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Experimental Techniques

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Mössbauer Spectroscopy

Abstract

In this chapter we shall consider the various techniques which have been used for observation of the Mössbauer effect, together with methods of source and absorber preparation and computer techniques for data analysis. Some of the advantages and limitations of Mössbauer spectroscopy will become apparent during the discussion of these problems. References to more recent development will be found in the review by J. R. De Voe and J. J. Spijkerman in Analytical Chemistry, 1970, 42, 366R, and in ‘Spectroscopic Properties of Inorganic and Organometallic Compounds’ published annually by the Chemical Society (London).

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References

  1. R. L. Mössbauer, Z. Physik, 1958, 151, 124.

    Article  Google Scholar 

  2. R. L. Mössbauer, Naturwiss., 1958, 45, 538.

    Article  Google Scholar 

  3. K. Cassell and A. H. Jiggins, J. Sci. Instr., 1967, 44, 212.

    Article  Google Scholar 

  4. R. Booth and C. E. Violet, Nuclear Instr. Methods, 1963, 25, 1.

    Article  Google Scholar 

  5. C. E. Johnson, W. Marshall, and G. J. Perlow, Phys. Rev., 1962, 126, 1503.

    Article  Google Scholar 

  6. C. W. Kocher, Rev. Sci. Instr., 1965, 36, 1018.

    Article  Google Scholar 

  7. A. J. Bearden, M. G. Hauser, and P. L. Mattern, ‘Mössbauer Effect Methodology Vol. 1’, Ed. I. J. Gruverman, Plenum Press, N.Y., 1965, p. 67.

    Google Scholar 

  8. H. M. Kappler, A. Trautwein, A. Mayer, and H. Vogel, Nuclear Instr. Methods, 1967, 53, 157.

    Article  Google Scholar 

  9. P. A. Flinn, Rev. Sci. Instr., 1963, 34, 1422.

    Article  Google Scholar 

  10. P. Flinn, ‘Mössbauer Effect Methodology Vol. 1’, Ed. I. J. Gruverman, Plenum Press, N.Y., 1965, p. 75.

    Google Scholar 

  11. J. Lipkin, B. Schechter, S. Shtrikman, and D. Treves, Rev. Sci. Instr., 1964, 35, 1336.

    Article  Google Scholar 

  12. F. W. D. Woodhams, J. Sci. Instr., 1967, 44, 285.

    Article  Google Scholar 

  13. V. P. Alfimenkov, Yu. M. Ostanevich, T. Ruskov, A. V. Strelkov, F. L. Shapiro, and W. K. Yen, Soviet Physics—J.E.T.P., 1962, 15, 713 (Zhur. eksp. teor. Fiz., 1962, 42, 1029).

