Skip to main content
SpringerLink
Log in

Application of FT-IR and NMR to epoxy resins

  • Conference paper
  • First Online:
Epoxy Resins and Composites II

Part of the book series: Advances in Polymer Science ((POLYMER,volume 75))

Abstract

The application of FT-IR and high resolution solid state NMR to the structural characterization of epoxies is described. Theoretical and experimental background is given and progress to date in these two fields summarized.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Log in via an institution

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

11 References

  1. Griffiths, P. R.: Chemical Infrared Transform Spectroscopy, New York, Wiley, 1975

    Google Scholar 

  2. Ferraro, J. R., et al.: Fourier Transform Infared Spectroscopy Applications to Chemical Systems, Academic Press, New York, 1978, J. R. Ferraro, L. J. Basile, Eds.

    Google Scholar 

  3. Koenig, J. L.: Acct. of Chem. Res., 14, 171 (1981)

    Article  Google Scholar 

  4. Bell, R. J.: Introductory Fourier Transform Spectroscopy, Academic Press, New York, 1982

    Google Scholar 

  5. Griffiths, P. R.: “FT-IR Theory and Instrumentation”, in: Transform Techniques in Chemistry, P. R. Griffiths, Ed., Plenum Press, 1978

    Google Scholar 

  6. Cooley, J. W., Tukey, J. W.: Math. Comput. 19, 297 (1965)

    Google Scholar 

  7. Antoon, M. K., Zehner, B. E., Koenig, J. L.: Polym. Comp. 1, 24 (1980)

    Article  Google Scholar 

  8. Antoon, M. K., Zehner, B. E., Koenig, J. L.: Polym. Comp. 2, 81, (1980)

    Article  Google Scholar 

  9. Antoon, M. K., Koenig, J. L.: J. Polym. Sci., Polym. Chem. Ed., 19, 549 (1981)

    Google Scholar 

  10. Koenig, J. L.: Adv. Polym. Sci., 54, 87 (1983)

    Google Scholar 

  11. Dannenberg, H.: SPE Trans., 78–88, Jan., 1963

    Google Scholar 

  12. Perkinson, J. L.: A Method of Obtaining a True Infrared Spectrum of the Epoxy from a Cured Fiber Glass-Epoxy Composite, Gov., Rep. Announce (U.S.), 71, No. 19, 88, 1971

    Google Scholar 

  13. Graf, R., Koenig, J. L., Ishida, H.: Appl. Spectrosc., (in press)

    Google Scholar 

  14. Fuller, M. P., Griffiths, P. R.: Anal. Chem., 50, 1906 (1978)

    Article  Google Scholar 

  15. Kirshnan, K.: Appl. Spectrosc., 35, 549 (1981)

    Article  Google Scholar 

  16. Lee, H., Neville, K.: Handbook of Epoxy Resins, New York, McGraw-Hill, 1967

    Google Scholar 

  17. Antoon, M. K.: Ph. D. Dissertation, Case Western Reserve University, Cleveland, Ohio, Appendix I, 1981

    Google Scholar 

  18. Pearce, E. M., Bulkin, B. J., Lin, S. C.: J. Polym. Sci., Polym. Chem. Ed., 17, 3121 (1979)

    Google Scholar 

  19. Murphy, W. J.: Ed., Ind. Eng. Chem., 15, 609 (1943)

    Google Scholar 

  20. Barnes, R. B.: Applications of Instruments in Chemistry, eds. R. E. Burk and O. Grummitt, Interscience, New York, p. 144, 1945

    Google Scholar 

  21. Murphy, W. J. Ed.: Ind. Eng. Chem., 15, 659 (1943)

    Google Scholar 

  22. Antoon, M. K., Koenig, J. H., Koenig, J. L.: Appl. Spectrosc., 31, 518 (1977)

    Article  Google Scholar 

  23. Haaland, D. M., Easterling, R. G.: Appl. Spectrosc., 34, 539 (1980)

    Article  Google Scholar 

  24. Haaland, D. M., Easterling, R. G.: Appl. Spectrosc., 36, 665 (1982)

    Article  Google Scholar 

  25. Antoon, M. K., Starkey, K. M., Koenig, J. L.: Applications of Fourier Transform Infrared Spectroscopy to Quality Control of the Epoxy Matrix, Composite Materials, Fifth Conference, ASTM, p. 541, 1979

