Abstract
Pollution is said to exist when the concentration of a contaminant is large enough to interfere with the normal use of the environment and the wellbeing of biota, especially Man. In order to quantify the effects of these contaminants measurements of their concentrations have to be made. In some cases it is possible to make measurements directly within the environmental reservoirs themselves by deployment of appropriate probes, but more frequently a sample of that compartment will have to be isolated and adequately processed before a final measurement can be made. A knowledge of pollutant levels may help to trace the origin of contaminants and to follow their decay processes and effects in the environment. Sampling may also be necessary to ensure the enforcement and adequacy of control measures on emissions.
Sadly Aristides Hall passed away during the preparation of this book.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
Preview
Unable to display preview. Download preview PDF.
References
Butcher, S. S. & Ruff, R. E., The effect of inlet residence time on the analysis of atmospheric nitrogen oxides and ozone. Analyt. Chem., 43 (1971) 1890–2.
Bowermaster, J. & Shaw, R. W. Jr, A source of gaseous HNO3 and its transmission efficiency through various materials. J. Air Pollut. Control Assoc., 31 (1981) 787–8.
Crittenden, P. P. & Read, D. J., PVC sample line interference with daily sulphur dioxide measurement. Atmos. Environ., 10 (1976) 897–8.
Smith, J. R., Estimating overall sample train efficiency. J. Air Pollut. Control Assoc., 29 (1979) 969–70.
Adams, D. F., Sulphur compounds. In Air Pollution, Vol. III, ed. A. C. Stern. Academic Press, New York, 1976.
Bracewell, J. M. & Hodgson, A. E. M., The hydrogen peroxide method for sulphur dioxide in the atmosphere-efficiency at low concentrations by radioactive tracer techniques. Int. J. Air Water Pollut., 9 (1965) 431–8.
BSI, Methods for the measurement of air pollution-determination of sulphur dioxide. BS 1747-Part III. British Standards Institution, London, 1969.
Persson, G. A., Automatic colorimetric concentration of sulphate for measuring sulphur dioxide in ambient air. J. Air Water Pollut., 10 (1966) 845–52.
West, P. W. & Gaeke, G. C., Fixation of sulphur dioxide as disulphitomercurate(II) and subsequent colorimetric estimation. Analyt. Chem., 28 (1956) 1816–19.
Selvapathy, P., Ramakrishna, T. V., Balasubramanian, N. & Pitchai, R.,Extraction-spectrophotometric determination of sulphur dioxide. Analyst (London), 112 (1987) 1139–41.
Paul, K. R. & Gupta, V. K., Oxaldihydroxamic acid as a new reagent for the fixation of atmospheric sulphur dioxide. Atmos. Environ., 11 (1983) 1773–7.
Leithe, W., The Analysis of Air Pollutants. Ann Arbor Science Publishers, Ann Arbor, 1971.
Baveja, A. K., Chaude, A. & Gupta, V. K., Extractive spectrophotometric method for the determination of atmospheric nitrogen dioxide. Atmos. Environ., 18 (1984) 989–93.
Mulik, J., Fuerst, R., Guyer, M., Meeker, J. & Sawicki, E., Development and optimization of twenty-four hour manual methods for the collection and colorimetric analysis of atmospheric NO,. Analyt. Chem., 3 (1974) 333–48.
Margeson, J. H., Suggs, J. C., Constant, P. C. Jr, Sharp, M. C. & Scheil, G. W., Collaborative testing of manual sodium arsenite method for measurement of nitrogen dioxide in ambient air. Environ. Sci. Technol., 12 (1978) 294–7.
Schenkel, A. & Broder, B., Interference of some trace gases with ozone measurements by KI method. Atmos. Environ., 16 (1982) 2187–90.
Bergshoeff, G., Lanting, R. W., Ham, J. V., Prop, J. M. & Reijneders, H. F., Spectrophotometric determination of ozone in air with indigo disulfonate. Analyst (London), 109 (1984) 1165–9.
Van den Berge, L. P., Devreese, A. & Vanhoorne, M., A simplified method for the determination of hydrogen sulfide in the work environment. Am. Ind. Hyg. Assoc. J., 46 (1985) 693–5.
Margeson, J. H., Knoll, J. E., Midgett, M. R., Ferguson, B. B. & Schworer, P. J., A manual method for measurement of reduced sulphur compounds. J. Air Pollut. Control Assoc., 35 (1985) 1280–5.
Balmat, J. L. & Meadows, G. W., Monitoring of formaldehyde in air. Am. Ind. Hyg. Assoc. J., 46 (1985) 578–84.
Daggett, D. L. & Stock, T. H., An investigation into the storage stability of environmental formaldehyde samples. Am. Ind. Hyg. Assoc. J., 46 (1985) 497–504.
Purnell, C. J. & Walker, R. F., Methods for the determination of atmospheric organic isocyanates: a review. Analyst (London), 110 (1985) 893–905.
Gabay, J., Davidson, M. & Donagi, A. E., Spectrophotometric determination of free chlorine in air. Analyst (London), 101 (1976) 128.
Fisher, R. P., Marks, M. D. & Jett, S. W., Measurement methods for chlorine dioxide emissions from bleach plants. TAPPI J., 70 (1987) 97–102.