    Google Scholar 

  14. R. C. Knauer and J. G. Mullen, Rev. Sci. Instr., 1967, 38, 1624.

    Article  Google Scholar 

  15. P. E. Clark, A. W. Nichol, and J. S. Carlow, J. Sci. Instr., 1967, 44, 1001.

    Article  Google Scholar 

  16. J. Pahor, D. Kelsin, A. Kodre, D. Hanzel, and A. Moljk, Nuclear Instr. Methods, 1967, 46, 289.

    Article  Google Scholar 

  17. Y. Hazony, Rev. Sci. Instr., 1967, 38, 1760.

    Article  Google Scholar 

  18. D. St P. Bunbury, J. Sci. Instr., 1966, 43, 783.

    Article  Google Scholar 

  19. R. Zane, Nuclear Instr. Methods, 1966, 43, 333.

    Google Scholar 

  20. D. Rubin, Rev. Sci. Instr., 1962, 33, 1358.

    Article  Google Scholar 

  21. R. L. Cohen, Rev. Sci. Instr., 1966, 37, 957.

    Article  Google Scholar 

  22. R. L. Cohen, P. G. McMullin, and G. K. Wertheim, Rev. Sci. Instr., 1963,34, 671.

    Article  Google Scholar 

  23. V. Vali and T. W. Nybakken, Rev. Sci. Instr., 1964, 35, 1085.

    Article  Google Scholar 

  24. R. Gerson and W. S. Denno, Rev. Sci. Instr., 1965, 36, 1344.

    Article  Google Scholar 

  25. L. Lovborg, Nuclear Instr. Methods, 1965, 34, 307.

    Article  Google Scholar 

  26. M. Bornaz, G. Filoti, A. Gelberg, V. Grabari, and C. Nistor, Nuclear Instr. Methods, 1966, 40, 61.

    Article  Google Scholar 

  27. J. D. Cooper, T. C. Gibb, N. N. Greenwood, and R, V. Parish, Trans. Faraday Soc., 1964, 60, 2097.

    Article  Google Scholar 

  28. J. D. Cooper and N. N. Greenwood, J. Sci. Instr., 1966, 43, 71.

    Article  Google Scholar 

  29. C. A. Miller and J. H. Broadhurst, Nuclear Instr. Methods, 1965, 36, 283.

    Article  Google Scholar 

  30. T. E. Cranshaw, Nuclear Instr. Methods, 1964, 30, 101.

    Article  Google Scholar 

  31. F. C. Ruegg, J. J. Spijkerman, and J. R. de Voe, Rev. Sci. Instr., 1965, 36, 356.

    Article  Google Scholar 

  32. E. Kankeleit, Rev. Sci. Instr., 1964, 35, 194.

    Article  Google Scholar 

  33. Y. Reggev, S. Bukshpan, M. Pasternak, and D. A. Segal, Nuclear Instr. Methods, 1967, 52, 193.

    Article  Google Scholar 

  34. E. Nadav and M. Palmai, Nuclear Instr. Methods, 1967, 56, 165.

    Article  Google Scholar 

  35. M. Michalski, J. Piekoszewskii, and A. Sawicki, Nuclear Instr. Methods, 1967, 48, 349.

    Article  Google Scholar 

  36. R. H. Goodman and J. E. Richardson, Rev. Sci. Instr., 1966, 37, 283.

    Article  Google Scholar 

  37. R. H. Goodman, ‘Mössbauer Effect Methodology Vol. 3’, Ed. I. J. Gruverman, Plenum Press, N.Y., 1967, p. 163.

    Google Scholar 

  38. J. E. S. Bradley and J. Marks, Nature, 1961, 192, 1176.

    Article  Google Scholar 

  39. T. Bressani, P. Brovetto, and E. Chiavassa, Phys. Letters, 1966, 21, 299; Nuclear Instr. Methods, 1967, 47, 164.

    Article  Google Scholar 

  40. H. Frauenfelder, ‘The Mössbauer Effect’, W. A. Benjamin, Inc., N.Y., 1962.

    Google Scholar 

  41. A. J. F. Boyle and H. E. Hall, Repts. Progr. in Physics, 1962, 25, 441.

    Article  Google Scholar 

  42. J. K. Major, ‘Mössbauer Effect Methodology Vol. 1’, Ed. I. J. Gruverman, Plenum Press, N.Y., 1965, p. 89.

    Google Scholar 

  43. P. Debrunner, ‘Mössbauer Effect Methodology Vol. 1’, Ed. I. J. Gruverman, Plenum Press, N.Y., 1965, p. 97.

    Google Scholar 

  44. R. Barloutaud, J-L. Picou, and C. Tzara, Compt. rend., 1960, 250, 2705.

    Google Scholar 

  45. P. J. Black, D. E. Evans, and D. A. O’Connor, Proc. Roy. Soc., 1962, A270, 168.

    Google Scholar 

  46. P. J. Black, G. Longworth, and D. A. O’Connor, Proc. Phys. Soc., 1964, 83, 925.

    Article  Google Scholar 

  47. C. M. Lederer, J. M. Hollander, and I. Perlman, ‘Table of Isotopes — 6th Ed.’, John Wiley & Sons, Inc., N.Y., 1967.

    Google Scholar 

  48. G. A. Chackett, K. F. Chackett, and B. Singh, J. Inorg. Nuclear Chem., 1960, 14, 138.

    Article  Google Scholar 

  49. S. L. Ruby and J. M. Hicks, Rev. Sci. Instr., 1962, 33, 27.

    Article  Google Scholar 

  50. D. A. O’Connor, Nuclear Instr. Methods., 1963, 21, 318.

    Article  Google Scholar 

  51. S. Margulies and J. R. Ehrman, Nuclear Instr. Methods, 1961, 12, 131.

    Article  Google Scholar 

  52. S. Margulies, P. Debrunner, and H. Frauenfelder, Nuclear Instr. Methods, 1963, 21, 217.

    Article  Google Scholar 

  53. J. D. Bowman, E. Kankeleit, E. N. Kaufmann, and B. Persson, Nuclear Instr. Methods, 1967, 50, 13.

    Article  Google Scholar 

  54. K. Siegbahn (Ed.), ‘Alpha, Beta, and Gamma Ray Spectroscopy’, North Holland Publ., Amsterdam, 1965.

    Google Scholar 

  55. N. Benczer-Koller and R. H. Herber, Chap. 2, ‘Experimental Methods’ in V. I. Goldanskii and R. H. Herber (Eds.), ‘Chemical Applications of Mössbauer Spectroscopy’, Academic Press, New York, 1968.

