydrogenation over Pt/Al2O3 catalyst. Ind. Eng. Chem. Res. 34, 1140–1148 (1995)
Huang, X., Varma, A., McCready, M.J.: Heat transfer characterization of gas-liquid flows in a trickle-bed. Chem. Eng. Sci. 59, 3767–3776 (2004)
Iliuta, I., Aydin, B., Larachi, F.: Onset of pulsing in trickle beds with non-Newtonian liquids at elevated temperature and pressure – modeling and experimental verification. Chem. Eng. Sci. 61, 526–537 (2006)
Iliuta, I., Bozga, G., Lupascu, M.: Liquid-phase alkylation of benzene with propylene catalysed by HY zeolites. Chem. Eng. Technol. 24, 933–944 (2001)
Iliuta, I., Larachi, F., Al-Dahhan, M.H.: Double-slit model for partially wetted trickle flow hydrodynamics. AIChE J. 46, 597–609 (2000)
Janecki, D., Burghardt, A., Bartelmus, G.: Computational simulation of the hydrodynamic parameters of a trickle-bed reactor operating at periodically changing feeding the bed with liquid. Chem. Process. Eng. 29, 583–596 (2008)
Jiang, Y., Khadilkar, M.R., Al-Dahhan, M.H., Dudukovic, M.P.: CFD modeling of multiphase flow distribution in catalytic packed bed reactors: scale down issues. Catal. Today 66, 209–218 (2001)
Jiang, Y., Khadilkar, M.R., Al-Dahhan, M.H., Dudukovic, M.P.: CFD of multiphase flow in packed-bed reactors: I. k-fluid modeling issues. AIChE J. 48, 701–715 (2002a)
Jiang, Y., Khadilkar, M.R., Al-Dahhan, M.H., Dudukovic, M.P.: CFD of multiphase flow in packed-bed reactors: II. Results and application. AIChE J. 48, 716–730 (2002b)
Joubert, R., Nicol, W.: Trickle flow liquid-solid mass transfer and wetting efficiency in small diameter columns. Can. J. Chem. Eng. 91, 441–447 (2013)
Julcour-Lebigue, C., Baussaron, L., Delmas, H., Wilhelm, A.-M.: Theoretical analysis of tracer method for the measurement of wetting efficiency. Chem. Eng. Sci. 62, 5374–5379 (2007)
Kan, K.M., Greenfield, P.F.: Multiple hydrodynamic states in concurrent two-phase downflow through packed-beds. Ind. Eng. Chem. Process Des. Dev. 17(4), 482–485 (1978)
Kan, K.M., Greenfield, P.F.: Pressure-drop and holdup in two-phase concurrent trickle flows through beds of small packings. Ind. Eng. Chem. Process. Des. Dev. 18, 740–746 (1979)
Kang, S.-H., Bae, J.W., Cheon, J.-Y., Lee, Y.-J., Ha, K.-S., Jun, K.-W., Lee, D.-H., Kim, B.-W.: Catalytic performance on iron-based Fischer-Tropsch catalyst in fixed-bed and bubbling fluidized-bed reactor. Appl Catal B. 103(1–2), 169–180 (2011)
Kawase, Y., Ulbrecht, J.J.: Motion of and mass-transfer from an assemblage of solid spheres moving in a non-Newtonian fluid at high Reynolds numbers. Chem. Eng. Commun. 8, 233–249 (1981)
Keil, F.J.: Process intensification. Rev. Chem. Eng. 34, 135–200 (2018)
Khadilkar, M.R., Al-Dahhan, M.H., Dudukovic, M.P.: Parametric study of unsteady-state flow modulation in trickle-bed reactors. Chem. Eng. Sci. 54, 2585–2595 (1999)
Klinken, J. van, van Dongen, R.H.: Catalyst dilution for improved performance of laboratory trickle-flow reactors. Chem. Eng. Sci. 35, 59–66 (1980)
Kolb, W.B., Melli, T.R., Desantos, J.M., Scriven, L.E.: Cocurrent downflow in packed-beds – flow regimes and their acoustic signatures. Ind. Eng. Chem. Res. 29, 2380–2389 (1990)
Korsten, H., Hoffmann, U.: Three-phase reactor model for hydrotreating in pilot trickle-bed reactors. AIChE J. 42, 1350–1360 (1996)
