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Metal Complexes with Tetrapyrrole Ligands I pp 71–114Cite as

Infrared and Raman spectra of metalloporphyrins

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Part of the book series: Structure and Bonding ((STRUCTURE,volume 64))

Abstract

Infrared and Raman spectra of metalloporphyrins, metallochlorins, and metallophthalocyanines are comprehensively reviewed. The review starts from general explanations of basic properties of resonance Raman (RR) spectra of these compounds. Vibrational assignments of IR and RR bands of symmetric metalloporphyrins and their application to asymmetric protoporphyrin IX are interpreted on the basis of the isotopic shift data observed for specifically isotope-labeled porphyrins and of the normal coordinate calculations. For iron porphyrins, empirical rules with regard to the relation between the RR spectra and the spin-, oxidation-, and coordination states are explained. FeI- and FeIV-porphyrins and porphyrin cation-radical states are also included. The internal modes of an axial ligand (L) coordinated to the metal ion (M) as well as the M-L stretching modes and their difference between organic solution and protein matrix are described. Based on these data, differences and similarities in the M-L bonds among the three types of metal complexes of the conjugated macrocycles are discussed.

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  1. Institute for Molecular Science, Okazaki National Research Institutes, Myodaiji, 444, Okazaki, Japan

    Teizo Kitagawa

  2. The Jikei University School of Medicine, Minato-ku, 105, Tokyo, Japan

    Yukihiro Ozaki

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  1. Teizo Kitagawa
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Kitagawa, T., Ozaki, Y. (1987). Infrared and Raman spectra of metalloporphyrins. In: Buchler, J.W. (eds) Metal Complexes with Tetrapyrrole Ligands I. Structure and Bonding, vol 64. Springer, Berlin, Heidelberg. https://doi.org/10.1007/BFb0036790

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  • DOI: https://doi.org/10.1007/BFb0036790

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  • Publisher Name: Springer, Berlin, Heidelberg

  • Print ISBN: 978-3-540-17531-5

  • Online ISBN: 978-3-540-47446-3

  • eBook Packages: Springer Book Archive

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