Morita, H., Mitshuhashi, T., Sakurai, H. & Shimomura, S., Absorption of mercury by solutions containing oxidants. Analyt. Chim. Acta, 153 (1983) 351–5.
Forrest, J., Tanner, R. L., Spandau, D., Ottavio, T. D. & Newman, L., Determination of total inorganic nitrate utilizing collection of nitric acid on NaCl-impregnated filters. Atmos. Environ., 14 (1980) 137–44.
Okita, T., Morimoto, S. & Izawa, M., Measurement of gaseous and particulate nitrates in the atmosphere. Atmos. Environ., 10 (1976) 1085–9.
Grosjean, D., Quantitative collection of total inorganic atmospheric nitrate on nylon filters. Analyt. Letters, 15 (1982) 785–96.
Thorogood, G., Rapsomanikis, S. & Harrison, R. M., Evaluation of a method for measurement of particulate chloride and gaseous hydrogen chloride in the atmosphere. Contract. Report, University of Essex, August 1986.
Forrest, J., Spandau, P. J., Tanner, R. L. & Newman, L., Determination of atmospheric nitrate and nitric acid employing a diffusion denuder with a filter pack. Atmos. Environ., 16 (1982) 1473–85.
Lewin, E. & Zachau-Christiansen, B., Technical note: efficiency of 0.5N KOH impregnated filters for SO2-collection. Atmos. Environ., 11 (1977) 861–2.
Huygen, C., The sampling of sulphur dioxide in air with impregnated filter paper. Analyt. Chim. Acta, 28 (1962) 349–60.
Lazrus, A. L., Grandrud, B. W., Woodard, R. N. & Sedlacek, W. A., Direct measurement of stratospheric chlorine and bromine. J. Geophys. Res., 81 (1976) 1067–70.
Farwell, S. O., Chatham, W. H. & Barinaga, C. J., Performance characterization and optimization of the AgNO3-filter/FMA fluorimetric method for atmospheric H2S measurements. J. Air Pollut. Control Assoc., 37 (1987) 1052–9.
Walsh, P. R., Duce, R. A. & Fasching, J. L., Impregnated filter sampling system for collection of volatile arsenic in the atmosphere. Environ. Sci. Technol., 11 (1977) 163–6.
Cormis, L. & Cantuel, J., Etude comparative de deux methodes dynamiques de prelevement atmospherique en matiere de pollution fluoree. Pollut. Atmos., 19 (1977) 377–80.
Spicer, C. W., Howes, J. E., Bishop, T. A. & Arnold, L. H., Nitric acid measurement methods: an intercomparison. Atmos. Environ., 16 (1982) 1487–500.
Huebert, B. J. & Lazarus, A. L., Tropospheric measurements of nitric acid vapor and particulate nitrate. In Nitrogeneous Air Pollutants, ed. D. Grosjean. Ann Arbor Science Publishers, Ann Arbor, 1979.
Bourbon, M. P., Alary, J., Escalassan, J. & Lepert, J. C., Dosage du NO atmospherique par captage sur support sec. Atmos. Environ., 11 (1977) 485–8.
Harrison, R. M. & McCartney, H. A., Some measurements of ambient air pollution arising from the manufacture of nitric acid and ammonium nitrate fertilizer. Atmos. Environ., 13 (1979) 1105–20.
Argese, E., Scalet, B., Lavagnini, I. & Rigo, A., Simultaneous collection of sulphur dioxide and sulphate by a selective sampler and their analysis at background levels. Analyst (London), 111 (1986) 543–5.
Anlauf, K. G., Wiebe, H. A. & Fellin, P., Characterization of several integrative sampling methods for nitric acid, sulphur dioxide and atmospheric particles. J. Air Pollut. Control Assoc., 36 (1986) 715–23.
Shaw, R. W., Stevens, R. K., Bowermaster, J., Tesch, J. W. & Tew, E., Measurements of atmospheric nitrate and nitric acid: the denuder difference experiment. Atmos. Environ., 16 (1982) 845–53.
Appel, B. R., Tokiwa, Y. & Aik, M., Sampling of nitrates. Atmos. Environ., 15 (1981) 283–9.
Ferm, M., Method for determination of atmospheric ammonia. Atmos. Environ., 13 (1979) 1385–93.
McMurry, P. H. & Stolzenburg, M. R., Mass accommodation coefficients from penetration measurements in laminar tube flow. Atmos. Environ., 21 (1987) 1231–4.
Mulawa, P. A. & Cadle, S. H., A comparison of nitric acid and particulate nitrate measurements by the penetration and denuder difference methods. Atmos. Environ., 19 (1985) 1317–24.
Braman, R. S., Shelley, T. J. & McClenny, W. A., Tungstic acid for preconcentration and determination of gaseous and particulate ammonia and nitric acid in ambient air. Analyt. Chem., 54 (1982) 358–64.
Linqvist, F., Determination of nitric acid in ambient air by gas chromatography//photoionization detection after collection in a denuder. J. Air Pollut. Control Assoc., 35 (1985) 19–23.
Durham, J. L., Spiller, L. L. & Ellestad, T. G., Nitric acid-nitrate aerosol measurements by a diffusion denuder: a performance evaluation. Atmos. Environ., 21 (1987) 589–98.
Durham, J. L., Wilson, W. E. & Baily, E. B., Application of an SO2-denuder for continuous measurement of sulphur in submicrometer aerosols. Atmos. Environ., 12 (1978) 883–6.
