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New Horizons for Magic-Angle Spinning NMR

  • Ago SamosonEmail author
  • Tiit Tuherm
  • Jean Past
  • Andres Reinhold
  • Tiit Anupõld
  • Ivo Heinmaa
Chapter
Part of the Topics in Current Chemistry book series (TOPCURRCHEM, volume 246)

Abstract

Recent developments in sample rotation technology have had a profound impact on magic-angle-spinning NMR. First, rotation frequencies approaching, and even exceeding, strong homonuclear spin interactions have made high-resolution solid-state 1H spectroscopy much more accessible. Second, the new concept of fast rotation sweep spectroscopy has emerged. Third, high-resolution NMR at cryogenic temperatures has become feasible, offering an enormous sensitivity gain and the opportunity to study a wide range of physical phenomena.

Magic-Angle Spinning NMR Sample rotation Rotor size Selectivity Sensitivity Spectral resolution 

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Copyright information

© Springer-Verlag Berlin Heidelberg 2005

Authors and Affiliations

  • Ago Samoson
    • 1
    Email author
  • Tiit Tuherm
    • 1
  • Jean Past
    • 1
  • Andres Reinhold
    • 1
  • Tiit Anupõld
    • 1
  • Ivo Heinmaa
    • 1
  1. 1.National Institute of Chemical Physics and BiophysicsTallinnEstonia

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