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Alline

Reference work entry

CAS Registry Number: 101053-34-3 Open image in new window

Taxonomy: Physicochemical and Pharmacological Properties of Alkaloids – Miscellaneous Alkaloids

Biological sources: Allium altaicum, A. anisopodium, A. odorum, A. senescens, A. splendens, A. stelleranum, A. victorialis

C11H14N2O: 190.1106

Mp: 91–92°C (Me2CO) [1], 197°C (hydrochloride) [2]

[α]D +136° (CHCl3) [2]

UV: 245, 303(3.68, 3.14) [2]

IR: 3350, 1615, 1495, 760, 710 [2]

MSm/z: 190(M+, 100), 189(11), 173(42), 172(27), 171(14), 162(32), 161(23), 148(19), 147(98), 146(100), 134(20), 133(55), 132(55), 131(88), 130(77), 128(19), 120(32), 119(32), 118(48), 117(28), 106(19), 105(16), 104(34), 103(14), 93(55), 92(28), 91(33), 78(12), 77(46) [2]

1H NMR: 2.00, 2.70(each 2H, m, NCH2CH2), 2.21(3H, s, NCH3), 4.03, 4.18(2H, s, 1H, s, OH, NH, CH), 6.45–7.12(4H, m, H–Ar) [2]

X-ray: [2]

References

  1. 1.
    T.P. Antsupova, K. Samikov, Chem. Nat. Comp. 20, 242 (1984)CrossRefGoogle Scholar
  2. 2.
    B. Tashkhodzhaev, K. Samikov, M.R. Yagudaev, T.P. Antsupova, R. Shakirov, S.Yu. Yunusov, Chem. Nat. Comp. 21, 645 (1985)CrossRefGoogle Scholar

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© Springer Science+Business Media New York 2013

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