Skip to main content

Preparation and Characterization Other Photocatalysts

  • Chapter
  • First Online:
  • 336 Accesses

Part of the book series: Energy and Environment Research in China ((EERC))

Abstract

A series of zinc-based photocatalyst and bismuth-based photocatalyst were prepared. Several preparation methods and their characteristics of zinc-based photocatalyst are given. BiOIO3 nanosheets are studied systematically, which possess superior photocatalytic properties. The fabricated CSs-BiOI/BiOIO3 composites with heterostructures show the enhanced photocatalytic performance than BiOIO3. The physical and chemical properties of the as-prepared materials are characterized by X-ray diffraction , X-ray photoelectron spectroscopy, scanning electron microscope , transmission electron microscopy , high resolution TEM, Brunauer-Emmett-Teller , Fourier transform infrared, UV-vis diffuse reflectance spectra, and Photoluminescence .

This is a preview of subscription content, log in via an institution.

Buying options

Chapter
USD   29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD   84.99
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD   109.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD   109.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Learn about institutional subscriptions

References

  1. J.H. Zeng, B.B. Jin, Y.F. Wang, Facet enhanced photocatalytic effect with uniform single-crystalline zinc oxide nanodisks. Chem. Phys. Lett. 472, 90–95 (2009)

    Article  CAS  Google Scholar 

  2. J. Becker, K.R. Raghupathi, J. St Pierre, D. Zhao, R.T. Koodali, Tuning of the crystallite and particle sizes of ZnO nanocrystalline materials in solvothermal synthesis and their photocatalytic activity for dye degradation. J. Phys. Chem. C 115, 13844–13850 (2011)

    Article  CAS  Google Scholar 

  3. F. Xu, Y. Shen, L. Sun, H. Zeng, Y. Lu, Enhanced photocatalytic activity ofhierarchical ZnO nanoplate-nanowire architecture as environmentally safe and acilely recyclable photocatalyst. Nanoscale 3, 5020–5025 (2011)

    Article  CAS  Google Scholar 

  4. A. Umar, M.S. Akhtar, A. Al-Hajry, M.S. Al-Assiri, G.N. Dar, M.S. Islam, Enhancedphotocatalytic degradation of harmful dye and phenyl hydrazine chemicalsensing using ZnO nanourchins. Chem. Eng. J. 262, 588–596 (2015)

    Article  CAS  Google Scholar 

  5. M.K. Kavitha, S.C. Pillai, P. Gopinath, H. John, Hydrothermal synthesis of ZnO decorated reduced graphene oxide: understanding the mechanism of photocatalysis. J. Environ. Chem. Eng. 3, 1194–1199 (2015)

    Article  CAS  Google Scholar 

  6. C.J. Xu, Y.Z. Wang, H.Y. Chen, Rapid and simple synthesis of 3D ZnO microflowers at room temperature. Mater. Lett. 158, 347–350 (2015)

    Article  CAS  Google Scholar 

  7. E. Pál, V. Hornok, A. Oszkó, I. Dékány, Hydrothermal synthesis of prism-like and flower-like ZnO and indium-doped ZnO structures. Colloids Surf. A 340, 1–9 (2009)

    Article  CAS  Google Scholar 

  8. X. Zhao, F. Lou, M. Li, X. Lou, Z. Li, J. Zhou, Sol-gel-based hydrothermal method for the synthesis of 3D flower-like ZnO microstructures composed of nanosheets for photocatalytic applications. Ceram. Int. 40, 5507–5514 (2014)

    Article  CAS  Google Scholar 

  9. J.L. Yang, S.J. An, W.I. Park, G.C. Yi, W. Choi, Photocatalysis using ZnO thin films and nanoneedles grown by metal-organic chemical vapor deposition. Adv. Mater. 16, 1661–1664 (2004)

    Article  CAS  Google Scholar 

  10. M. Parhizkar, M. Kumar, P.K. Nayak, S. Singh, S.S. Talwar, S.S. Major, R.S. Srinivasa, Nanocrystalline ZnO films prepared by pyrolysis of Zn-arachidate LB multilayers. Colloids Surf. A 257–58, 445–449 (2005)

    Article  CAS  Google Scholar 

  11. Ruixing Zhou, Wu Jiang, Jing Zhang, Huan Tian, Pankun Liang, Tao Zeng, Lu Ping, Jianxing Ren, Tianfang Huang, Xiao Zhou, Pengfei Sheng, Photocatalytic oxidation of gas-phase Hg0 on the exposed reactive facets of BiOI/BiOIO3 heterostructures. Appl. Catal. B 204, 465–474 (2017)

    Article  CAS  Google Scholar 

  12. H.W. Huang, K. Xiao, K. Liu, S.X. Yu, Y.H. Zhang, In situ composition-transforming fabrication of BiOI/BiOIO3 heterostructure: semiconductor p-n junction and dominantly exposed reactive facets. Cryst. Growth Des. 16, 221–228 (2016)