    Google Scholar 

  26. Dannenberg, H., Harp, W. R. Jr.: Anal. Chem., 28, 86 (1956)

    Article  Google Scholar 

  27. Patterson, W. A.: Anal. Chem., 26, 823 (1954)

    Article  Google Scholar 

  28. Malinowski, E. R., Lowery, D. G.: Factor Analysis in Chemistry, John Wiley, New York, 1980

    Google Scholar 

  29. Antoon, M. K., D'Esposito, L., Koenig, J. L.: Appl. Spectrosc., 33, 351 (1979)

    Article  Google Scholar 

  30. Luston, J., Manasek, A., Kulickova, M.: J. Macromol. Sci., Chem. 12, 995 (1978)

    Google Scholar 

  31. Feltzin, J., Longenecker, D. M., Petker, I.: S.P.E. Trans., 111–116, April, 1965

    Google Scholar 

  32. Antoon, M. K., Koenig, J. L.: J. Macromol. Sci., Rev. Macromol Chem., C19, 135 (1980)

    Google Scholar 

  33. Hojo, H., Tsuda, K.: Effects of Chemical Environments and Stress on Corrosion Behaviors of Glass Fiber Reinforced Plastics and Vinyl Ester Resin, Proc., 34th Ann. Tech. Conf., Reinf. Plast./Compos. Inst., SPI, Sec. 13-B, 1979

    Google Scholar 

  34. Antoon, M. K., Koenig, J. L., Serafini, T.: J. Polym. Sci., Polym. Phys. Ed., 19, 1567 (1981)

    Google Scholar 

  35. Antoon, M. K., Koenig, J. L.: J. Polym. Sci., Polym. Phys. Ed., 19, 197 (1981)

    Google Scholar 

  36. Chiang, C. H., Koenig, J. L.: Polym. Comp., 1, 88 (1980)

    Article  Google Scholar 

  37. Chiang, C. H., Koenig, J. L.: Polym. Comp., 2, 192 (1981)

    Article  Google Scholar 

  38. Bloch, F.: Phys. Rev., 111, 841 (1958)

    Article  Google Scholar 

  39. Sarles, L. R., Cotts, R. M.: Phys. Rev., 111, 853 (1958)

    Article  Google Scholar 

  40. Pines, A., Gibby, M. G., Waugh, J. S.: J. Chem. Phys., 59, 569 (1973)

    Article  Google Scholar 

  41. Andrew, E. R.: Phil. Tran. Roy. Soc. Lond., A299, 29 (1981)

    Google Scholar 

  42. Andrew, E. R.: Arch. Sci., (Geneva), 12, 103 (1959)

    Google Scholar 

  43. Andrew, E. R.: Prog. NMR Spectros., 8, 1 (1971)

    Article  Google Scholar 

  44. Lowe, I. J.: Phys. Rev. Lett., 2, 285 (1959)

    Article  Google Scholar 

  45. Kessemeier, H., Norberg, R. E.: Phys. Rev., 155, 321 (1967)

    Article  Google Scholar 

  46. Mag. Res. Rev., 7, No. 2, 87 (1982)

    Google Scholar 

  47. Hartmann, S. R., Hahn, E. L.: Phys. Rev., 128, 3042 (1952)

    Google Scholar 

  48. Sojka, S. A., Moniz, W. B.: J. Appl. Polym. Sci., 20, 1977 (1976)

    Article  Google Scholar 

  49. Kennedy, J. P., Guhaniyogi, S. C., Percec, V.: Polym. Bull., 8, 571 (1982)

    Google Scholar 

  50. Gaul, J. H. Jr., Carr, T. M.: Spectros. Lett., 16, 9, 651 (1983)

    Google Scholar 

  51. Strothers, J. B.: Carbon-13 NMR Spectroscopy, New York: Academic Press, p. 311, 1972

    Google Scholar 

  52. Hayes, S., et al.: J. Polym. Sci., Polym. Chem. Ed., 19, 9, 2185 (1981)

    Google Scholar 

  53. Hayes, S., et al.: J. Polym. Sci., Polym. Chem. Ed., 19, 11, 2977 (1981)

    Google Scholar 

  54. Williams, E. A., Cargioli, J. D.: “Silicon-29 NMR Spectroscopy” Annual Reports in NMR Spectroscopy, 9, Academic Press, London, G. A. Webb, Ed., p. 222, 1979

    Google Scholar 

  55. Hinton, J. A., Briggs, R. W.: NMR and the Periodic Table, Academic Press, R. K. Harris, and B. E. Mann, Eds., Chap. 9, p. 279, 1978

    Google Scholar 

  56. Larsen, D. W., Strange, J. H.: J. Polym. Sci., Polym. Phy. Ed., 11, 65 (1973)

    Google Scholar 

  57. Slichter, W. P.: NMR, Basic Principles and Progress, 4, Springer Berlin, p. 209, 1971

    Google Scholar 

  58. Connor, T. M.: NMR, Basic Principles and Progress, 4, Springer Berlin, p. 244, 1971

    Google Scholar 

  59. Clark-Monks, C., Ellis, B.: J. Polym. Sci., 8, A-2, 2003 (1970)

    Google Scholar 

  60. Resing, H. A., Moniz, W. B.: Macrom., 8, 4, 560 (1975)

    Article  Google Scholar 

  61. Garroway, A. N., Moniz, W. B., Resing, H. A.: Am. Chem. Soc., Coating and Plastics Preprint of the 172nd Meeting, 36, No. 2, 1976