Kulkarni, R.R., Wood, J., Winterbottom, J.M., Stitt, E.H.: Effect of fines and porous catalyst on hydrodynamics of trickle bed reactors. Ind. Eng. Chem. Res. 44, 9497–9501 (2005)
Kundu, A., Nigam, K.D.P., Verma, R.P.: Catalyst wetting characteristics in trickle-bed reactors. AIChE J. 49, 2253–2263 (2003)
Kundu, A., Saroha, A.K., Nigam, K.D.P.: Liquid distribution studies in trickle-bed reactors. Chem. Eng. Sci. 56, 5963–5967 (2001)
Kunii, D., Suzuki, M.: Particle-to-fluid heat and mass transfer in packed beds of fine particles. Int. J. Heat Mass Transf. 10, 845–852 (1967)
Kunzle, S., Soler, J.W., Baiker, A.: Continuous enantioselective hydrogenation in fixed-bed reactor: towards process intensification. Catal. Today 79, 503–509 (2003)
Lamine, A.S., Gerth, L., LeGall, H., Wild, G.: Heat transfer in a packed bed reactor with cocurrent downflow of a gas and a liquid. Chem. Eng. Sci. 51, 3813–3827 (1996)
Lämmermann, M., Horak, G., Schwieger, W., Freund, H.: Periodic open cellular structures (POCS) for intensification of multiphase reactors: liquid holdup and two-phase pressure drop. Chem. Eng. Process. 126, 178–189 (2018)
Lange, R., Hanika, J., Stradiotto, D., Hudgins, R.R., Silveston, P.L.: Investigations of periodically operated trickle-bed reactors. Chem. Eng. Sci. 49, 5615–5621 (1994)
Lange, R., Schubert, M., Dietrich, W., Grünewald, M.: Unsteady-state operation of trickle-bed reactors. Chem. Eng. Sci. 59, 5355–5361 (2004)
Lappalainen, K., Manninen, M., Alopaeus, V.: CFD modeling of radial spreading of flow in trickle-bed reactors due to mechanical and capillary dispersion. Chem. Eng. Sci. 64, 207–218 (2009)
Larachi, F., Belfares, L., Grandjean, B.P.A.: Prediction of liquid-solid wetting efficiency in trickle flow reactors. Int. Commun. Heat Mass Transf. 28, 595–603 (2001)
Larachi, F., Belfares, L., Iliuta, I., Grandjean, B.P.A.: Heat and mass transfer in cocurrent gas-liquid packed beds. Analysis, recommendations, and new correlations. Ind. Eng. Chem. Res. 42, 222–242 (2003)
Larachi, F., Cassanello, M., Laurent, A.: Gas-liquid interfacial mass transfer in trickle-bed reactors at elevated pressures. Ind. Eng. Chem. Res. 37, 718–733 (1998)
Larachi, F., Iliuta, I., Chen, M., Grandjean, B.P.A.: Onset of pulsing in trickle beds: evaluation of current tools and state-of-the-art correlation. Can. J. Chem. Eng. 77, 751–758 (1999)
Larachi, F., Laurent, A., Midoux, N., Wild, G.: Experimental study of a trickle-bed reactor operating at high-pressure – two-phase pressure drop and liquid saturation. Chem. Eng. Sci. 46, 1233–1246 (1991)
Larachi, F., Laurent, A., Wild, G., Midoux, N.: Effect of pressure on trickle-to-pulse transition in catalytic trickle-bed reactors. Can. J. Chem. Eng. 71, 319–321 (1993)
Latifi, M.A., Rode, S., Midoux, N., Storck, A.: The use of microelectrodes for the determination of flow regimes in a trickle-bed reactor. Chem. Eng. Sci. 47, 1955–1961 (1992)
Lazzaroni, C.L., Keselman, H.R., Figoli, N.S.: Trickle bed reactors – multiplicity of hydrodynamic states – relation between the pressure-drop and the liquid holdup. Ind. Eng. Chem. Res. 28, 119–121 (1989)
Leung, P.C., Recasens, F., Smith, J.M.: Hydration of isobutene in a trickle-bed reactor – wetting efficiency and mass-transfer. AIChE J. 33, 996–1007 (1987)
