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119mSn Mössbauer studies on tin compounds

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Book cover Chemistry of Tin

Abstract

Information extracted from 119Sn Mössbauer spectroscopy of tin compounds essentially concerns (1) the valence state in inorganic derivatives, (2) structure and bonding in the m et al. environment (mainly in organotins) and (3) the dynamics of tin nuclei, the latter possibly correlated to the nature of the substrate (mono- or polymeric). Measurements are effected on solids (crystalline as well as amorphous), gels and solutions (frozen to glassy phases). It then appears that Mössbauer spectroscopic measurements give information analogous, or complementary, to data gained from other spectroscopic techniques, such as NMR spectroscopy, X-ray diffractometry, neutron diffraction, etc. There are advantages, as well as disadvantages, in the data extracted from Mössbauer spectroscopy: the first concerns, inter alia, the easy experimental procedures, the simple and inexpensive instrumentation, the possibility of obtaining information about the m et al. properties in high molecular weight systems; the second lies essentially in the time needed to collect a spectrum (∼1 day). In fact, the circumstance that the absorber samples must contain Sn at the milligram level [about 0.5(mg119Sn)cm-2], and the near impossibility of quantitative Sn analysis, are common to other widely employed spectroscopic techniques.

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Authors
  1. Renato Barbieri
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  2. Friedo Huber
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  3. Lorenzo Pellerito
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  4. Gìuseppe Ruisi
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  5. Arturo Silvestri
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Editors and Affiliations

  1. Department of Chemistry, Christopher Ingold Laboratories, University College London, 20 Gordon Street, WC1H 0AJ, London, UK

    Peter J. Smith (Honorary Research Fellow) (Honorary Research Fellow)

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Barbieri, R., Huber, F., Pellerito, L., Ruisi, G., Silvestri, A. (1998). 119mSn Mössbauer studies on tin compounds. In: Smith, P.J. (eds) Chemistry of Tin. Springer, Dordrecht. https://doi.org/10.1007/978-94-011-4938-9_14

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