    Google Scholar 

  62. Garroway, A. N., Moniz, W. B., Resing, H. A.: Pulsed Nuclear Magnetic Resonance in Solids, The Faraday Disc. Chem. Soc., Lond., No. 13, p. 63, 1978

    Google Scholar 

  63. Moniz, W. B., Poranski, C. F., Jr.: Epoxy Resin Chemistry, Chap. 7, ACS Symp. Ser., No. 114, Washington D.C., Amer. Chem. Soc. 1979

    Google Scholar 

  64. Dorsey, J. G., Dorsey, G. F., Rutenberg, A. C., Green, L. A.: Anal. Chem., 49, 1144 (1977)

    Article  Google Scholar 

  65. Hammerich, A. D., Willeboordse, F. G.: Anal. Chem., 45, 1696 (1973)

    Article  Google Scholar 

  66. Shoolery, J. N.: Prog. NMR Spectros., 11, 79 (1977)

    Article  Google Scholar 

  67. Garroway, A. N., Moniz, W. B., Resing, H. A.: Carbon-13 NMR in Polymer Science, ACS Symp. Ser., No. 103, W. M. Pasika, Ed., 1979

    Google Scholar 

  68. Balimann, G. E., Groombridge, C. J., Harris, R. K., Packer, K. J., Say, B. J., Tanner, S. F.: Phil. Trans. R. Soc. Lond., A299, 643 (1981)

    Google Scholar 

  69. VanderHart, D. L., Earl, W. L., Garroway, A. N.: J. Magn. Reson. 44, 361 (1981)

    Google Scholar 

  70. Garroway, A. N., VanderHart, D. L., Earl, W. L.: Phil. Trans. R. Lond., A299, 609 (1981)

    Google Scholar 

  71. Garroway, A. N., Ritchey, W. M., Moniz, W. B.: Macromolecules, 15, 1051 (1982)

    Article  Google Scholar 

  72. Poranski, C. F., Jr., Moniz, W. B., Birkle, D. L., Kopfle, J. T., Sojka, S. A.: NRL Report No. 8092, Naval Research Laboratory, Wash. D.C., 1977

    Google Scholar 

  73. Flippen-Anderson, J. L., Gilardi, R.: Acta Crystallogr., B37, 1433 (1981)

    Google Scholar 

  74. Grant, D. M., Chaney, B. V.: J. Am. Chem. Soc., 89, 5315 (1967)

    Article  Google Scholar 

  75. Cholli, A., Ritchey, W. M., Koenig, J. L.: Preprint Am. Chem. Soc., 1984

    Google Scholar 

  76. Dušek, K., Ilavský, M., Luňák, S.: J. Polym. Sci., Polym. Symp. 53, 29 (1975)

    Google Scholar 

  77. Luňák, S., Dušek, K.: J. Polym. Sci., Polym. Symp. 53, 45 (1975)

    Google Scholar 

  78. Dušek, K.: in Rubber-Modified Thermoset Resins, ACS Adv. Chem. Ser. 208, eds. Riew, C. K., Gillham, J. K., Washington: Amer. Chem. Soc. (1984) p. 3

    Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Department of Macromolecular Science, Case Western Reserve University, 44106, Cleveland, Ohio, U.S.A.

    Elaine Mertzel & Jack L. Koenig

Authors
  1. Elaine Mertzel
    View author publications

    You can also search for this author in PubMed Google Scholar

  2. Jack L. Koenig
    View author publications

    You can also search for this author in PubMed Google Scholar

Editor information

K. Dušek

Rights and permissions

Reprints and permissions

Copyright information

© 1986 Springer-Verlag

About this paper

Cite this paper

Mertzel, E., Koenig, J.L. (1986). Application of FT-IR and NMR to epoxy resins. In: Dušek, K. (eds) Epoxy Resins and Composites II. Advances in Polymer Science, vol 75. Springer, Berlin, Heidelberg. https://doi.org/10.1007/BFb0017915

Download citation

  • DOI: https://doi.org/10.1007/BFb0017915

  • Received:

  • Published:

  • Publisher Name: Springer, Berlin, Heidelberg

  • Print ISBN: 978-3-540-15825-7

  • Online ISBN: 978-3-540-39657-4

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics

Search

Navigation