Levec, J., Smith, J.M.: Oxidation of acetic-acid solutions in a trickle-bed reactor. AIChE J. 22, 159–168 (1976)
Li, Y.X., Cheng, Z.M., Liu, L.H., Yuan, W.K.: Catalytic oxidation of dilute SO2 over activated carbon coupled with partial liquid phase vaporization. Chem. Eng. Sci. 54, 1571–1576 (1999)
Liu, G., Mi, Z., Wang, L., Zhang, X., Zhang, S.: Hydrogenation of dicyclopentadiene into endo-tetrahydrodicyclopentadiene in trickle-bed reactor: experiments and modeling. Ind. Eng. Chem. Res. 45, 8807–8814 (2006)
Liu, G.Z., Duan, Y., Wang, Y.Q., Wang, L., Mi, Z.T.: Periodically operated trickle-bed reactor for EAQs hydrogenation: experiments and modeling. Chem. Eng. Sci. 60, 6270–6278 (2005)
Liu, G.Z., Lan, J.A., Cao, Y.B., Huang, Z.B., Cheng, Z.M., Mi, Z.T.: New insights into transient behaviors of local liquid-holdup in periodically operated trickle-bed reactors using electrical capacitance tomography (ECT). Chem. Eng. Sci. 64, 3329–3343 (2009)
Llano, J.J., Rosal, R., Sastre, H., Diez, F.V.: Determination of wetting efficiency in trickle-bed reactors by a reaction method. Ind. Eng. Chem. Res. 36, 2616–2625 (1997)
Lopes, R.J.G., Quinta-Ferreira, R.M.: Trickle-bed CFD studies in the catalytic wet oxidation of phenolic acids. Chem. Eng. Sci. 62, 7045–7052 (2007)
Lopes, R.J.G., Quinta-Ferreira, R.M.: Volume-of-Fluid-based model for multiphase flow in high-pressure trickle-bed reactor: optimization of numerical parameters. AIChE J. 55, 2920–2933 (2009a)
Lopes, R.J.G., Quinta-Ferreira, R.M.: CFD modelling of multiphase flow distribution in trickle beds. Chem. Eng. J. 147, 342–355 (2009b)
Lopes, R.J.G., Quinta-Ferreira, R.M.: Assessment of CFD-VOF method for trickle-bed reactor modeling in the catalytic wet oxidation of phenolic wastewaters. Ind. Eng. Chem. Res. 49, 2638–2648 (2010a)
Lopes, R.J.G., Quinta-Ferreira, R.M.: Hydrodynamic simulation of pulsing-flow regime in high-pressure trickle-bed reactors. Ind. End. Chem. Res. 49, 1105–1112 (2010b)
Lopes, R.J.G., Quinta-Ferreira, R.M.: Assessment of CFD Euler-Euler method for trickle-bed reactor modelling in the catalytic wet oxidation of phenolic wastewaters. Chem. Eng. J. 160, 293–301 (2010c)
Maiti, R.N., Nigam, K.D.P.: Gas-liquid distributors for trickle-bed reactors: a review. Ind. Eng. Chem. Res. 46, 6164–6182 (2007)
Marcandelli, C., Wild, G., Lamine, A.S., Bernard, J.R.: Measurement of local particle–fluid heat transfer coefficient in trickle-bed reactors. Chem. Eng. Sci. 54, 4997–5002 (1999)
Mariani, N.J., Martinez, O.M., Barreto, G.F.: Evaluation of heat transfer parameters in packed beds with cocurrent downflow of liquid and gas. Chem. Eng. Sci. 56, 5995–6001 (2001)
Martin, H.: Low Péclet number particle-to-fluid heat and mass transfer in packed beds. Chem. Eng. Sci. 33, 913–919 (1978)
Mary, G., Chaouki, J., Luck, F.: Trickle-bed laboratory reactors for kinetic studies. Int. J. Chem. React. Eng. 7, 1542–1580 (2009)
Matsuura, A., Hitaka, Y., Akehata, T., Shirai, T.: Apparent wall heat transfer coefficient in packed beds with downward cocurrent gas-liquid flow. Heat Transfer Jpn. Res. 8, 53–60 (1979)
Maugans, C.B., Akgerman, A.: Catalytic wet oxidation of phenol in a trickle bed reactor over a Pt/TiO2 catalyst. Water Res. 37, 319–328 (2002)
