Abstract
The practical limitations of the high-power-decoupling/ cross-polarization/magic-angle-rotation suite of NMR techniques are discussed, with mention made of such matters as “dilution,” mobility, and physical state. Various types of information available from such solid-state NMR studies which distinguish them from solution work are listed. A number of examples of applications for 13C are reviewed, including questions of crystal symmetry, molecular conformation and motion, polymorphism, and tautomerism. Work on the silicon-29 nucleus, especially in studies of zeolites and related materials, is discussed and references given.
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Harris, R.K. (1983). High Resolution Solid-State NMR Studies of Group IV Elements. In: Lambert, J.B., Riddell, F.G. (eds) The Multinuclear Approach to NMR Spectroscopy. NATO ASI Series, vol 103. Springer, Dordrecht. https://doi.org/10.1007/978-94-009-7130-1_17
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DOI: https://doi.org/10.1007/978-94-009-7130-1_17
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