Abstract
It has been realized in recent decades that a proper investigation of gasification reactor requires the detailed information over the entire flow field, as well as time, at multiple scales. Such detailed information needs the use of sophisticated measuring techniques with capability to provide the required information over the entire flow field, as well as time, at multiple scales. Aside from the mean velocities and volume fractions, information about the flow fluctuations or dynamics (quantified in terms of cross-correlations and auto-correlations) is also desirable. In addition, it is preferable if such techniques are amenable to automation to reduce extensive human involvement in the data collection process. While such data are “stand-alone” sets of information, which can be used for design and scale-up strategies, it also provides information that is crucial to establish the validity of conventional models like phenomenological flow models describing residence time distribution (RTD), as well as more recent and sophisticated models like those based on computational fluid dynamics (CFD). In fact, it almost seems imprudent to validate CFD predictions on overall holdup and flow rates, because these spatial integrals of point properties are simply averages of a complete flow field that a CFD code is designed to and claims to compute. Thus, fair validation must involve validation at multiple scales, for which one needs experimental information also at multiple scales (and not just spatial and temporal averages). Several experimental techniques have been reported in past to quantify the flow field in gas–solid gasification reactors, with each technique having its own advantages and disadvantages. In this chapter, details of pressure, solid velocity, solid fraction, and RTD measurement techniques will be presented. Techniques will be divided majorly in two types, invasive and non-invasive. The postprocessing methods for each technique, advantages, and limitations will be discussed. Finally, some of the recent findings on gas–solids circulating fluidized bed using radioactive particle tracking (RPT) technique will be discussed in detail to explain the use of the experimental techniques for design and scale-up of these reactors.
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References
Ambler PA, Milne BJ, Berruti F, Scott DS (1990) Residence time distribution of solids in a circulating fluidized bed: experimental and modeling studies. Chem Eng Sci 45(8):2179–2188
Bader R, Findlay J, Knowlton TM (1988) Gas/solid flow patterns in a 30.5-cm-diameter circulating fluidized bed riser. In: Basu P, Large JF (eds) Circulating fluidized bed technology II. Pergamon, Oxford, pp 123–137
Bi J, Yang G, Kojima T (1995) Lateral mixing of coarse particles in fluidized beds of fine particles. Trans Inst Chem Eng 73:162–167
Breault RW (2010) Gasification processes old and new: a basic review of the major technologies. Energies 3(2):216–240
Bhusarapu S (2005) Solid flow mapping in gas-solid risers. DSc thesis, Washington University, USA
Bhusarapu S, Al-Dahhan MH, Dudukovic MP (2004) Quantification of solids flow in a gas–solid riser: single radioactive particle tracking. Chem Eng Sci 59:5381–5386
Bhusarapu S, Al-Dahhan MH, Duduković MP (2006) Solids flow mapping in a gas–solid riser: Mean holdup and velocity fields. Powder Technol 163:98–123
Bhusarapu S, Cassanello M, Al-Dahhan MH, Dudukovic MP, Trujillo S, O’Hern TJ (2007) Dynamical features of solids motion in gas-solid risers. Int J Multiph Flow 33:164–181
Callaghan PT (1991) Principles of nuclear magnetic resonance microscopy. Clarendon Press, Oxford
Caloz YP (2000) Experimental investigation of local solids fluid dynamics in different industrial-scale circulating fluidized beds with optical probes. PhD thesis, Swiss Federal Institute of Technology, Zurich
