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Retrieval of object information from electron diffraction as Ill-posed inverse problems

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Part of the book series: Lecture Notes in Physics ((LNP,volume 486))

Abstract

Inverse problems as direct solutions of electron scattering equations can be deduced using either an invertible linearized eigenvalue system or a discretized form of the diffraction equations. The analysis is based on the knowledge of the complex electron wave at the exit plane of an object reconstructed for single reflections by electron holography or other wave reconstruction techniques. In principle, this enables the direct retrieval of the local thickness and orientation of a sample as well as the refinement of potential coefficients or the determination of the atomic displacements, caused by a crystal lattice defect, relative to the atom positions of the perfect lattice. Considering the sample orientation as perturbation the solution is given by a generalized and regularized Moore-Penrose inverse. Extracting solely the atomic displacements the latter are given by the zeros of a function with an incompletely known Fourier spectrum. The numerical algorithms resulting from the fundamental relations imply ill-posed inverse problems.

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References

  • Anstis, G.R. (1989): Simulation techniques for reflection electron microscopy, in: Computer Simulation of Electron Microscope Diffraction and Images, Krakow, W., O'Keefe, M.A. (eds.), The Minerals, Metals and Materials Society, pp. 229–238

    Google Scholar 

  • Bertero, M. (1989): Linear Inverse and Ill-Posed Problems, Advances in Electronics and Electron Physics 75, 1–114

    Google Scholar 

  • Coene, W., Janssen, G., Op de Beeck, M., van Dyck, D. (1992): Phase retrieval through focus variation for ultra-resolution in field-emission transmission electron microscopy, Phys. Rev. Letters 69, 3743–6

    Article  ADS  Google Scholar 

  • van Dyck, D. (1985): Image calculation in high resolution electron microscopy: Problems, progress and prospects, in: Advances in Electronics and Electron Physics, Hawkes, P.W. (ed.), 65, 295–355

    Google Scholar 

  • van Dyck, D. (1989): Three-dimensional reconstruction from two-dimensional projections with unknown orientation, position and projection axis, Ultramicroscopy 30, 435–8

    Article  Google Scholar 

  • van Dyck, D., Beeck, M. Op de, Coene, W. (1993): A new approach to object wavefunction reconstruction in electron microscopy, Optik 93, 103–7

    Google Scholar 

  • Howie, A., Basinski, Z.S. (1968): Approximations of the dynamical theory of diffraction contrast, Philos. Mag. 17, 1039–1063

    Article  ADS  Google Scholar 

  • Huang, S. (Editor) (1975), Picture Processing and Digital Filtering, Springer Vlg., N.Y.

    Google Scholar 

  • Lavrentiev, M.M. (1967): Some Improperly Posed Problems of Mathematical Physics, Springer, Berlin, pp. 10–20

    MATH  Google Scholar 

  • Lichte, H. (1986): Electron holography approaching atomic resolution, Ultramicroscopy 20, 293–304

    Article  Google Scholar 

  • Lichte, H. (1991): Electron image plane off-axis electron holography of atomic structures, Advances in Optical and Electron Microscopy 12, 25–91

    Google Scholar 

  • Lichte, H. (1992): Holography-just another method of image processing?, Scanning Microscopy Suppl. 6, 433–440

    Google Scholar 

  • Lichte, H., Völkl, E., Scheerschmidt, K. (1991): Electron image plane off-axis electron holography of atomic structures, Advances in Optical and Electron Microscopy 12, 25–91

    Google Scholar 

  • Lois A.K. (1989): Inverse und schlecht gestellte Probleme, Teubner Vlg., Stuttgart

    Google Scholar 

  • Orchowski, A., Lichte, H., Scheerschmidt, K., Scholz, R. (1993): Hochauflösende Elektroenmikroskopie zur Analyse von ∑ 13 Tilt-Korngrenzen in Gold, Optick 94, Suppl. 5, 79

    Google Scholar 

  • Orchowski, A., Rau, W.D., Lichte, H. (1995): Electron holography surmounts resolution limit of electron microscopy, Phys. Rev. Letters 74, 399–402

    Article  ADS  Google Scholar 

  • Orchowski, A., Lichte, H. (1996): High resolution electron holography of real structures at the example of a = 13 grain boundary in gold, Ultramicroscopy 69, 199–209

    Article  Google Scholar 

  • Rousseeuw, P.J. (1987), Robust regression and outlier detection, John Wiley & Sons, N.Y.

    Book  MATH  Google Scholar 

  • Scheerschmidt, K., Hillebrand, R. (1991): Image interpretation in HREM: Direct and indirect methods. Proc. 32nd Course Int. Centre of Electron Microscopy “High-Resolution Electron Microscopy — Fundamentals and applications”. Heydenreich, J., Neumann, W. (eds.), Halle, p. 56–65

    Google Scholar 

  • Scheerschmidt, K., Knoll, F. (1994): Retrieval of Object Information from Electron Diffraction, I. Theoretical preliminaries, phys. stat. sol. (a) 146, 491–502

    Article  Google Scholar 

  • Scheerschmidt, K., Knoll, F. (1995): Retrieval of atomic displacements from reconstructed electron waves as an ill-posed inverse problem, Proc. Int. Workshop Electron Holography, Knoxville Tennessee USA 1994, Tonomura, A., Allard, L.F., Pozzi, G., Joy, D.C., Ono, Y.A. (eds.), Elsevier Science, p. 117–124

    Google Scholar 

  • Scheerschmidt, K., Knoll, F. (1995): Zur Rekonstruktion von Verschiebungsfeldern aus elektronen-holographisch ermittelten Objektwellen, Optik 100, Suppl. 6, 50.

    Google Scholar 

  • Scheerschmidt, K. (1997): Direct retrieval of object information from diffracted electron waves, Proc. 15 Pfefferkorn Conf. on Electron Imaging and Signal Processing, May 18–22, 1996, Silver Bay, N.Y., Scanning Microscopy Suppl. 11, submitted

    Google Scholar 

  • Spence, J.C.H., Zuo, J.M. (1992): Electron Microdiffraction, Plenum Press, New York, pp. 134–5

    Google Scholar 

  • Tichonov, A.N., Arsenin, Y.Y. (1977): Solutions of Ill-Posed Problems, Wiley, New York, pp. 1–30

    Google Scholar 

  • Zakhariev, B.N., Suzko, A.A. (1990): Direct and Inverse Problems, Springer Vlg., Bln.-Heidelbg.

    Google Scholar 

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Guy Chavent Pierre C. Sabatier

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© 1997 Springer-Verlag

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Scheerschmidt, K. (1997). Retrieval of object information from electron diffraction as Ill-posed inverse problems. In: Chavent, G., Sabatier, P.C. (eds) Inverse Problems of Wave Propagation and Diffraction. Lecture Notes in Physics, vol 486. Springer, Berlin, Heidelberg. https://doi.org/10.1007/BFb0105761

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  • DOI: https://doi.org/10.1007/BFb0105761

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  • Publisher Name: Springer, Berlin, Heidelberg

  • Print ISBN: 978-3-540-62865-1

  • Online ISBN: 978-3-540-68713-9

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