Mears, D.E.: The role of axial dispersion in trickle-flow laboratory reactors. Chem. Eng. Sci. 26, 1361–1366 (1971a)
Mears, D.E.: Diagnostic criteria for heat transport limitations in fixed bed reactors. J. Catal. 20, 127–131 (1971b)
Mears, D.E.: Role of liquid holdup and effective wetting in performance of trickle-bed reactors. Adv. Chem. Ser. 133, 218–227 (1974)
Mears, D.E.: On criteria for axial dispersion in nonisothermal packed-bed catalytic reactors. Ind. Eng. Chem. Fundam. 15, 20–23 (1976)
Mederos, F.S., Elizalde, I., Ancheyta, J.: Steady-state and dynamic reactor models for hydrotreatment of oil fractions: a review. Catal. Rev. Sci. Eng. 51, 485–607 (2009)
Merchan, A., Emig, G., Hofmann, H., Chaudhari, R.V.: Zur Frage des Katalysator-Wirkungsgrades bei Folge-Reaktionen in Mehrphasensystemen. Chem. Ing. Tech. 58, 50–53 (1986)
Merwe, W. van der, Nicol, W.: Characterization of multiple flow morphologies within the trickle flow regime. Ind. Eng. Chem. Res. 44, 9446–9450 (2005)
Merwe, W. van der, Nicol, W.: Trickle flow hydrodynamic multiplicity: experimental observations and pore-scale capillary mechanism. Chem. Eng. Sci. 64, 1267–1284 (2009)
Metaxas, K.C., Papayannakos, N.G.: Kinetics and mass transfer of benzene hydrogenation in a trickle-bed reactor. Ind. Eng. Chem. Res. 45, 7110–7119 (2006)
Meyers, R.A.: Handbook of Petroleum Refining Processes, 3. Aufl. McGraw-Hill Education, New York (2003)
Michell, R.W., Furzer, I.A.: Trickle flow in packed-beds. Trans. Inst. Chem. Eng. 50, 334–342 (1972)
Mogalicherla, A.K., Sharma, G., Kunzru, D.: Estimation of wetting efficiency in trickle-bed reactors for nonlinear kinetics. Ind. Eng. Chem. Res. 48, 1443–1450 (2009)
Morsi, B.I., Laurent, A., Midoux, N., Barthole-Delaunay, G., Storck, A., Charpentier, J.C.: Hydrodynamics and gas-liquid-solid interfacial parameters of co-current downward two-phase flow in trickle-bed reactors. Chem. Eng. Commun. 25, 267–293 (1984)
Mülheims, P., Kraushaar-Czarnetzki, B.: Temperature profiles and process performances of sponge packings as compared to spherical catalysts in the oxidation of o-xylene to phthalic anhydride. Ind. Eng. Chem. Res. 50, 9925–9935 (2011)
Muroyama, K., Hashimoto, K., Tomita, T.: Heat transfer from wall in gas-liquid cocurrent packed beds. Kagaku Kokaku Ronbun. 3, 612–616 (1977)
Nakayama, A., Kuwahara, F.: A general macroscopic turbulence model for flows in packed beds, channels, pipes and rod bundles. J. Fluids Eng. 130, 1–7 (2008)
Nelson, P.A., Galloway, T.R.: Particle-to-fluid heat and mass transfer in dense systems of fine particles. Chem. Eng. Sci. 30, 1–6 (1975)
Ng, K.M.: A model for flow regime transitions in cocurrent downflow trickle-bed reactors. AIChE J. 32, 115–122 (1986)
Nicol, W., Joubert, R.: Liquid-solid mass transfer distributions in trickle bed reactors. Chem. Eng. J. 230, 361–366 (2013)
Nigam, K.D.P., Larachi, F.: Process intensification in trickle-bed reactors. Chem. Eng. Sci. 60, 5880–5894 (2005)
Nishizawa, A., Kitano, T., Ikenaga, N., Miyake, T., Suzuki, T.: Use of trickle bed reactor for Fischer-Tropsch reaction over Co-Mn/oxidized diamond catalyst. J. Jpn. Petrol. Inst. 57, 109–117 (2014)
Perego, C., Peratello, S.: Experimental methods in catalytic kinetics. Catal. Today 52, 133–145 (1999)