Cassanello M, Larachi F, Marie-Noelle M, Guy C, Chaouki J (1995) Experimental characterization of the solid phase chaotic dynamics in three-phase fluidization. Ind Eng Chem Res 34(9):2971–2980
Cents AHG, Kersten SRA, Brilman DWF (2003) Gas-Phase RTD Measurement in Gas and Gas−Solids Reactors Using Ultrasound. Ind Eng Chem Res 42:5506–5515
Chan CW, Seville J, Yang Z, Baeyens J (2009) Particle motion in the CFB riser with special emphasis on PEPT-imaging of the bottom section. Powder Technol 196:318–325
Chaouki J, Larachi F, Dudukovic MP (1997) Noninvasive tomographic and velocimetric monitoring of multiphase flows. Ind Eng Chem Res 36(11):4476–4503
Chen RC, Fan LS (1992) Particle image velocimetry for characterizing the flow structure in three-dimensional gas-liquid-solid fluidized beds. Chem Eng Sci 47:3615–3622
Chew JW, Hays R, Findlay JG, Knowlton TM, Reddy Karri SB, Cocco RA, Hrenya CM (2012) Cluster characteristics of Geldart Group B particles in a pilot-scale CFB riser. II. Polydisperse systems. Chem Eng Sci 68:72–81
Cui H, Chaouki J (2004) Effects of temperature on local two-phase flow structure in bubbling and turbulent fluidized beds of FCC particles. Chem Eng Sci 59(16):3413–3422
Cutolo A, Rendima I, Arena U, Marzocchella A, Massimilla L (1990) Optoelectronic technique for the characterization of high concentration gas-solid suspension. Appl Opt 29:1317–1322
Degaleesan S (1997) Fluid dynamic measurements and modeling of liquid mixing in bubble columns. DSc thesis, Washington University, St. Louis
Delnoij E, Kuipers JAM, van Swaaij WPM, Westerweel J (2000) Measurement of gas-liquid two-phase flow in bubble columns using ensemble correlation PIV. Chem Eng Sci 55:3385–3395
Du B, Warsito W, Fan LS (2003) Bed nonhomogeneity in turbulent gas-solid fluidization. AIChE J 49(5):1109–1126
Durst F, Melling A, Whitelaw JH (1981) Principles and practice of laser Doppler anemometry. Academic press, London
Dyakowski T, Edwards RB, Xie CG, Williams RA (1997) Application of capacitance tomography to gas–solid flows. Chem Eng Sci 52:2099–2110
Fan LT, Ho TC, Hiraoka S, Walawender WP (1981) Pressure fluctuations in fluidized bed AIChE J 27:388–396
Fraguío MS, Cassanello MC, Larachi F, Chaouki J (2006) Flow regime transition pointers in three-phase fluidized beds inferred from a solid tracer trajectory. Chem Eng Process Process Intensif 45:350–358
Gao X, Wu C, Cheng Y, Wang L, Li X (2012) Experimental and numerical investigation of solid behavior in a gas–solid turbulent fluidized bed. Powder Technol 228:1–13
Geldart D, Kelsey JR (1972) The use of capacitance probes in gas fluidised beds. Powder Technol 6(1):45–50
Geldart D, Xie HY (1992) The use of pressure probes in fluidized beds of group a powders. In: Potter OE, Nicklin DJ (eds) Fluidization VII. Engineering Foundation, New York, USA, pp 749–756
Gladden LF (1994) Nuclear magnetic resonance in chemical engineering: principles and applications. Chem Eng Sci 49:3339–3408
Gladden LF, Alexander P (1996) Applications of nuclear magnetic resonance imaging in process engineering. Meas Sci Technol 7:423–435
Gopalan B, Shaffer F (2013) Higher order statistical analysis of Eulerian particle velocity data in CFB risers as measured with high speed particle imaging. Powder Technol 242:13–26
Hage B, Werther J (1997) The guarded capacitance probe—a tool for the measurement of solids flow patterns in laboratory and industrial fluidized bed combustors. Powder Technol 93:235–245
Hampel U, Speck M, Koch D, Menz H-J, Mayer H-G, Fietz J, Hoppe D, Schleicher E, Prasser H-M (2005) Experimental ultra fast X-ray computed tomography with a linearly scanned electron beam source. Flow Meas Instrum 16:65–72
Harris AT, Davidson JF, Thorpe RB (2003) Particle residence time distributions in circulating fluidised beds. Chem Eng Sci 58:2181–2202
