Abstract
Chemical analysis of C-fibres after controlled surface treatment (wet oxidation and anodic oxidation)have been performed by total oxygen and nitrogen analysis, organic blocking methods, thermal desorption with in situ gas analysis, ESCA and IGC.
Additionally, the fibre surfaces have been characterized by BET, Laser RAMAN Spectroscopy and Relative Fibre Capacitance (RFC).
The effect of surface treatment on the adhesion in resins was measured directly by the conventional ILSS method. RFC-results correlate surprisingly well with ILSS data.
It is shown, that the improved adhesion by surface treatment is mainly due to chemical interaction in the interface. BET-effects play a minor role. Carboxylic groups contribute not more than 1/3 to the effect caused by the total of surface oxides. The role of basicity is discussed in more detail.
This is a preview of subscription content, log in via an institution to check access.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
Preview
Unable to display preview. Download preview PDF.
References
K.-H. Geigl, Ph.D. Thesis, University of Karlsruhe, FRG, Institut für Chemische Technik (1980)
R. Weil, Ph.D. Thesis, University of Karlsruhe, FRG, Institut für Chemische Technik (1983)
H. Jäger, Ph.D. Thesis, University of Karlsruhe, FRG, Institut für Chemische Technik (1986)
J.B. Donnet, E. Papirer, H. Dauksch, Int.Conf. on Carbon Fibres, Their Place in Modern Technology, London, paper 9 (1974)
E. Fitzer, K.-H. Geigl and L.M. Manocha, Proc. of the 5th London Inter.Carbon and Graphite Conf., 405–418 (1978)
H.-P. Boehm, E. Diehl and E. Heck, Proc. 2nd Int. Conf. on Carbon and Graphite, London, p. 369 (1966)
E. Fitzer and R. Weill, Carbon 25, 455–467 (1987)
E. Fitzer and H. Jäger, Proc. 4th Int. Carbon Conf. Baden-Baden, 863–866 (1986)
E. Fitzer and H. Jäger, Ext. Abstracts, 17th Bienn. Conf. of Carbon, 317–319 (1985)
E. Fitzer and M. Heine, Fibre Reinforcement for Composite Materials, edit. A.R. Bunsel, 73–148 (1988)
E. Fitzer, H. Jäger, von Sturm, F., N. Popovska, Journal of Applied Electrochemistry 18, 178–182 (1988)
R. Spiegler, Master thesis, University of Karlsruhe, FRG, Institut für Chemische Technik (1988)
S. Dong, Ph.D.Thesis, Université de Haute Alsace (1989)
F. Künkele, Ph.D.Thesis, University of Karlsruhe, FRG, Institut für Chemische Technik - in preparation -
A.F. Mac Lean and I.L. Kalnin, US-Pat. 3. 864. 626, (1975)
I.L. Kalnin, Preprints 2nd Int. Carbon 76, Deutsche Keramische Gesellschaft, Bad Honnef, FRG, 94–98 (1976)
E. Fitzer, E. Fuder and H.P. Rensch, 19th Bienn. Conf. on Carbon, Pennstate, 246–247 (1989)
Author information
Authors and Affiliations
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 1990 Elsevier Science Publishing Co., Inc.
About this paper
Cite this paper
Fitzer, E., Rensch, HP. (1990). Carbon Fibre Surfaces and Their Analysis. In: Ishida, H. (eds) Controlled Interphases in Composite Materials. Springer, Dordrecht. https://doi.org/10.1007/978-94-011-7816-7_24
Download citation
DOI: https://doi.org/10.1007/978-94-011-7816-7_24
Publisher Name: Springer, Dordrecht
Print ISBN: 978-94-011-7818-1
Online ISBN: 978-94-011-7816-7
eBook Packages: Springer Book Archive