Pintar, A., Batista, J.: Catalytic hydrogenation of aqueous nitrate solutions in fixed-bed reactors. Catal. Today 53, 35–50 (1999)
Pintar, A., Batista, J., Tisler, T.: Catalytic wet-air oxidation of aqueous solutions of formic acid, acetic acid and phenol in a continuous-flow trickle-bed reactor over Ru/TiO2 catalysts. Appl Catal B. 84, 30–41 (2008)
Pironti, F., Mizrahi, D., Acosta, A., Gonzalez-Mendizabal, D.: Liquid-solid wetting factor in trickle-bed reactors: its determination by a physical method. Chem. Eng. Sci. 54, 3793–3800 (1999)
Rajashekharam, M.V., Jaganathan, R., Chaudhari, R.V.: A trickle-bed reactor model for hydrogenation of 2,4 dinitrotoluene: experimental verification. Chem. Eng. Sci. 53, 787–805 (1998)
Ramachandran, P.A., Dudukovic, M.P., Mills, P.L.: A new model for assessment of external liquid-solid contacting in trickle-bed reactors from tracer response measurements. Chem. Eng. Sci. 41, 855–860 (1986)
Ramachandran, P.A., Smith, J.M.: Effectiveness factors in trickle-bed reactors. AIChE J. 25, 538–542 (1979)
Ramirez, L.F., Escobar, J., Galvan, E., Vaca, H., Murrieta, F.R., Luna, M.R.S.: Evaluation of diluted and undiluted trickle-bed hydrotreating reactor with different catalyst volume. Pet. Sci. Technol. 22, 157–175 (2004)
Ranade, V.V., Chaudhari, R.V., Gunjal, R.R.: Trickle bed reactors. Reactor Engineering and Applications, 1. Aufl. Elsevier, Amsterdam (2011)
Ring, Z.E., Missen, R.W.: Trickle-bed reactors – tracer study of liquid holdup and wetting efficiency at high temperature and pressure. Can. J. Chem. Eng. 69, 1016–1020 (1991)
Saez, A.E., Carbonell, R.G.: Hydrodynamic parameters for gas-liquid cocurrent flow in packed-beds. AIChE J. 31, 52–62 (1985)
Saroha, A.K., Nigam, K.D.P.: Trickle bed reactors. Rev. Chem. Eng. 12, 207–347 (1996)
Sato, Y., Hirose, T., Takahasi, F., Toda, M., Hashiguchi, Y.: Flow pattern and pulsation properties of cuocurrent gas-liquid downflow in packed beds. J. Chem. Eng. Jpn. 6, 315–319 (1973)
Satterfield, C.N.: Trickle-bed reactors. AIChE J. 21, 209–228 (1975)
Satterfield, C.N., Pelossof, A.A., Sherwood, T.K.: Mass transfer limitations in a trickle-bed reactor. AIChE J. 15, 226–234 (1969)
Satterfield, C.N., Way, P.F.: Role of liquid-phase in performance of a trickle bed reactor. AIChE J. 18, 305–311 (1972)
Schubert, M.: Festbettreaktor. DE 10 2018 110 091.4 (2018)
Schubert, M., Bauer, T., Lange, R.: Instationäre Betriebsweise zur Leistungssteigerung technischer Rieselbettreaktoren. Chem. Ing. Technik. 78, 1023–1032 (2006)
Schubert, M., Hamidipour, M., Duchesne, C., Larachi, F.: Hydrodynamics of cocurrent two-phase flows in slanted porous media – modulation of pulse flow via bed obliquity. AIChE J. 56, 3189–3205 (2010a)
Schubert, M., Hessel, G., Zippe, C., Lange, R., Hampel, U.: Liquid flow texture analysis in trickle bed reactors using high-resolution gamma ray tomography. Chem. Eng. J. 140, 332–340 (2008)
Schubert, M., Kryk, H., Hampel, U.: Slow-mode gas/liquid-induced periodic hydrodynamics in trickling packed beds derived from direct measurement of cross-sectional distributed local capacitances. Chem. Eng. Process. 49, 1107–1121 (2010b)
Sederman, A.J., Gladden, L.F.: Magnetic resonance imaging as a quantitative probe of gas-liquid distribution and wetting efficiency in trickle-bed reactors. Chem. Eng. Sci. 56, 2615–2628 (2001)