Hartge EU, Rensner D, Werther J (1988) Solids concentration and velocity patterns in circulating fluidized beds. In: Basu P, Large JF (eds) Circulating fluidized bed technology II. Pergamon, Oxford, pp 165–180
Hassan YA, Blanchat TK, Seeley CH Jr, Canaan RE (1992) Simultaneous velocity measurements of both components of a two-phase flow using particle image velocimetry. Int J Multiph Flow 18:371–395
He Y, Deen NG, Annaland MVS, Kuipers JAM (2009) Gas–solid turbulent flow in a circulating fluidized bed riser: experimental and numerical study of monodisperse particle systems. Ind Eng Chem Res 48(17):8091–8197
Hori K, Fujimoto T, Kawanishi K (1996) Application of cadmium telluride detector to high speed X-ray CT scanner. Nucl Instrum Methods A 380–397
Isaksen O (1996) A review of reconstruction techniques for capacitance tomography. Meas Sci Technol 7:325–337
Johansen GA, Froystein T, Hjertaker BT, Olsen O (1996) A dual sensor flow imaging tomographic system Meas. Sci Technol 7:297–307
Johnsson H, Johnsson F (2001) Measurements of local solids volume-fraction in fluidized bed boilers. Powder Technol 115(1):13–26
Kamalanathan P (2016) Investigation of gas solid circulating fluidized bed at two scales using experimental and numerical techniques. PhD thesis, IIT Guwahati, India
Keane RD, Adrian RJ (1992) Theory of cross-correlation analysis of PIV images. Appl Sci Res 49:191–215
Kunii D, Yosmda K, Hmxta J (1967) The behaviour of freely bubbling fluidized beds. In: Proceedings of the international symposium on fluidization, 243, Eindhoven
Kunii D, Levenspiel O (1991) Fluidization engineering, 2nd edn. Butterworth-Heinemann, Stoneham
Kumar S (1994) Computed tomographic measurements of void fraction and modeling of the flow in bubble columns. PhD thesis, Florida Atlantic University, USA
Lange K, Carson R (1984) EM reconstruction algorithms for emission and transmission tomography. J Comput AssistTomogr 8:306–316
Ligrani PM, Singer BA, Baun LR (1989) Miniature five-hole pressure probe for measurement of three mean velocity components in low-speed flows. J Phys E: Sci Instrum 22:868–876
Lischer OJ, Louge MY (1992) Optical fiber measurements of particle concentration in dense suspensions: calibration and simulation. Appl Optics 31:5106–5113
Liu J, Grace JR, Bi X (2003) Novel multifunctional optical-fiber probe: II. Development and validation. AIChE J 49(6):1405–1420
Mahmoudi S, Seville JPK, Baeyens J (2010) The residence time distribution and mixing of the gas phase in the riser of a circulating fluidized bed. Powder Technol 203(2):322–330
Manyele SV, Pärssinen JH, Zhu J (2002) Characterizing particle aggregates in a high-density and high-flux CFB riser. Chem Eng J 88:151–161
Muller CR, Davidson JF, Dennis JS, Fennell PS, Gladden LF, Hayhurst AN, Mantle MD, Rees AC, Sederman AJ (2007) Rise velocities of bubbles and slugs in gas-fluidised beds: ultra-fast magnetic resonance imaging. Chem Eng Sci 62:82–93
Nauman EB, Buftham BA (1983) Mixing in continuous flow systems. Wiley, NY
Nauman EB (2008) Residence time theory. Ind Eng Chem Res 47:3752–3766
Nieuwland JJ, Meijer R, Kuipers JAM, van Swaaij WPM (1996) Measurements of solids concentration and axial solids velocity in gas-solid two-phase flows. Powder Technol 87(2):127–139
Nijenhuis J, Korbee R, Lensselink J, Kiel JHA, van Ommen JR (2007) A method for agglomeration detection and control in full-scale biomass fired fluidized beds. Chem Eng Sci 62:644–654
O’Sullivan JA, Benac J (2007) Alternating minimization algorithms for transmission tomography. IEEE Trans Med Imaging 26:283–297
Pant HJ, Sharma VK, Goswami S, Samantray JS, Mohan IN, Naidu T (2014) Residence time distribution study in a pilot-scale gas -solid fluidized bed reactor using radiotracer technique. J Radioanal Nucl Chem 302:1283–1288
