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High Resolution Multinuclear Magnetic Resonance: Instrumentation Requirements and Detection Procedures

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Book cover The Multinuclear Approach to NMR Spectroscopy

Part of the book series: NATO ASI Series ((ASIC,volume 103))

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Abstract

The entire Periodic Table is now available to NMR spectroscopists and chemists. This availability, however, hides some traps that need to be appreciated. A clear knowledge of both spectrometer capabilities and frontiers of high resolution detection will lessen the experimentalist’s burden. An examination of multinuclear instrumentation will include discussion of computer and spectrometer hardware, probeheads, traps, and hints (frequency range, receptivity, detectability, and magic pulse sequences). By way of example, applications will be discussed of exotic INEPT experiments and ruthenium NMR spectroscopy.

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References

  1. K. Lee, W. A. Anderson, “Handbook of Chemistry and Physics,” p. E 69, 55th edition, C.R.C. Press, Cleveland.

    Google Scholar 

  2. G. H. Fuller, J. Phys. Chem. Ref. Data (National Bureau of Standards, Washington), 5, 835 (1976).

    Article  Google Scholar 

  3. “NMR and the Period Table,” R. K. Harris and B. E. Mann, Eds., Academic Press, 1978.

    Google Scholar 

  4. C. Brevard and P. Granger, “Handbook of High Resolution Multinuclear NMR,” Wiley-Interscience, 1981.

    Google Scholar 

  5. P. Pregosin and H. Rüegger, in press.

    Google Scholar 

  6. C. Brown, B. T. Heaton, P. Chini, A. Fuornazalli, and G. Longoni, J. Chem. Soc. Chem. Commun., 309 (1977).

    Google Scholar 

  7. A. Abragam, “Les Principes du Magnétisme Nucléaire,” Presses Universitaires de France, 1961, p. 88.

    Google Scholar 

  8. T. C. Farrar and E. D. Becker, “Pulse and Fourier Transform NMR,” Academic, New York, 1971.

    Google Scholar 

  9. R. R. Ernst and W. A. Anderson, Rev. Sci. Inst., 37, 93 (1966).

    Article  Google Scholar 

  10. G. A. Morris and R. Freeman, J. Am. Chem. Soc., 101, 760 (1979).

    Article  Google Scholar 

  11. A. Bax, R. Freeman, and S. P. Kempsell, J. Am. Chem. Soc., 102, 4849 (1980).

    Article  Google Scholar 

  12. J. Lefebvre, F. Chauveau, P. Doppelt, and C. Brevard, J. Am. Chem. Soc., 103, 4589 (1981).

    Article  Google Scholar 

  13. P. R. Sethruaman, M. A. Leparulo, M. T. Pope, F. Zonnevijlle, C. Brevard, and J. Leraerle, J. Am. Chem. Soc., 103, 7665 (1981).

    Article  Google Scholar 

  14. E. L. Hahn, Phys. Rev., 80, 580 (1950).

    Article  MATH  Google Scholar 

  15. K. G. R. Pachler and P. L. Wessels, J. Magn. Reson., 12, 337 (1973).

    Google Scholar 

  16. E. Fukushima and S. B. W. Roder, J. Magn. Reson., 33, 199 (1979).

    Google Scholar 

  17. C. Brevard, G. C. Van Stein, and G. Van Koten, J. Am. Chem. Soc., 103, 6746 (1981); G. C. Van Stein, G. Van Koten, and C. Brevard, J. Organometal. Chem., 226, C.27 (1982); G. Van Koten, H. Van der Poel, and C. Brevard, Inorg. Chem., 21, 2878 (1982).

    Article  Google Scholar 

  18. R. Schimpf and C. Brevard, J. Magn. Reson., 47, 108 (1982).

    Google Scholar 

  19. R. W. Dykstra and A. M. Harrison, J. Magn. Reson., 45, 108 (1981).

    Google Scholar 

  20. C. Brevard and P. Granger, J. Chem. Phys., 75, 417 (1981).

    Article  Google Scholar 

  21. P. Granger and C. Brevard, Inorg. Chem., in press.

    Google Scholar 

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© 1983 D. Reidel Publishing Company

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Brevard, C. (1983). High Resolution Multinuclear Magnetic Resonance: Instrumentation Requirements and Detection Procedures. In: Lambert, J.B., Riddell, F.G. (eds) The Multinuclear Approach to NMR Spectroscopy. NATO ASI Series, vol 103. Springer, Dordrecht. https://doi.org/10.1007/978-94-009-7130-1_1

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  • DOI: https://doi.org/10.1007/978-94-009-7130-1_1

  • Publisher Name: Springer, Dordrecht

  • Print ISBN: 978-94-009-7132-5

  • Online ISBN: 978-94-009-7130-1

  • eBook Packages: Springer Book Archive

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