Taxonomy: Physicochemical and Pharmacological Properties of Alkaloids – Miscellaneous Alkaloids
Biological sources: Stachybotrys alternans
C25H35NO5: 429.2483
Mp: 202°C (MeOH) [1]
IR: 3350–3140; 1675; 1650; 1630; 1475; 1360 [1]
MS m/z: M+ 429 (95), 411 (17.5), 398 (100), 396 (11.3), 386 (16.3), 380 (10), 368 (2.8), 354 (2), 342 (1.9), 339 (1.8), 312 (1.9), 300 (3), 287 (3.3), 274 (10), 260 (10), 256 (7.5), 242 (10), 234 (12.5), 223 (30), 221 (20), 207 (12.5), 189 (15), 149 (12.5), 135 (12.5), 129 (12.5), 109 (12.5) [1]
1 H NMR: 0.80 (3H, J = 5.8, CH3-18), 0.88 (3H, c, CH3-21), 0.97 (3H, c, CH3-19), 1.13 (1H, dt, J = 13, 3, H-1в), 1.19 (3H, s, CH3-20), 1.42 (1H, qd, J = 13, 3.5, H-6в), 1.55 (1H, H-7в), 1.70 (1H, H-7α), 1.70 (1H, H-2α), 1.75 (1H, H-8), 11.95 (1H, tt, J = 13, 3, H-2в), 2.35 (1H, td, J = 13, 3, H-1α), 2.56 (1H, dd, J = 13, 2.4, H-5), 3.09 (1H, d, J = 16.7, H-11в), 3.50 (1H, d, J = 16.7, H-11α), 3.65, 3.90 (each 1H, m, 2H-25), 3.90 (2H, m, H-24), 4.90, 4.35 (each 1H, d, J...
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References
L.S. Kamalov, S.F. Aripova, B. Tashkhodjaev, M.I. Isaev, Chem. Nat. Comp. 34, 605 (1998)
L.S. Kamalov, S.F. Aripova, M.I. Isaev, Chem. Nat. Comp. 33, 462 (1997)
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(2013). Stachybotryne. In: Azimova, S.S., Yunusov, M.S. (eds) Natural Compounds. Springer, New York, NY. https://doi.org/10.1007/978-1-4614-0560-3_946
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DOI: https://doi.org/10.1007/978-1-4614-0560-3_946
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