Pantzali MN, Lozano Bayón N, Heynderickx GJ, Marin GB (2013) Three-component solids velocity measurements in the middle section of a riser. Chem Eng Sci 101:412–423
Pantzali MN, De Ceuster B, Marin GB, Heynderickx GJ (2015) Three-component particle velocity measurements in the bottom section of a riser. Int J Multiph Flow 72:145–154
Parker DJ, Dijkstra AE, Martin ITW, Seville JPK (1997) Positron emission particle tracking studies of spherical particle motion in rotating drums. Chem. Engng. Sci. 52:2011–2022
Parker DJ, Forster RN, Fowles P, Takhar PS (2002) Positron emission particle tracking using the new Birmingham positron camera. Nucl Instrum Meth A 477:540–545
Parker DJ, Fan X (2008) Positron emission particle tracking—application and labelling techniques. Particuology 6:16–23
Patience GS, Chaouki J, Grandejean BPA (1990) Solids flow metering from pressure drop measurement in circulating fluidized beds. Powder Technol 61:95–99
Patience GS, Chaouki J (1993) Gas phase hydrodynamics in the riser of a circulating fluidized bed. Chem Eng Sci 48:3195–3205
Powell RL (2008) Experimental techniques for multiphase flows. Phys Fluids 20:040605-1–040605-22
Prasad AK (2000) Particle image velocimetry. Curr Sci 79:51–60
Rados N, Shaikh A, Al-Dahhan MH (2005) Solids flow mapping in a high pressure slurry bubble column. Chem Eng Sci 60:6067–6072
Reese J, Fan LS (1994) Transient flow structure in the entrance region of a bubble column using particle image velocimetry. Chem Eng Sci 49:5623–5636
Reinecke N, Mewes D (1994) Resolution enhancement for multi-electrode capacitance sensors. In: Proceedings of European concerted action on process tomography, Oporto, pp 50–61
Rhodes MJ, Zhou S, Hirama T, Cheng H (1991) Effects of operating conditions on longitudinal solids mixing in a circulating fluidized bed riser. AIChE J 37:1450–1458
Roy S (2000) Quantification of two-phase flow in liquid-solid risers. PhD thesis, Washington University, USA
Roy S, Kemoun A, Al-Dahhan MH, Dudukovic MP (2005) Experimental Investigation of the Hydrodynamics in a Liquid-Solid Riser. AIChE J 51:802–835
Sanaei S, Mostoufi N, Radmanesh R, Sotudeh-Gharebagh R, Guy C, Chaouki J (2010) Hydrodynamic characteristics of gas-solid fluidization at high temperature. Can J Chem Eng 88:1–11
Sederman AJ, Johns ML, Bramley AS, Alexander P, Gladden LF (1997) Magnetic resonance imaging of liquid flow and pore structure within packed beds. Chem Eng Sci 52:2239–2250
Sederman AJ, Johns ML, Alexander P, Gladden LF (1998) Structure-flow correlations in packed beds. Chem Eng Sci 53:2117–2128
Sederman AJ, Gladden LF (2001) Magnetic resonance imaging as a quantitative probe of gas-liquid distribution and wetting efficiency in trickle-bed reactors. Chem Eng Sci 56:2615–2628
Seville JPK, Ingram A, Parker DJ (2005) Probing processes using positrons. Chem Eng Res Des 83:788–793
Sharma AK, Tuzla K, Matsen J, Chen JC (2000) Parametric effects of particle size and gas velocity on cluster characteristics in fast fluidized beds. Powder Technol 111(1–2):114–122
Shi TM, Xie CG, Huang SM, Williams RA, Beck MS (1991) Capacitance-based instrumentation for multi-interface level measurement. Meas Sci Technol 2:923–933
Smolders K, Baeyens J (2000) Overall solids movement and solids residence time distribution in a CFB-riser. Chem Eng Sci 55:4101–4116
Soong CH, Tuzla K, Chen JC (1993) Identification of particle clusters in circulating fluidized bed. In: Avidan AA (ed) Proceedings of 4th international conference on circulating fluidized beds. Somerset, USA, pp 615–620
Sun J, Yan Y (2016) Non-intrusive measurement and hydrodynamics characterization of gas–solid fluidized beds: a review. Meas Sci Technol 27:112001
Tartan M, Gidaspow D (2004) Measurement of granular temperature and stresses in risers. AIChE J 50:1760–1775
