Abstract
Fracture properties at the interface of hard and brittle Alumina (Al2O3) coating over a soft Al (Al 6061) substrate are studied using the double cantilever bend (DCB) test. These coatings were thermally sprayed and included substantial porosity. Elastic properties of the Alumina layer were determined by three-point bending (3PB) of the coated specimens. Fracture energy of Alumina was determined using a notched sample of the free-standing Alumina coating. FEM analysis of DCB was performed to estimate the stress intensity factor at the crack tip along the Al/Al2O3 interface. The experimental results show mixed mode fracture behaviour in most of the coatings. Average fracture energy of the interface, 6.46 J/m2, was estimated using these measurements.
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References
C. Xie, W. Tong, Cracking and decohesion of a thin Al2O3film on a ductile Al-5%Mg substrate. Acta Mater. 53(2), 477–485 (2005)
C. Edeleanu T.J. Law, Fracture of oxide films on strained aluminium. Philos. Mag. A J. Theor. Exp. Appl. Phys. 7(76), 573–581 (1962)
R.H. Dauskardt, M. Lane, Q. Ma, N. Krishna, Adhesion and debonding of multi-layer thin film structures. Eng. Fract. Mech. 61(1), 141–162 (1998)
M.S. Hu, A.G. Evans, The cracking and decohesion of thin films on ductile substrates. Acta Metall. 37(3), 917–925 (1989)
D. Müller, E. Fromm, Mechanical properties and adhesion strength of TiN and Al coatings on HSS, steel, aluminium and copper characterized by four testing Methods. Thin Solid Films 270(1–2), 411–416 (1995)
X. You, H. Zhao, Y. Wei, Determination of interfacial mechanical parameters for an Al/Epoxy/Al2o3system by using peel test simulations. Acta Mech. Solida Sin. 21(3), 198–206 (2008)
N.G. Chechenin, J. Bøttiger, J.P. Krog, Nanoindentation of amorphous aluminum oxide films III. The influence of the substrate on the elastic properties. Thin Solid Films 304(1–2), 70–77 (1997)
M.D. Kriese, D.A. Boismier, N.R. Moody, W.W. Gerberich, Nanomechanical fracture-testing of thin films. Eng. Fract. Mech. 61(1), 1–20 (1998)
A. Abdul-Baqi, E. Van der Giessen, Delamination of a strong film from a ductile substrate during indentation unloading. J. Mater. Res. 16(5), 1396–1407 (2001)
Y. Okajima, T. Nakamura, S. Sampath, Effect of powder injection on the interfacial fracture toughness of plasma-sprayed zirconia. J. Therm. Spray Technol. 22(2–3), 166–174 (2013)
G.M. Smith, M. Resnick, K. Flynn, G. Dwivedi, S. Sampath, Nature inspired, multi-functional, damage tolerant thermal spray coatings. Surf. Coat. Technol. 297, 43–50 (2016)
I. ASM Aerospace Specification Metals, “Aluminum 6061-T6; 6061-T651.” http://asm.matweb.com/search/SpecificMaterial.asp?bassnum=ma6061t6
Bangs Laboratories, Material Properties of Polystyrene and Poly(methyl methacrylate) (PMMA) Microspheres, 1–2 (2015
J.N. Reddy, Mechanics of Laminated Composite Plates and Shells: Theory and Analysis (2003)
ASTM, ASTM—E1290 Standard Test Method for Crack-Tip Opening Displacement (CTOD) Fracture. ASTM. 03(no. March), 1–13 (2003)
M.D. Thouless, Shear forces, root rotations, phase angles and delamination of layered materials. Eng. Fract. Mech. 191, 153–167 (2018)
B.F. Sørensen, K. Jørgensen, T.K. Jacobsen, R.C. Østergaard, DCB-specimen loaded with uneven bending moments. Int. J. Fract. 141(1–2), 163–176 (2006)
94% Alumina Material Properties. Accuratus Ceramic Corporation (2002). https://accuratus.com/alumox.html
M.Y. He, J. W Hutchinson, Kinking of a crack out of an interface. J. Appl. Mech. 270–278 (1989)
Acknowledgements
The authors would like to thank the Max Planck Partner Group Project for funding this study. The authors would like to duly acknowledge the FIST lab for Mechanical Testing, Metallurgical Engineering and Materials Science, IIT Bombay for providing the test facilities.
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Mishra, A.K., Sampath, S., Smith, G.M., Balila, N.J. (2020). Experimental Measurements of Interface Fracture Toughness Using Double Cantilever Bending. In: Prakash, R., Suresh Kumar, R., Nagesha, A., Sasikala, G., Bhaduri, A. (eds) Structural Integrity Assessment. Lecture Notes in Mechanical Engineering. Springer, Singapore. https://doi.org/10.1007/978-981-13-8767-8_43
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