Slanina, J., Schoonebeek, C. A. M., Klockow, D. & Niessner, R., Determination of sulfuric acid and ammonium sulfates by means of a computer-controlled thermo-denuder system. Analyt. Chem., 57 (1985) 1955–60.
Liberti, A., Allegrini, I., Febo, A. & Possanzini, M., Atmospheric acidity: analytical problems related to its determination. In Environmental Inorganic Chemistry, ed. K. J. Irgalic & A. E. Martell. Deerfield Beach, Fla, 1985, pp. 419–30.
Lochmuller, C. H., Dwyer, E. & Spiller, L., Chemically-modified ion exchange membranes as sampling devices for gas-phase ammonia. Analyt. Letters, 18 (1985) 423–8.
De Santis, F., Liberti, A. & Rotatori, M., Determination of hydrochloric acid in air by sampling with high-efficiency diffusion tubes. Acqua Aria, 6 (1985) 529–34.
ASTM, Separation and collection of particulate and gaseous fluorides in the atmosphere (sodium bicarbonate-coated glass tube and particulate filter method). Annual Book of ASTM Standards, Part 26,1978.
Appel, B. R., Tokiwa, Y. & Kothny, E. L., Sampling of carbonaceous particles in the atmosphere. Atmos. Environ., 17 (1983) 1787–96.
Buttini, P., Di Palo, V. & Possanzini, M., Coupling of denuder and ion chromatographic techniques for nitrogen dioxide trace level determination in air. Sci. Total Environ., 61 (1987) 59–72.
Eatough, D. J., White, V. F., Hansen, L. D.,Eatough, N. L. & Cheney, J. L., Identification of gas-phase dimethyl sulfate and monoethyl sulfate in the Los Angeles atmosphere. Environ. Sci. Technol., 20 (1986) 867–72.
De Santis, F., Di Palo, V. & Perrino, C., Accurate determination of inorganic ions in water-soluble particulate matter by coupling high efficiency diffusion and filtration techniques. J. Aerosol Sci., 17 (1986) 582.
Ferm, M. & Sjodin, A., A sodium carbonate coated denuder for the determination of nitrous acid in the atmosphere. Atmos. Environ., 19 (1985) 979–83.
Possanzini, M., Febo, A. & Liberti, A., New design of a high-performance denuder for the sampling of atmospheric pollutants. Atmos. Environ., 17 (1983) 2605–10.
Hara, H., Kurita, M. & Okita, T., Ammonia denuder for field sampling of sulphuric acid particles. Atmos. Environ., 16 (1982) 1565–6.
Harrison, R. M. & Pio, C. A., Size-differentiated composition of inorganic atmospheric aerosols of both marine and polluted continental origin. Atmos. Environ., 17 (1983) 1733–8.
Stevens, R. K., Russwurm, G., Rickel, D. & Dzubay, T. G., Sampling and analysis of atmospheric sulphates and related species. Atmos. Environ., 12 (1978) 55–68.
Lamb, S. I., Petrowski, C., Kaplan, I. R. & Simoneit, B. R. T., Organic compounds in urban atmospheres: a review of distribution, collection and analysis. J. Air Pollut. Control Assoc., 30 (1980) 1098–115.
Hill, R. H. Jr, McCammon, C. S., Saalwaechter, A. T., Teass, A. W. & Woodfin, W. J., Gas-chromatographic determination of vinyl chloride in air samples collected on charcoal. Analyt. Chem., 48 (1976) 1395–7.
Fraust, C. L., The use of activated carbon for sampling industrial environments. Am. Indust. Hyg. Assoc. J., 36 (1975) 278.
ASTM, Sampling atmospheres to collect organic compound vapors (activated charcoal adsorption method). ASTM D 3686–78. Annual Book of ASTM Standards, Part 26,1978.
Fung, K. K. & Wright, B. J., Monitoring of benzene in ambient air with organic vapor badges. I Air Pollut. Control Assoc., 36 (1986) 819–21.
Van den Hoed, N., Van Asselen, O. L. J. & Van Dongen, J. P. C. M., Replicate side-by-side field comparison of 3M diffusive samplers versus charcoal tube samplers for styrene. Am. Ind. Hyg. Assoc. J., 48 (1987) 252–6.
Vincent, R., Limasset, J. C., Cicolella, A., Hecht, G. & Gerber, J. M., Simultaneous determination of hydrogen sulfide and carbon disulfide in working atmospheres. Analysis, 13 (1985) 415–19.
Wathne, B. M., Measurements of benzene, toluene and xylenes in urban air. Atmos. Environ., 17 (1983) 1713–22.
Pellizzari, E. D., Gutknecht, W. F., Cooper, S. & Hardison, D., Evaluation of sampling methods for gaseous atmospheric samples. EPA-600/3–84–062. Environmental Protection Agency, USA, 1984.
ASTM, Standard practice for analysis of organic compounds vapors collected by the activated charcoal adsorption method. Annual Book of ASTM Standards, Part 26, ASTM D 3687–78,1978.
Guenier, J. P., Simon, P., Delcourt, J., Didierjean, M. F., Lefevre, C. & Muller, J., Air-sampling of aldehydes-application to chromatographic determination of formaldehyde and acetaldehyde. Chromatografia, 18 (1984) 137–44.
