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Closed Loop Stripping and Cryogenic On-Column Focusing of Trihalomethanes and Related Compounds for Capillary Gas Chromatography

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Analysis of Organic Micropollutants in Water

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Summary

The activated carbon filters, commonly used for sampling and enrichment of organic volatiles in the closed loop stripping system, are thermally desorbed by inserting them into the injection port of a gas chromatograph-mass spectrometer-data system. The desorbed substances are trapped at liquid nitrogen temperature onto a “U-shaped” glass capillary, packed with Chromosorb and then transfered to the analytical column by rapid heating of the trap. Using this system, highly volatile halocarbons in drinking water were analyzed, using a glass capillary column provided with a stationary phase film thickness of 2.5 um.

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References

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Author information

Authors and Affiliations

  1. Institut de Recherches Chimiques, Administration de la recherche agronomique, Secrétariat d’état à l’agriculture Museumlaan, 5 - B198O, Tervuren, Belgium

    M. Termonia, J. Walravens, P. Dourte & X. Monseur

Authors
  1. M. Termonia
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  2. J. Walravens
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  3. P. Dourte
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  4. X. Monseur
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Editor information

Editors and Affiliations

  1. Commission of the European Communities, Brussels, Belgium

    G. Angeletti (Directorate-General for Science) (Directorate-General for Science)

  2. Central Institute for Industrial Research, Oslo, Norway

    A. Bjørseth

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© 1984 ECSC, EEC, EAEC, Brussels and Luxembourg

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Termonia, M., Walravens, J., Dourte, P., Monseur, X. (1984). Closed Loop Stripping and Cryogenic On-Column Focusing of Trihalomethanes and Related Compounds for Capillary Gas Chromatography. In: Angeletti, G., Bjørseth, A. (eds) Analysis of Organic Micropollutants in Water. Springer, Dordrecht. https://doi.org/10.1007/978-94-009-6345-0_18

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  • DOI: https://doi.org/10.1007/978-94-009-6345-0_18

  • Publisher Name: Springer, Dordrecht

  • Print ISBN: 978-94-009-6347-4

  • Online ISBN: 978-94-009-6345-0

  • eBook Packages: Springer Book Archive

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