Skip to main content

Comparison of Aroma Compounds in Sauce-Flavor and Sesame-Flavor “Shan Zhuang Lao Jiu” Liquors by Headspace Solid-Phase Microextraction Coupled with Gas Chromatography-Mass Spectrometry

  • Conference paper
  • First Online:
Advances in Applied Biotechnology (ICAB 2016)

Part of the book series: Lecture Notes in Electrical Engineering ((LNEE,volume 444))

Included in the following conference series:

  • 1900 Accesses

Abstract

A method was used for the analysis of aroma compounds in sauce-flavor and sesame-flavor “Shan Zhuang Lao Jiu” liquors based on headspace solid-phase microextraction (HS-SPME) coupled with gas chromatography-mass spectrometry (GC-MS). By the method, a total of 120 aroma compounds were identified, of which 103 aroma compounds were identified in sauce-flavor liquor and 115 in sesame-flavor liquor. Both the sauce-flavor liquor aroma and sesame-flavor liquor aroma were mainly contributed by esters, alcohols and aldehydes. However, the content of acids (1.27 and 0.84%) was relatively less. Moreover, seventeen key aroma compounds were quantified by the approximated curve using the linear least-squares method. Among, isoamyl alcohol showed the highest content (468.59 mg/L) in sauce-flavor liquor, while ethyl hexanoate showed the highest content (667.09 mg/L) in sesame-flavor liquor. Butyl acetate (2.06 mg/L) was a unique compound of the sesame-flavor liquor.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 169.00
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 219.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 219.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

References

  1. Fan W, Qian MC (2006) Identification of aroma compounds in Chinese ‘Yanghe Daqu’ liquor by normal phase chromatography fractionation followed by gas chromatography/olfactometry. Flavour Fragr J 21(2):333–342

    Article  CAS  Google Scholar 

  2. Zhu S, Lu X, Ji K et al (2007) Characterization of flavor compounds in Chinese liquor Moutai by comprehensive two-dimensional gas chromatography/time-of-flight mass spectrometry. Anal Chim Acta 597(2):340–348

    Article  CAS  Google Scholar 

  3. Ferreira V, López R, Cacho JF (2000) Quantitative determination of the odorants of young red wines from different grape varieties. J Sci Food Agric 80:1659–1667

    Article  CAS  Google Scholar 

  4. López R, Aznar M, Cacho J et al (2002) Determination of minor and trace volatile compounds in wine by solid-phase extraction and gas chromatography with mass spectrometric detection. J Chromatogr A 966:167–177

    Article  Google Scholar 

  5. Fan W, Shen H, Xu Y (2011) Quantification of volatile compounds in Chinese soy sauce aroma type liquor by stir bar sorptive extraction and gas chromatography–mass spectrometry. J Sci Food Agric 91(7):1187–1198

    Article  CAS  Google Scholar 

  6. Boutou S, Chatonnet P (2007) Rapid headspace solid-phase microextraction/gas chromatographic/mass spectrometric assay for the quantitative determination of some of the main odorants causing off-flavours in wine. J Chromatogr A 1141:1–9

    Article  CAS  Google Scholar 

  7. Du LP, He TT, Li W (2015) Analysis of volatile compounds in Chinese Laobaigan liquor using headspace solid-phase microextraction coupled with GC-MS. Anal Methods 7:1906–1913

    Article  CAS  Google Scholar 

  8. Fan W, Qian MC (2005) Headspace solid phase micro-extraction (HS–SPME) and gas chromatography-olfactometry dilution analysis of young and aged Chinese “Yanghe Daqu” liquors. J Agric Food Chem 53(20):7931–7938

    Article  CAS  Google Scholar 

  9. Luo T, Fan W, Xu Y (2008) Characterization of volatile and semi-volatile compounds in Chinese rice wines by headspace solid phase microextraction followed by gas chromatography-mass spectrometry. J Inst Brew 114(2):172–179

    Article  CAS  Google Scholar 

  10. Chin HW, Lindsay RC (1994) Mechanisms of formation of volatile sulfur compounds following the action of cysteine sulfoxide lyases. J Agric Food Chem 42:1529–1536

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Corresponding author

Correspondence to Liping Du .

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 2018 Springer Nature Singapore Pte Ltd.

About this paper

Cite this paper

Liu, F., Yin, W., Du, L., Xiao, D. (2018). Comparison of Aroma Compounds in Sauce-Flavor and Sesame-Flavor “Shan Zhuang Lao Jiu” Liquors by Headspace Solid-Phase Microextraction Coupled with Gas Chromatography-Mass Spectrometry. In: Liu, H., Song, C., Ram, A. (eds) Advances in Applied Biotechnology. ICAB 2016. Lecture Notes in Electrical Engineering, vol 444. Springer, Singapore. https://doi.org/10.1007/978-981-10-4801-2_25

Download citation

Publish with us

Policies and ethics