Shah, Y.T., Paraskos, J.A.: Criteria for axial dispersion effects in adiabatic trickle bed hydroprocessing reactors. Chem. Eng. Sci. 30, 1169–1176 (1976)
Sicardi, S., Hofmann, H.: Influence of gas velocity and packing geometry on pulsing inception in trickle-bed reactors. Chem. Eng. J. 20, 251–253 (1980)
Sie, S.T.: Scale effects in laboratory and pilot-plant reactors for trickle-flow processes. Rev. Inst. Fr. du Pet. 46, 501–515 (1991)
Sie, S.T., Krishna, R.: Process development and scale up: III. Scale-up and scale-down of trickle bed processes. Rev. Chem. Eng. 14, 203–252 (1988)
Sie, S.T., Krishna, R.: Process development and scale up: III. Scale-up and scale-down of trickle bed processes. Rev. Chem. Eng. 14, 203–252 (1998)
Silveston, P.L., Hudgins, R.R.: Periodic Operation of Chemical Reactors, 1. Aufl. Elsevier, Butterworth-Heinemann (2013)
Singh, B.K., Jain, E., Buwa, V.V.: Feasibility of electrical resistance tomography for measurements of liquid holdup distribution in a trickle bed reactor. Chem. Eng. J. 358, 564–579 (2019)
Sokolov, V. N., Yablokova, M. A., Krylov, V. N.: 1983, Heat transfer to the wall in a gas-liquid reactor with stationary granular bed. J. Appl. Chem. USSR (Zh. Prikl. Khim.) 56, 554–558 (1983)
Specchia, V., Baldi, G.: Heat-transfer in trickle-bed reactors. Chem. Eng. Commun. 3, 483–499 (1979)
Specchia, V., Baldi, G., Gianetto, A.: Solid-liquid mass transfer in concurrent two-phase flow through packed-beds. Ind. Eng. Chem. Proc. Des. Dev. 17, 362–367 (1978)
Stanek, V., Hanika, J.: The effect of liquid flow distribution on catalytic hydrogenation of cyclohexene in an adiabatic trickle-bed reactor. Chem. Eng. Sci. 37, 1283–1288 (1982)
Storsaeter, S., Borg, O., Blekkan, E.A., Holmen, A.: Study of the effect of water on Fischer-Tropsch synthesis over supported cobalt catalysts. J. Catal. 231, 405–419 (2005)
Stradiotto, D.A., Hudgins, R.R., Silveston, P.L.: Hydrogenation of crotonaldehyde under periodic flow interruption in a trickle bed. Chem. Eng. Sci. 54, 2561–2568 (1999)
Subramanian, K., Winkler, M., Harting, H.-U., Schubert, M.: Prediction of flow patterns of rotating inclined reactors by using a modified permeability approach. Chem. Eng. Technol. 39, 2077–2086 (2016)
Subramanian, K., Zalucky, J., Schubert, M., Lucas, D., Hampel, U.: An Eulerian-Eulerian computational approach for simulating descending gas-liquid flows in reactors with solid foam internals. Chem. Eng. Technol. 40, 2044–2057 (2017)
Tan, C.S., Smith, J.M.: A dynamics method for liquid-particle mass-transfer in trickle beds. AIChE J. 28, 190–195 (1982)
Teruel, F.E., Rizwan-uddina: A new turbulence model for porous media flows. Part I: constitutive equations and model closure. Int. J. Heat Mass Transf. 52, 4264–4272 (2009)
Tukač, V., Šimíčková, M., Chyba, V., Lederer, J., Kolena, J., Hanika, J., Jiřičný, V., Staněk, V., Stavárek, P.: The behavior of pilot trickle-bed reactor under periodic operation. Chem. Eng. Sci. 62, 4891–4895 (2007)
Uraz, C., Atalay, F.S., Atalay, S.: Catalytic hydrogenation of crotonaldehyde in trickle-bed reactor. Chem. Biochem. Eng. Q. 18, 373–383 (2004)
Urrutia, G., Bonelli, P., Cassanello, M.C., Cassanello, A.L., Cukierman, A.L.: On dynamic liquid holdup determination by the drainage method. Chem. Eng. Sci. 51, 3721–3726 (1996)