Riba, M. L., Randrianalimanana, E., Mathieu, J., Torres, L. & Namiesnik, J., Preconcentration of atmospheric terpenes on solid sorbents. Int. J. Environ. Anal. Chem., 19 (1985) 133–43.
Billings, W. N. & Bidleman, T. F., Field comparison of polyurethane foam and Tenax-GC for high volume air sampling of chlorinated hydrocarbons. Environ. Sci. Technol., 14 (1980) 679–83.
Krist, K. J., Pellizzani, E. D., Walburn, S. G. & Hubbard, S. A., Collection and analysis of hazardous organic emissions. Analyt. Chem., 54 (1982) 810–17.
Van der Straete, N. D., Comparison between theoretical and experimental sampling efficiencies on Tenax GC. J. Chromatogr., 331 (1985) 207–18.
Tangerman, A., Determination of volatile sulfur compounds in air at the parts per trillion level by Tenax trapping and gas chromatography. J. Chromatogr., 366 (1986) 205–16.
Brown, R. H. & Purnell, C. J., Collection and analysis of trace organic vapor pollutants in ambient atmospheres. The performance of a Tenax-GC adsorbent tube. J. Chromatogr., 178 (1979) 79–90.
Walling, J. F., Bumgarner, J. E., Driscoll, D. J., Morris, C. M., Riley, A. E. & Wright, L. H., Apparent reaction products desorbed from Tenax used to sample ambient air. Atmos. Environ., 20 (1986) 51–7.
Crist, H. L. & Mitchell, W. J., Field audit results with organic gas standards on volatile organic ambient air samplers equipped with Tenax GC. Environ. Sci. Technol., 20 (1986) 1260–2.
Josephson, J., Monitoring airborne organics. Environ. Sci. Technol., 15 (1981) 731–3.
Zielinska, B., Arey, J., Ramdahl, T., Atkinson, R. & Winer, A. M., Potential for artifact formation during Tenax sampling of polycyclic aromatic hydrocarbons. J. Chromatogr., 363 (1986) 382–6.
Davies, C. N., Filtration of aerosols. J. Aerosol Sci., 14 (1983) 147–61.
Stafford, R. G. & Ettinger, H. J., Filter efficiency as a function of particle size and velocity. Atmos. Environ., 6 (1972) 353.
Dolske, D. A., Schneider, J. & Sievering, H., Trace element pass-through for cellulose filters when used for aerosol collection. Atmos. Environ., 18 (1984) 2557–8.
John, W. & Reischl, G., Measurements of the filtration efficiencies of selected filter types. Atmos. Environ., 12 (1978) 2015–19.
Liu, B. Y. A. & Lee, K. W., Efficiency of membrane and nucleopore filters for submicrometer aerosols. Environ. Sci. Technol., 10 (1976) 345–50.
Baudo, R., The chemical analysis of particulate matter. Trends Analyt. Chem., 1 (1982) 393–7.
Dams, R., Rahn, K. A. & Winchester, J. W., Evaluation of filter materials and impaction surfaces for nondestructive neutron activation analysis of aerosols. Environ. Sci. Technol., 6 (1972) 441–8.
Sparrow, S. D. & Masiak, D. T., Errors in analyses for ammonium and nitrate caused by contamination from filter papers. Soil Sci. Soc. Am. J., 51 (1987) 107–10.
Leahy, D. F., Phillips, M. F., Garber, R. W. & Tanner, R. L., Filter material for sampling of ambient aerosols. Analyt. Chem., 52 (1980) 1779–80.
Witz, S. & Wendt, J. G., Artifact sulfate and nitrate formation at two sites in the south coast air basin. Environ. Sci. Technol., 15 (1981) 79–83.
Pierson, W. R., Brachaczek, W. W., Truex, T. J. & Butler, J. W., Artifact formation of sulfate, nitrate and hydrogen ion on back-up filters. Allegheny Mountain experiment. J. Air Pollut. Control Assoc., 30 (1980) 30–4.
Appel, B. R., Wall, S. M., Tokiwa, Y. & Haik, M., Interference effects in sampling particulate nitrate in ambient air. Atmos. Environ., 13 (1972) 319–25.
Witz, S., Effect of environmental factors on filter alkalinity and artifact formation. Environ. Sci. Technol., 19 (1985) 831–5.
Pierson, W. R., Hammerle, R. H. & Brachaczek, W. W., Sulfate formed by interaction of sulfur dioxide with filters and aerosol deposits. Analyt. Chem., 48 (1976) 1808–11.
Tanner, R. L., Cederwall, R. & Garber, R., Separation and analysis of aerosol sulfate species at ambient concentrations. Atmos. Environ., 11 (1977) 955–66.
Spicer, C. W. & Schumacher, P. M., Particulate nitrate: laboratory and field studies of major sampling interferences. Atmos. Environ., 13 (1979) 543–52.
Hitchcock, D. R., Spiller, L. L. & Wilson, W. E., Sulfuric acid aerosols and HC1 release in coastal atmospheres: evidence of rapid formation of sulfuric acid particulates. Atmos. Environ., 14 (1980) 165–82.
Appel, B. R. & Tokiwa, Y., Atmospheric particulate nitrate sampling errors due to reactions with particulate and gaseous strong acids. Atmos. Environ., 15 (1981) 1087–9.