Upadhyay RK (2010) Investigation of multiphase reactors using radioactive particle tracking. PhD thesis, IIT Delhi, India
Upadhyay RK, Roy S, Pant HJ (2012) Benchmarking Radioactive Particle Tracking (RPT) with Laser Doppler Anemometry (LDA). Int J Chem React Eng 10:1–14
Upadhyay RK, Pant HJ, Roy S (2013) Liquid flow patterns in rectangular air-water bubble column investigated with radioactive particle tracking. Chem Eng Sci 96:152–164
van Ommen JR, van der Schaaf J, Schouten JC, van Wachem BGM, Coppens M-O, van den Bleek CM (2004) Optimal placement of probes for dynamic pressure measurements in large-scale fluidized beds. Powder Technol 139:264–276
van Ommen JR, Mudde RF (2008) Measuring the gas-solids distribution in fluidized beds—a review. Int J Chem React Eng 6:1–29
van Ommen JR, Sasic S, van der Schaaf J, Gheorghiu S, Johnsson F, Coppens MO (2011) Time-series analysis of pressure fluctuations in gas-solid fluidized beds—a review. Int J Multiph Flow 37:403–428
Varma R, Bhusarapu S, O’Sullivan JA, Al-Dahhan MH (2008) A comparison of alternating minimization and expectation maximization algorithms for single source gamma ray tomography. Meas Sci Technol 19(015506):1–13
Warsito W, Fan LS (2001) Network based multi-criterion optimization image reconstruction technique for imaging two-and three-phase flow systems using electrical capacitance tomography. Meas Sci Technol 12:2198–2210
Wei F, Wang Z, Jin Y, Yu Z, Chen W (1994) Dispersion of lateral and axial solids in a concurrent down flow circulating fluidization. Powder Technol 81:25–30
Werther J, Molerus O (1973) The local structure of gas fluidized beds. II: The spatial distribution of bubbles. Int J Multiph Flow 1:123–138
Werther J, Hartge EU, Kruse M (1992) Radial gas mixing in the upper dilute core of a circulating fluidized bed. Powder Technol 70:293–301
Xu J, Zhu JX (2012) A new method for the determination of cluster velocity and size in a circulating fluidized bed. Ind Eng Chem Res 51:2143–2151
Xu G, Liang C, Chen X, Liu D, Xu P, Shen L, Zhao C (2013) Investigation on dynamic calibration for an optical-fiber solids concentration probe in gas-solid two-phase flows. Sensors 13(7):9201–9222
Yang WQ, Spink DM, York TA, McCann H (1999) An image reconstruction algorithm based on Landweber’s iteration method for electrical-capacitance tomography. Meas Sci Technol 10:1065–1069
Yang Z, Parker DJ, Fryer PJ, Bakalis S, Fan X (2006) Multiple-particle tracking an improvement for positron particle tracking. Nucl Instrum Meth A 564:332–338
Yang Z, Fryer PJ, Bakalis S, Fan X, Parker DJ, Seville JPK (2007) An improved algorithm for tracking multiple, freely moving particles in a positron emission particle tracking system. Nucl Instrum Meth A 577:585–594
Yang J, Zhu J (2014) A novel method based on image processing to visualize clusters in a rectangular circulating fluidized bed riser. Powder Technol 254:407–415
Zhang M, Qian Z, Yu H, Wei F (2003) The solid flow structure in a circulating fluidized bed riser/downer of 0.42-m diameter. Powder Technol 129:46–52
Zhang Z (2010) LDA application methods. Springer, Heidelberg
Zheng CG, Tung YK, Li HZ, Kwauk M (1992) Characteristics of fast fluidized beds with internals. In: Proceedings of the 7th engineering foundation conference on fluidization. Brisbane, Australia, pp 275–283
Zhu J, Li G, Qin S, Li F, Zhang H, Yang Y (2001) Direct measurements of particle velocities in gas—solids suspension flow using a novel five-fiber optical probe. Powder Technol 115:184–192
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Kamalanathan, P., Upadhyay, R.K. (2018). Measurement Techniques: Cold Flow Studies. In: De, S., Agarwal, A., Moholkar, V., Thallada, B. (eds) Coal and Biomass Gasification. Energy, Environment, and Sustainability. Springer, Singapore. https://doi.org/10.1007/978-981-10-7335-9_7
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