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Fact-Finding on Physical and Mechanical Properties of 3Y-TZP Toughened Alumina (ZTA) Composites Incorporation of Functionalized Multi-walled Carbon Nanotubes

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Advances in Materials and Metallurgy

Part of the book series: Lecture Notes in Mechanical Engineering ((LNME))

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Abstract

Zirconia-toughened alumina (ZTA) has been the famous composite utilized for the fabrication of articulating components in a hip joint prosthetics. The demand for longer life and better performance the material characteristics of the articulating components have to be enhanced. In recent literatures it has been described that the addition of multi-walled carbon nanotubes (MWCNT) into an alumina matrix of zirconia-toughened alumina, ZTA to improve the flexural strength, fracture toughness, and fatigue resistance. The intent of the current work is to establish and authenticate that the material’s toughness and hardness could be significantly tailored by preparing 3Y-TZP toughened alumina (ZTA) composites by the combination of functionalized MWCNT using conventional sintering method. For this method, homogenous spreading of CNTs in ceramic matrix has been reached from 0.5 wt% up to 1.8 wt% CNTs using ball milling then compacted and finally sintered. The density and micro hardness were studied related to the experimental runs established using box-behnken design. A clear enhancement in the physical properties was achieved after the adding MWCNTs at the range of 0.5 to 1.8 wt% and sintering temperature varied from 1500 to 1600 °C. The addition of MWCNT in the matrix exhibited the better porosity, density over 3Y-TZP toughened alumina (ZTA) sintered at the same temperature. This results designates that the properties of Zirconia-toughened alumina (ZTA) with MWCNT reinforcements based composites are strongly rely on the process of adding CNT and sintering. The optimized process parameter were also identified form the studies.

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References

  1. De Mattia JS, Castiello E, Affatato S (2017) Clinical issues of ceramic devices used in total hip arthroplasty. In: Advances in ceramic biomaterials, pp 313–328

    Google Scholar 

  2. Nevarez-Rascon A, Aguilar-Elguezabal A, Orrantia E, Bocanegra-Bernal MH (2011) Compressive strength, hardness and fracture toughness of Al2O3 whiskers reinforced ZTA and ATZ nanocomposites: Weibull analysis. Int J Refract Met Hard Mater 29(3):333–340

    Article  Google Scholar 

  3. Liu Jian, Yan H, Reece MJ, Jiang K (2012) Toughening of zirconia/alumina composites by the addition of graphene platelets. J Eur Ceram Soc 32(16):4185–4193

    Article  Google Scholar 

  4. Pfeifer S, Demirci P, Duran R, Stolpmann H, Renfftlen A, Nemrava S, Niewa R, Clauß B, Buchmeiser MR (2016) Synthesis of zirconia toughened alumina (ZTA) fibers for high performance materials. J Eur Ceram Soc 36(3):725–731

    Article  Google Scholar 

  5. Rincón A, Moreno R, Chinelatto ASA, Gutierrez CF, Salvador MD, Borrell A (2016) Effect of graphene and CNFs addition on the mechanical and electrical properties of dense alumina-toughened zirconia composites. Ceram Int 42(1):1105–1113

    Google Scholar 

  6. Lupo F, Kamalakaran R, Scheu C, Grobert N, Ruhle M (2004) Microstructural investigations on zirconium oxide–carbon nanotube composites synthesized by hydrothermal crystallization. Carbon 42(10):1995–1999

    Article  Google Scholar 

  7. Sun J, Gao L, Jin X (2005) Reinforcement of alumina matrix with multi-walled carbon nanotubes. Ceram Int 31(6):893–896

    Article  Google Scholar 

  8. Sun J, Iwasa M, Nakayama T, Niihara K, Gao L, Jin X (2004) Pressureless sintering of alumina carbon nanotubes composites in air atmosphere furnace and their mechanical properties. J Ceram Soc Jpn Supplement 112–1, PacRim5 Special Issue

    Google Scholar 

  9. Yu M-F, Lourie Oleg, Dyer MJ, Moloni K, Kelly TF, Ruoff RS (2000) Strength and breaking mechanism of multiwalled carbon nanotubes under tensile load. Science 287(5453):637–640

    Article  Google Scholar 

  10. Renold Elsen S, Ramesh T, Aravinth B (2014) Optimization of process parameters of zirconia reinforced alumina by powder forming process using response surface method. Adv Mater Res 984:129–139

    Article  Google Scholar 

  11. Fan J, Zhao D, Wu M, Xu Z, Song J (2006) Preparation and microstructure of multi-wall carbon nanotubes-toughened Al2O3 composite. J Am Ceram Soc 89(2):750–753

    Article  Google Scholar 

  12. Santos C, Maeda LD, Cairo CAA, Acchar W (2008) Mechanical properties of hot-pressed ZrO2–NbC ceramic composites. Int J Refract Met Hard Mater 26(1):14–18

    Article  Google Scholar 

  13. Rose L, Spear RE (2008) Carbon nanotubes for orthopaedic implants. IntJ Mater Form 1(2):127–133

    Article  Google Scholar 

  14. Renold Elsen S, Ramesh T (2016) Analysis and optimization of dry sliding wear characteristics of zirconia reinforced alumina composites formed by conventional sintering using response surface method. Int J Refract Met Hard Mater 58:92–103

    Article  Google Scholar 

  15. Renold Elsen S, Jegadeesan K, Ronald Aseer J (2017) X-Ray diffraction analysis of mechanically milled alumina and zirconia powders. Nano Hybrids Compos 17:96–100

    Article  Google Scholar 

  16. Renold Elsen S, Ramesh T (2015) Optimization to develop multiple response hardness and compressive strength of zirconia reinforced alumina by using RSM and GRA. Int J Refract Met Hard Mater 52:159–164

    Article  Google Scholar 

  17. Ipek AKIN (2015) Investigation of the microstructure, mechanical properties and cell viability of zirconia-toughened alumina composites reinforced with carbon nanotubes. J Ceram Soc Jpn Supplement 123–5:405–413

    Google Scholar 

  18. Renold Elsen S, Ramesh T (2016) Shrinkage characteristics studies on conventional sintered zirconia toughened alumina using computed tomography imaging technique. Int J Refract Met Hard Mater 54:383–394

    Article  Google Scholar 

  19. Aseer JR, Sethupathi PB, Chandradass J, Renold Elsen S (2017) Taguchi based analysis on hole diameter error of drilled glass/BahuniaRacemosa fiber polymer composites. In: SAE Technical Paper. Issue 2017-28-1983

    Google Scholar 

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Manikandan, D., Renold Elsen, S. (2019). Fact-Finding on Physical and Mechanical Properties of 3Y-TZP Toughened Alumina (ZTA) Composites Incorporation of Functionalized Multi-walled Carbon Nanotubes. In: Lakshminarayanan, A., Idapalapati, S., Vasudevan, M. (eds) Advances in Materials and Metallurgy. Lecture Notes in Mechanical Engineering. Springer, Singapore. https://doi.org/10.1007/978-981-13-1780-4_25

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  • DOI: https://doi.org/10.1007/978-981-13-1780-4_25

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  • Publisher Name: Springer, Singapore

  • Print ISBN: 978-981-13-1779-8

  • Online ISBN: 978-981-13-1780-4

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