Dunwoody, C. L., Rapid nitrate loss from PM10 filters. J. Air Pollut. Control Assoc., 36 (1986) 817–18.
Galasyn, J. F., Horning, J. F. & Soderberg, R. H., The loss of PAH from quartz fiber high volume filters. J. Air Pollut. Control Assoc., 34 (1984) 57–9.
You, F. & Bidleman, T. F., Influence of volatility on the collection of polycyclic aromatic hydrocarbon vapors with polyurethane foam. Environ. Sci. Technol., 18 (1984) 330–3.
Konig, J., Funcke, W., Balfanz, E., Grosch, B. & Pott, F., Testing a high volume air sampler for quantitative collection of polycyclic aromatic hydrocarbons. Atmos. Environ., 14 (1980) 609–13.
Laskus, L., Prescher, K. E. & Baker, D., Evaluation of the relative error. Conditioning of samples of suspended particulates. Staub-Reinhalt. Luft, 45 (1985) 47–53.
Highsmith, V. R., Bond, A. E. & Howes, J. E., Particle and substrate losses during shipment of teflon and quartz filters. EPA-600/9–84–19. Environmental Protection Agency, USA, 1984.
Smith, J. P., Grosjean, D. & Pitts, J. N. Jr, Observation of significant losses of particulate nitrate and ammonium from high volume glass fiber filter samples stored at room temperature. J. Air Pollut. Control Assoc., 28 (1986) 930–3.
Clement, R. E. & Karasek, F. W., Sample composition changes in sampling and analysis of organic compounds in aerosols. Int. J. Environ. Anal. Chem., 7 (1979) 109–20.
Brenchley, D. L., Turley, C. D. & Yarmac, R. F., Industrial Source Sampling. Ann Arbor Science Publishers, Ann Arbor, MI, 1973.
Van der Meulen, A., Van de Vate, J. F., Hofschreuder, P. & Oeseburg, F., Feasibility of high volume sampling for determination of total suspended particulate matter and trace metals. J. Air Pollut. Control Assoc., 31 (1984) 144–51.
Pashel, G. E. & Egner, D. R., A comparison of ambient suspended particulate matter concentrations as measured by the British smoke sampler and high volume sampler at 16 sites in the United States. Atmos. Environ., 15 (1981) 919–27.
Hileman, B., Particulate matter: the inhalable variety. Environ. Sci. Technol., 15 (1981) 983–6.
Miller, S. S., Inhaled particulates. Environ. Sci. Technol., 12 (1978) 1353–5.
Kashdan, E. R., Ranade, M. B., Purdue, L. J. & Rehme, K. A., Interlaboratory evaluation of two inlets for sampling particles less than 10 pm. Environ. Sci. Technol., 20 (1986) 911–16.
Ortiz, C. A. & McFarland, A. R., A 10μm two-stage inlet for sampling indoor aerosols. J. Air Pollut. Control Assoc., 35 (1985) 1057–60.
Rodes, C. E., Holland, D. M., Purdue, L. J. & Rehme, K. A., A field comparison of PM10 inlets at four locations. J. Air Pollut. Control Assoc., 35 (1985) 345–54.
Wedding, J. B., Ambient aerosol sampling. History, present thinking and a proposed inlet for inhalable particles. Environ. Sci. TechnoL, 16 (1982) 154–61.
Miller, F. J., Gardner, D. E., Graham, J. A., Lee, R. E. Jr, Wilson, W. E. & Bachman, J. D., Size concentrations for establishing a standard for inhalable particles. J. Air Pollut. Control Assoc., 29 (1979) 610–15.
Dzubay, T. G., Hines, L. E. & Stevens, R. K., Particle bounce errors in cascade impactors. Atmos. Environ., 10 (1976) 229–34.
Cheng, Y. & Yeh, H., Particle bounce in cascade impactors. Environ. Sci. Technol., 12 (1978) 1392–6.
Lawson, D. R., Impaction surface coatings intercomparison and measurements with cascade impactors. Atmos. Environ., 14 (1980) 195–9.
Markowski, G. R., Reducing blow off in cascade impactor measurements. Aerosol Sci. Technol., 3 (1984) 431–9.
McFarland, A. R., Wedding, J. B. & Cermak, J. E., Wind tunnel evaluation of a modified Anderson impactor and an allweather sampler inlet. Atmos. Environ., 11 (1977) 535–42.
Cushing, K. M., McCain, J. D. & Smith, W. B., Experimental determination of sizing parameters and wall losses of live source-test cascade impactors. Environ. Sci. Technol., 13 (1979) 726–31.
Conner, W. D., An inertial-type particle separator for collecting large samples. J. Air Pollut. Control Assoc., 16 (1966) 35–8.
Marple, V. A. & Chien, C. M., Virtual impactors: a theoretical study. Environ. Sci. Technol., 14 (1980) 976–84.
Dzubay, T. G. & Stevens, R. K., Ambient air analysis with dichotomous sampler and X-ray fluorescence spectrometer. Environ. Sci. Technol., 9 (1975) 663–8.
Kratochvil, B., Wallace, D. & Taylor, J. K., Sampling for chemical analysis. Anal. Chem., 56 (1984) 113R–129R.