Urseanu, M.I., Boelhouwer, J.G., Bosman, H.J.M., Schroijen, J.C., Kwant, G.: Estimation of trickle-to-pulse flow regime transition and pressure drop in high-pressure trickle bed reactors with organic liquids. Chem. Eng. J. 111, 5–11 (2005)
Utikar, R.P., Ranade, V.V.: Intensifying multiphase reactions and reactors: strategies and examples. ACS Sustain. Chem. Eng. 5, 3607–3622 (2017)
Wache, W., Datsevich, L.B., Jess, A.: Fischer-tropsch synthesis in a two-phase reactor with presaturation. Oil Gas-Eur. Mag. 33, 35–38 (2007)
Wache, W., Datsevich, L.B., Jess, A., Neumann, G.: Improved deep desulphurisation of middle distillates by a two-phase reactor with pre-saturator. Fuel 85, 1483–1493 (2006)
Wakao, N., Funazkri, T.: Effect of fluid dispersion coefficients on particle-to-fluid mass-transfer coefficients in packed-beds – correlation of Sherwood numbers. Chem. Eng. Sci. 33, 1375–1384 (1978)
Wang, Y., Chen, J., Larachi, F.: Modelling and simulation of trickle-bed reactors using computational fluid dynamics: a state-of-the-art review. Can. J. Chem. Eng. 91, 136–180 (2013)
Wang, Y.F., Mao, Z.S., Chen, J.Y.: The relationship between hysteresis and liquid flow distribution in trickle beds. Chin. J. Chem. Eng. 7, 221–229 (1999)
Weekman, V.W., Myers, J.E.: Heat transfer characteristics of concurrent gas-liquid flow in packed beds. AIChE J. 11, 13–17 (1965)
Westhuizen, I. van der, du Toit, E., Nicol, W.: Trickle flow multiplicity: the influence of the prewetting procedure on flow hysteresis. Chem. Eng. Res. Des. 85, 1604–1610 (2007)
Wild, G., Larachi, F., Charpentier, J.-C.: Heat and mass transfer in gas-liquid-solid fixed bed reactors. In: Quintard, M., Todorovic, M. (Hrsg.) Heat and Mass Transfer in Porous Media, S. 615–632. Elsevier, Amsterdam (1992)
Wörz, N., Arras, J., Claus, P.: Continuous selective hydrogenation of citral in a trickle-bed reactor using ionic liquid modified catalysts. Appl. Catal., A. 391, 319–324 (2011)
Young, L.C., Finlayson, B.A.: Axial dispersion in nonisothermal packed bed chemical reactors. Ind. Eng. Chem. Fundam. 12, 412–422 (1973)
Zalucky, J.: Hydrodynamics and mass transfer performance of solid-foam packed reactors at descending gas-liquid flows. Dissertation. Technische Universität Dresden (2018)
Zalucky, J., Wagner, M., Schubert, M., Lange, R., Hampel, U.: Hydrodynamics of descending gas-liquid flows in solid foams: liquid holdup, multiphase pressure drop and radial dispersion. Chem. Eng. Sci. 168, 480–494 (2017)
Zhukova, T.B., Pisarenko, V.N., Kafarov, V.V.: Modeling and design of industrial reactors with a stationary bed of catalyst and two-phase gas-liquid flow – a review. Int. Chem. Eng. 30, 57–102 (1990)
Zimmerman, S.P., Chu, C.F., Ng, K.M.: Axial and radial dispersion in trickle-bed reactors with trickling gas-liquid downflow. Chem. Eng. Commun. 50, 213–240 (1987)
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Schubert, M. (2019). Reaktoren für Dreiphasen-Reaktionen: Rieselbettreaktoren. In: Reschetilowski, W. (eds) Handbuch Chemische Reaktoren. Springer Reference Naturwissenschaften . Springer Spektrum, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-56444-8_32-1
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