    Article  CAS  Google Scholar 

  13. H. Cheng, B. Huang, Y. Dai, X. Qin, X. Zhang, One-step synthesis of the nanostructured AgI/BiOI composites with highly enhanced visible-light photocatalytic performances. Langmuir 26, 6618–6624 (2010)

    Article  CAS  Google Scholar 

  14. Y. Xu, M.A. Schoonen, The absolute energy positions of conduction and valence bands of selected semiconducting minerals. Am. Mineral. 85, 543–556 (2000)

    Article  CAS  Google Scholar 

  15. M.C. Long, W.M. Cai, J. Cai et al., Efficient photocatalytic degradation of phenol over Co3O4/BiVO4 composite under visible light irradiation. J. Phys. Chem. B. 110(41), 20211–20216 (2006)

    Article  CAS  Google Scholar 

  16. H. Zhang, R. Zong, J. Zhao et al., Dramatic visible photocatalytic degradation performances due to synergetic effect of titanium dioxide with PANI. Environ. Sci. Technol. 42(10), 3803–3807 (2008)

    Article  CAS  Google Scholar 

  17. F. Dong, T. Xiong, Y.J. Sun, Y.X. Zhang, Y. Zhou, Controlling interfacial contact and exposed facets for enhancing photocatalysis via 2D-2D heterostructure. Chem. Commun. 10, 1039 (2010)

    Google Scholar 

  18. J. Wu, X. Chen, C. Li, Y. Qi, X. Qi, J. Ren, B. Yuan, B. Ni, R. Zhou, J. Zhang, T. Huang, Hydrothermal synthesis of carbon spheres—BiOI/BiOIO3 heterojunctions for photocatalytic removal of gaseous Hg0 under visible light. Chem. Eng. J. 304, 533–543 (2016)

    Article  CAS  Google Scholar 

  19. G. Dai, J. Yu, G. Liu, Synthesis and enhanced visible-light photoelectrocatalytic activity of p-n junction BiOI/titanium dioxide nanotube arrays. J. Phys. Chem. C 115, 7339–7346 (2011)

    Article  CAS  Google Scholar 

  20. J. Zhong, F. Chen, J. Zhang, Carbon-deposited titanium dioxide: synthesis, characterization, and visible photocatalytic performance. J. Phys. Chem. C 114, 933–939 (2010)

    Article  CAS  Google Scholar 

  21. Y. Zhang, Z. Zhao, J. Chen, L. Cheng, J. Chang, W. Sheng, C. Hu, S. Cao, C-doped hollow titanium dioxide spheres: in situ synthesis, controlled shell thickness, and superior visible-light photocatalytic activity. Appl. Catal. B 165, 715–722 (2015)

    Article  CAS  Google Scholar 

  22. H. Li, D. Wang, H. Fan, P. Wang, T. Jiang, T. Xie, Synthesis of highly efficient C doped titanium dioxide photocatalyst and its photo-generated charge-transfer properties. J. Colloid Interface Sci. 354, 175–180 (2011)

    Article  CAS  Google Scholar 

  23. J. Zhuang, Q. Tian, H. Zhou, Q. Liu, P. Liu, H. Zhong, Hierarchical porous titanium dioxide@C hollow microspheres: one-pot synthesis and enhanced visible-light photocatalysis. J. Mater. Chem. 22, 7036–7042 (2012)

    Article  CAS  Google Scholar 

  24. X. Chen, P.-A. Glans, X. Qiu, S. Dayal, W.D. Jennings, K.E. Smith, C. Burda, J. Guo, X-ray spectroscopic study of the electronic structure of visible-light responsive N, Cand Sdoped titanium dioxide. J. Electron. Spectrosc. 162, 67–73 (2008)

    Article  CAS  Google Scholar 

  25. X. Chen, C. Burda, The electronic origin of the visible-light absorption properties of C, N and S doped titanium dioxide nanomaterials. J. Am. Chem. Soc. 130, 5018–5019 (2008)

    Article  CAS  Google Scholar 

  26. S. Sakthivel, H. Kisch, Daylight photocatalysis by carbon-modified titanium dioxide. Angew. Chem. Int. Ed. 42, 4908–4911 (2003)

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Jiang Wu .

Rights and permissions

Reprints and permissions

Copyright information

© 2019 Shanghai Jiao Tong University Press and Springer Nature Singapore Pte Ltd.

About this chapter

Check for updates. Verify currency and authenticity via CrossMark

Cite this chapter

Wu, J., Ren, J., Pan, W., Lu, P., Qi, Y. (2019). Preparation and Characterization Other Photocatalysts. In: Photo-catalytic Control Technologies of Flue Gas Pollutants. Energy and Environment Research in China. Springer, Singapore. https://doi.org/10.1007/978-981-10-8750-9_3

Download citation

  • DOI: https://doi.org/10.1007/978-981-10-8750-9_3

  • Published:

  • Publisher Name: Springer, Singapore

  • Print ISBN: 978-981-10-8748-6

  • Online ISBN: 978-981-10-8750-9

  • eBook Packages: EnergyEnergy (R0)

Publish with us

Policies and ethics