Sturgeon, R. & Berman, S. S., Sampling and storage of natural water for trace metals. CRC Crit. Rev. Anal. Chem., 18 (1987) 209–44.
EPA, Handbook for Sampling and Sample Preservation of Water and Wastewater. EPA-600/4–82–029, Cincinnati, 1982,402 pp.
Suess, M. J., Examination of Water for Pollution Control. Vol. 1—Sampling, Data Analysis and Laboratory Equipment. Pergamon Press, Oxford, 1982, 381 pp.
Environment Canada, Sampling for Water Quality. Water Quality Branch, Inland Waters Directorate, Ottawa, 1983, p. 55.
Grasshoff, K., Ehrhardt, M. & Kremling, K. (eds), Methods of Seawater Analysis. Verlag-Chimie, Veinheim, FRG, 1983.
ASTM, Annual Book of ASTM Standards: Water, Vol. 11.01. American Society for Testing and Materials, Philadelphia, PA, 1987.
ISO 5667, Part 1-Guidance on the design of sampling programs; Part 2 Water quality, sampling, guidance on sampling techniques. International Standards Organization, Geneva, 1980.
Lafleur, P. D., Accuracy in Trace Analysis: Sampling, Sample Handling, Analysis. US Government Printing Office, Washington, DC, 1976.
Keith, L. H., Principles of Environmental Sampling. American Chemical Society, Washington, DC, 1988.
ASTM D3370, Standard Practices for Sampling Water. American Society for Testing and Materials, Philadelphia, PA, 1982.
Casey, H. & Walker, S. M., Storage and filtration of water samples. Int. Environ. Safety (October 1981) 16–17.
Eaton, A. D., Inorganics. J. Water Pollut. Control Fed., 59 (1987) 313–28.
Schofield, T., Sampling of water and waste water: practical aspects of sample collection. Water Pollut. Control, 79 (1980) 468–76.
Kratochvil, B. & Tayloy, J. K., Sampling for chemical analysis. Analyt. Chem., 53 (1981) 924A–938A.
Mickelson, M. J., Axelrad, D. M., Longmore, A. R. & Critchley, G. W., Inexpensive in-situ time-integrating seawater nutrient sampler. Water Res., 20 (1986) 1457–9.
Griepink, B., Improving the quality of environmental trace analysis. Fresenius Z. Analyt. Chem., 317 (1984) 210–12.
EPA, Handbook for Analytical Quality Control in Water and Waste Water Laboratories. EPA-600/4–79–019, Cincinnati, 1979.
Lamotte, A. & Revel, G., L’analyse élémentaire dans le domaine des traces et des ultra-traces. ler partie—Quelques problemes posés à l’analyste. Analysis, 12 (1984) 423–31.
Mart, L., Minimization of accuracy risks in voltammetric ultratrace determination of heavy metals in natural waters. Talanta, 29 (1982) 1035–40.
Frigieri, P., Ultrapurity in trace metal analysis. Int. Environ. Safety (August 1982) 36–7.
Adeloju, S. B. & Bond, A. M., Influence of laboratory environment on the precision and accuracy of trace element analysis. Analyt. Chem., 57 (1985) 1728–33.
Wilile, S. N., Sturgeon, R. E. & Berman, S. S., Determination of total chromium in seawater by graphite furnace atomic absorption spectrometry. Analyt. Chem., 55 (1983) 981–3.
Mart, L., Prevention of contamination and other accuracy risks in voltammetric trace metal analysis of natural waters. Part I: Preparatory steps, filtration and storage of water samples. Fresenius Z. Anal. Chem., 296 (1979) 350–7.
Ross, H. B., The importance of reducing sample contamination in routine monitoring of trace metals in atmospheric precipitation. Atmos. Environ., 20 (1986) 401–5.
Morley, N. H., Fay, C. W. & Statham, P. J., Design and use of a clean shipboard handling system for seawater samples. Advances in Underwater Technology, Ocean Science and Offshore Engineering, 16 (1988) 283–9.
Bruland, K. W., Knauer, G. A. & Martin, J. H., Cadmium in northeast Pacific waters. Limnol. Oceanogr., 23 (1978) 618–25.
Mart, L., Nürnberg, H. W. & Dyrssen, D., Low level determination of trace metals in Arctic sea water and snow by differential pulse anodic stripping voltammetry. In Trace Metals in Seawater, ed. C. S. Wong, E. A. Boyle, K. W. Bruland, J. D. Burton & E. D. Goldberg. Plenum Press, New York, 1983, pp. 113–30.
Statham, P. J., Burton, J. D. & Hydes, D. J., Cd and Mn in the Alboran Sea and adjacent North Atlantic: geochemical implications for the Mediterranean. Nature, 313 (1985) 565–7.
Robertson, D. E., Role of contamination in trace element analysis of sea water. Analyt. Chem., 40 (1968) 1067–72.
Moody, J. R. & Lindstrom, R. M., Selection and cleaning of plastic containers for storage of trace element samples. Analyt. Chem., 49 (1977) 2264–7.
Wong, C. S., Kremling, K., Riley, J. P., Johnson, W. K., Stukas, V., Berrang, P. G., Erickson, P., Thomas, D., Petersen, H. & Imber, B., An intercomparison of sampling devices and analytical techniques using sea water from a CEPEX enclosure. In Trace Metals in Seawater,ed. C. S. Wong, E. A. Boyle, K. W. Bruland, J. D. Burton & E. D. Goldberg. Plenum Press, New York, 1983, pp. 175–93.
