Abstract
The properties of ZnO synthesized by sol–gel centrifugation (SGC) and sol–gel storage (SGS) are presented in this chapter. Furthermore, the physical appearance of ZnO has been discussed. The ZnO structural, morphological and optical properties are characterize using X-ray diffraction (XRD), field-emission scanning electron microscopy (FESEM), transmission electron microscopy (TEM) and UV-visible (UV-vis) spectroscopy.
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Duval, D.J., McCoy, B.J., Risbud, S.H., Munir, Z.A.: Size selected silicon particles in sol–gel glass by centrifugal processing. J. Appl. Phys. 83, 2301–2307 (1998)
Alias, S.S., Ismail, A.B., Mohamad, A.A.: Effect of pH on ZnO nanoparticle properties synthesized by sol–gel centrifugation. J. Alloy. Compd. 499, 231–237 (2010)
Rani, S., Suri, P., Shishodia, P.K., Mehra, R.M.: Synthesis of nanocrystalline ZnO powder via sol–gel route for dye-sensitized solar cells. Sol. Energy Mater. Sol. Cells 92, 1639–1645 (2008)
Li Jian, K.: Synthesis and Characterization of Zinc Oxide Powder via Sol–Gel Route for Quasi-Solid-State Solar Cells, Final Year Project Report, Universiti Sains Malaysia, Nibong Tebal, Penang, Malaysia (2009)
Tan, A.L., Khoo, L.J., Alias, S.S., Mohamad, A.A.: ZnO nanoparticles and poly(acrylic) acid-based polymer gel electrolyte for photo electrochemical cell. J. Sol–Gel Sci. Technol. 64, 184–192 (2012)
Maensiri, S., Laokul, P., Promarak, V.: Synthesis and optical properties of nanocrystalline ZnO powders by a simple method using zinc acetate dihydrate and poly(vinyl pyrrolidone). J. Cryst. Growth 289, 102–106 (2006)
Du, H., Yuan, F., Huang, S., Li, J., Zhu, Y.: A new reaction to ZnO nanoparticles. Chem. Lett. 33, 770–771 (2004)
Mazloumi, M., Taghavi, S., Arami, H., Zanganeh, S., Kajbafvala, A., Shayegh, M.R., Sadrnezhaad, S.K.: Self-assembly of ZnO nanoparticles and subsequent formation of hollow microspheres. J. Alloy. Compd. 468, 303–307 (2009)
Hosono, E., Fujihara, S., Kimura, T., Imai, H.: Non-basic solution routes to prepare ZnO nanoparticles. J. Sol–Gel. Sci. Technol. 29, 71–79 (2004)
Jang, J.-M., Kim, S.-D., Choi, H.-M., Kim, J.-Y., Jung, W.-G.: Morphology change of self-assembled ZnO 3D nanostructures with different pH in the simple hydrothermal process. Mater. Chem. Phys. 113, 389–394 (2009)
Lin, C.-C., Li, Y.-Y.: Synthesis of ZnO nanowires by thermal decomposition of zinc acetate dihydrate. Mater. Chem. Phys. 113, 334–337 (2009)
Musić, S., Dragčević, Đ., Popović, S., Ivanda, M.: Precipitation of ZnO particles and their properties. Mater. Lett. 59, 2388–2393 (2005)
Elkhidir, S.A., Tang, Y., Xu, L.: Preparation of ZnO nanoparticles and nanosheets and their application to dye-sensitized solar cells. Sol. Energy Mater. Sol. Cells 91, 1658–1662 (2007)
Kamalasanan, M.N., Chandra, S.: Sol-gel synthesis of ZnO thin films. Thin Solid Films 288, 112–115 (1996)
Bacaksiz, E., Parlak, M., Tomakin, M., Özçelik, A., Karakız, M., Altunbaş, M.: The effects of zinc nitrate, zinc acetate and zinc chloride precursors on investigation of structural and optical properties of ZnO thin films. J. Alloy. Compd. 466, 447–450 (2008)
Marotti, R.E., Guerra, D.N., Bello, C., Machado, G., Dalchiele, E.A.: Bandgap energy tuning of electrochemically grown ZnO thin films by thickness and electrodeposition potential. Sol. Energy Mater. Sol. Cells 82, 85–103 (2004)
Bhargava, R.N. (ed.): Properties of Wide Bandgap II–VI Semiconductors., EMIS Datareviews Series No.17, INSPEC, London, United Kingdom.27 (1997)
Monticone, S., Tufeu, R.: Kanaev: complex nature of the UV and visible fluorescence of colloidal ZnO nanoparticles. J. Phys. Chem. B 102, 2854–2862 (1998)
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Alias, S.S., Mohamad, A.A. (2014). ZnO: Effect of Centrifugation and Storage on Sol–Gel Process. In: Synthesis of Zinc Oxide by Sol–Gel Method for Photoelectrochemical Cells. SpringerBriefs in Materials. Springer, Singapore. https://doi.org/10.1007/978-981-4560-77-1_3
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DOI: https://doi.org/10.1007/978-981-4560-77-1_3
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