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Analysis by SAXS and cryo-TEM on polymerization with a surfactant

  • Formation of Structures
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Formation and Dynamics of Self-Organized Structures in Surfactants and Polymer Solutions

Part of the book series: Progress in Colloid & Polymer Science ((PROGCOLLOID,volume 106))

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Abstract

The polymerization process in a solution was examined by SAXS and cryo-TEM in the case of chemical polymerization of pyrrole in aqueous solution using sodium cellulose sulfonate (SCS) and FeCl3 as oxidizing agents. Observations with SAXS and cryo-TEM indicated the formation of micelle of SCS in SCS + water system. By adding FeCl3 in the solution, large spherical aggregates were formed as revealed by cryo-TEM, which is considered to be a precursor for the polymer spherical particles produced with a constant diameter.

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References

  1. Ezquerra TA, Mohammadi M, Kremer F, Vilgis T, Wegner G (1988) J Phys C: Solid State Phys 21:927–941

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  2. Isoda S, Kita Y, Donkai N, Sano Y, Wegner G (1991) Bull Inst Chem Res Kyoto Univ 69:331–341

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Authors and Affiliations

  1. Institute for Chemical Research, Kyoto University, Uji, 611, Kyoto, Japan

    T. Ogawa, Dr. S. Isoda, T. Suga, M. Tsujimoto, Y. Hiragi & T. Kobayashi

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  1. T. Ogawa
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  2. Dr. S. Isoda
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  3. T. Suga
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  4. M. Tsujimoto
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  5. Y. Hiragi
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  6. T. Kobayashi
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Editor information

K. Kawasaki B. Lindman H. Okabayashi

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© 1997 Steinkopff Verlag

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Ogawa, T., Isoda, S., Suga, T., Tsujimoto, M., Hiragi, Y., Kobayashi, T. (1997). Analysis by SAXS and cryo-TEM on polymerization with a surfactant. In: Kawasaki, K., Lindman, B., Okabayashi, H. (eds) Formation and Dynamics of Self-Organized Structures in Surfactants and Polymer Solutions. Progress in Colloid & Polymer Science, vol 106. Steinkopff. https://doi.org/10.1007/BFb0111046

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  • DOI: https://doi.org/10.1007/BFb0111046

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  • Publisher Name: Steinkopff

  • Print ISBN: 978-3-7985-1096-8

  • Online ISBN: 978-3-7985-1659-5

  • eBook Packages: Springer Book Archive

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