Van Vleet, E. S. & Williams, P. M., Sampling sea surface films: a laboratory evaluation of techniques and collecting materials. Limnol. Oceanogr., 25 (1980) 64–77.
Laxen, D. P. H. & Harrison, R. M., Cleaning methods for polythene containers prior to the determination of trace metals in freshwater samples. Analyt. Chem., 53 (1981) 345–50.
Bloom, N. S. & Crecelius, E. A., Determination of mercury in seawater at subnanogram per liter level. Marine Chem., 14 (1983) 49–59.
Horowitz, A. J., Comparison of methods for the concentration of suspended sediment in river water for subsequent chemical analysis. Environ. Sci. Technol., 20 (1986) 155–60.
Jones, R. E., Heavy metals in the estuarine environment. Water Research Center Technical Report TR73, Medmenham, UK, 1978.
Brügmann, L., Danielsson, L. G., Magnusson, B. & Westerlund, S., Intercomparison of different methods for the determination of trace metals in seawater. Marine Chem., 13 (1983) 327–39.
Mart, L., Nurnberg, H. W. & Riltzel, H., Comparative studies on cadmium levels in the North Sea, Norwegian Sea, Barents Sea and eastern Arctic Ocean. Fresenius Z. Anal. Chem., 317 (1984) 201–9.
Flegal, A. R., Schaule, B. K. & Patterson, C. C., Stable isotopic ratios in surface waters of the central Pacific. Marine Chem., 14 (1984) 281–7.
Weisel, C. P., Duce, R. A. & Fasching, J. L., Determination of aluminium, lead and vanadium in North Atlantic seawater after coprecipitation with ferric hydroxide. Analyt. Chim., 56 (1984) 1050–2.
Mart, L., Prevention of contamination and other accuracy risks in voltammetric trace metal analysis of natural waters. Part II: Collection of surface water samples. Fresenius Z. Anal. Chem., 299 (1979) 97–102.
Scarponi, G., Capodaglio, G., Cescon, P., Cosma, B. & Frache, R., Anodic stripping voltammetric determination of the contamination of seawater samples by cadmium, lead and copper during filtration and storage. Analyt. Chem. Acta, 135 (1982) 263–76.
Mills, G. L. & Quinn, J. G., Dissolved copper and copper-organic complexes in the Narragansett Bay estuary. Marine Chem., 15 (1984) 151–72.
Batley, G. E. & Gardner, D., Sampling and storage of natural waters for trace metal analysis. Water Res., 11 (1977) 745–56.
Wallace, G. T., The association of copper, mercury and lead with surface active organic matter in coastal seawater. Marine Chem., 11 (1982) 379–94.
Hardy, J. T., Apts, C. W., Crecelius, E. S. & Fellingham, G. W., The sea-surface microlayer: fate and residence times of atmospheric metals. Limnol. Oceanogr., 30 (1985) 93–101.
Carlson, D. J., A field evaluation of plate and screen microlayer sampling techniques. Marine Chem., 11 (1982) 189–208.
Gershey, R. M., A bubble adsorption device for the isolation of surface-active organic matter in seawater. Limnol. Oceanogr., 28 (1983) 395–400.
Berman, S. S. & Yeats, P. A., Sampling of seawater for trace metals. CRC Crit. Rev. Anal. Chem., 16 (1985) 1–14.
Bewers, J. M., Dalziel, J., Yeats, P. A. & Barron, J. L., An intercalibration for trace metals in seawater. Marine Chem., 10 (1981) 173–93.
Yeats, P. A., Trace metals in seawater: sampling and storage methods. Techniques in marine environmental sciences, No. 2, ICES, Copenhagen, 1987, 8 pp.
Freimann, P., Schmidt, D. & Schomaker, K., MERCOS—a simple Teflon sampler for ultratrace metal analysis in seawater. Marine Chem., 14 (1983) 43–8.
Ranson, L. & Wilson, A. L., Determination of lead in tap water: inter-laboratory harmonization. Water Research Center Technical Report TR28, Medmenham, 1976.
Lacey, R. F. & Jolly, P. K., Sampling for household water-lead. Water Research Center Technical Report TR244, Medmenham, 1986.
Scalf, M. R., McNabb, J. F., Dunlap, W. J., Crosby, R. L. & Fryberger, J. S., Manual of Groundwater Quality Sampling Procedures. National Water Well Association and USEPA, Cincinnati, 1981,93 pp.
Lee, G. F. & Jones, R. A., Guidelines for sampling groundwater. J. Water Pollut. Control Fed., 55 (1983) 92–6.
Bryden, G. W., Mabey, W. R. & Robine, K. M., Sampling for toxic contaminants in groundwater. Ground Water Monitoring Review, 6 (1986) 67–72.
Naylor, J. A., Rowland, C. D., Young, C. P. & Barber, C., The investigation of landfill sites. Water Research Center Technical Report TR91, Medmenham, 1978.
Gibb, J. P., Schuller, R. M. & Griffin, R. A., Collection of representative water quality data from monitoring wells. In Land Disposal: Municipal Solid Waste, ed. D. W. Shultz. EPA 600/9–81–002a, Cincinnati, 1981, pp. 126–37.
Pettyjohn, W. A., Dunlap, W. J., Cosby, R. & Keeley, J. W., Sampling groundwater for organic contaminants. Ground Water, 19 (1981) 180–9.
Canter, L. W., Knox, R. C. & Fairchild, D. M., Ground Water: Quality Protection. Lewis Publishers, Inc., Chelsea, MI, 1987.
Fetter, C. W., Potential sources of contamination in ground-water monitoring. Ground Water Monitoring Review (Spring 1983) 60–4.
Barber, C. & Davis, G. B., Representative sampling of ground water from short-screened boreholes. Ground Water, 25 (1987) 581–7.
McAuliffe, C. D., Measuring hydrocarbons in water. Chem. Eng. Progr. (November 1987) 40–5.
Institute of Petroleum, Methods of Analysis and Sampling of Oil in Water. Institute of Petroleum Pub. No. IP 84–010, London, 1984,21 pp.
Gavens, A., Revitt, D. M. & Ellis, J. B., Sedimentary aliphatic hydrocarbons of an urban stormwater receiving basin. In Proc. Second Int. Conf. on Urban Storm Drainage, ed. B. C. Yen. Water Resources Publications Ltd, Littleton, Colorado, 1981, pp. 79–88.
Owens, J. W., Gladney, E. S. & Purtymun, W. D., Modification of trace element concentrations in natural waters by various field sampling techniques. Analyt. Letters, 13 (1980) 253–60.
Meranger, J. C., Subramanian, K. S. & Langford, C. H., On-site sampling with preconcentration for trace metal analysis of natural waters. Rev. Analyt. Chem., 5 (1980) 29–51.
Ellis, A. T., Leyden, D. E., Wegscheider, W., Jablonski, B. B. & Bodnar, W. B., Preconcentration methods for the determination of trace elements in water by X-ray fluorescence spectrometry. Part 1: Response characteristics. Analyt. Chim. Acta, 142 (1982) 73–87.
Otson, R., Purgeable organics in Great Lakes raw and treated water. Int. J. Environ. Anal. Chem., 31 (1987) 41–53.
Zygmunt, B., Brinkman, U. A. Th. & Frei, R. W., Preconcentration and analysis of selected organic pollutants in industrial waste water. Toxicol. Environ. Chem., 7 (1983) 1–25.
Afghan, B. K., Wilkinson, R. J., Chow, A., Findley, T. W., Gesser, H. D. & Srikameswaran, K. I., A comparative study of the concentration of polynuclear aromatic hydrocarbons by open cell polyurethane foams. Water Res., 18 (1984) 9–16.
Hunt, D. T. E., Filtration of water samples for trace metal determinations. Water Research Center Technical Report TR104, Medmenham, 1979.
Danielsson, L. G., On the use of filters for distinguishing between dissolved and particulate fractions in natural waters. Water Res., 16 (1982) 179–82.
Florence, T. M. & Batley, G. E., Chemical speciation in natural waters. CRC Crit. Rev. Anal. Chem., 9 (1980) 219–96.
Institute of Soil Fertility (Netherlands), Contribution to the standardization of the methods of analysis for heavy metals in sediments. Delft Hydraulics Laboratory Pub. No. R1578, Delft, 1981.
Chester, R., Kudoja, W. M., Thomas, A. & Tower, J., Pollution reconnaissance in stream sediments using non-residual trace metals. Environ. Pollution (Ser. B), 10 (1985) 213–38.
Readman, J. W., Mantoura, R. F. C. & Rhead, M. M., A record of polycyclic aromatic hydrocarbon (PAH) pollution obtained from accreting sediments of the Tamar estuary, UK: evidence for non-equilibrium behaviour of PAH. Sci. Total Environ., 66 (1987) 73–94.
Mawhinney, M. R. & Bisutti, C., Operating’ Manual for Common Corers and Grab Samplers. National Water Research Institute, Canada Center for Inland Waters, Burlington, Ontario, 1981.
Duursma, E. K., Problems of sediment sampling and conservation for radionuclide accumulation studies. In Sediments and Pollution in Water Ways: General Considerations. IAEA-TECDOC-302, Vienna, 1984, pp. 127–35.
Rapin, F., Tessier, A., Campbell, P. G. C. & Carignan, R., Potential artifacts in the determination of metal partitioning in sediments by a sequential extraction procedure. Environ. Sci. Technol., 20 (1986) 836–40.
DOE/NWC, The Sampling and Initial Preparation of Sewage and Waterworks’ Sludges, Soils, Sediments, Plant Materials and Contaminated Wildlife Prior to Analysis, 2nd edn. HMSO, London, 1986.
Author information
Authors and Affiliations
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 1991 Elsevier Science Publishers Ltd
About this chapter
Cite this chapter
Pio, C.A., Hall, A. (1991). Sampling Methods. In: Hewitt, C.N. (eds) Instrumental Analysis of Pollutants. Environmental Management Series. Springer, Dordrecht. https://doi.org/10.1007/978-94-011-3860-4_1
Download citation
DOI: https://doi.org/10.1007/978-94-011-3860-4_1
Publisher Name: Springer, Dordrecht
Print ISBN: 978-1-85166-548-8
Online ISBN: 978-94-011-3860-4
eBook Packages: Springer Book Archive