    Google Scholar 

  56. C. E. Violet, ‘The Mössbauer Effect and its Appl. to Chem.’, Adv. Chem. Ser., 1967, 68, Chap. 10.

    Google Scholar 

  57. L. Levy, L. Mitrani, and S. Ormandjiev, Nuclear Instr. Methods, 1964, 31, 233.

    Article  Google Scholar 

  58. K. P. Mitrofanov and V. S. Shpinel, Zhur. eksp. teor. Fiz., 1961, 40, 983.

    Google Scholar 

  59. D. A. O’Connor, N. M. Butt, and A. S. Chohan, Rev. Mod. Phys., 1964, 36, A 361.

    Google Scholar 

  60. K. P. Mitrofanov, N. V. Illarionova, and V. S. Shpinel, Pribory i Tekhn. Eksperim., 1963, 8, 49; English Transl. in Instr. Exptl. Tech. USSR, 1963, 3, 415.

    Google Scholar 

  61. J. S. Eck, N. Hershkowitz, and J. C. Walker, Bull Am, Phys. Soc., 1965, 10, 577.

    Google Scholar 

  62. H. Frauenfelder, D. R. F. Cochran, D. E. Nagle, and R. D. Taylor, Nuovo Cimento, 1961, 19, 183.

    Article  Google Scholar 

  63. N. Hershkowitz and J. C. Walker, Nuclear Instr. Methods, 1967, 53, 273.

    Article  Google Scholar 

  64. E. Kankeleit, Z. Physik, 1961, 164, 442.

    Article  Google Scholar 

  65. M. Kalvius, ‘Mössbauer Effect Methodology Vol. 1’, Ed. I. J. Gruverman, Plenum Press, N.Y., 1965, p. 163.

    Google Scholar 

  66. D. P. Johnson, G. A. Erickson, and J. G. Dash, Rev. Sci. Instr., 1968, 39, 420.

    Article  Google Scholar 

  67. A. J. Nozik and M. Kaplan, Anal. Chem., 1967, 39, 854.

    Article  Google Scholar 

  68. F. Van der Woude and G. Boom, Rev. Sci. Instr., 1965, 36, 800.

    Article  Google Scholar 

  69. B. Sharon and D. Treves, Rev. Sci. Instr., 1966, 37, 1252.

    Article  Google Scholar 

  70. D. E. Nagle, H. Frauenfelder, R. D. Taylor, D. R. F. Cochran, and B. T. Matthias, Phys. Rev. Letters, 1960, 5, 364.

    Article  Google Scholar 

  71. R. S. Preston, S. S. Hanna, and J. Heberle, Phys. Rev., 1962, 128, 2207.

    Article  Google Scholar 

  72. R. G. Barnes, R. L. Mössbauer, E. Kankeleit, and J. M. Poindexter, Phys. Rev., 1964, 136, A 175.

    Google Scholar 

  73. R. Ingalls, ‘Mössbauer Effect Methodology Vol. 1’, Ed. I. J. Gruverman, Plenum Press, N.Y., 1965, p. 185.

    Google Scholar 

  74. D. Pipkorn, C. K. Edge, P. Debrunner, G. de Pasquali, H. G. Drickamer, and H. Frauenfelder, Phys. Rev., 1964, 135, A 1604.

    Article  Google Scholar 

  75. P. Debrunner, R. W. Vaughan, A. R. Champion, J. Cohen, J. A. Moyzis, and H. G. Drickamer, Rev. Sci. Instr., 1966, 37, 1310.

    Article  Google Scholar 

  76. J. Heberle, ‘Mössbauer Effect Methodology Vol. 2’ Ed. I. J. Gruverman, Plenum Press, N.Y., 1966, p. 95.

    Google Scholar 

  77. H. de Waard, Rev. Sci. Instr., 1965, 36, 1728.

    Article  Google Scholar 

  78. J. J. Spijkerman, F. C. Ruegg, and J. R. De Voe, International Atomic Energy Agency Technical Reports Series No. 50, Vienna, 1966, p. 53.

    Google Scholar 

  79. T. E. Cranshaw and P. Reivari, Proc. Phys. Soc., 1967, 90, 1059.

    Article  Google Scholar 

  80. B. J. Duke and T. C. Gibb, J. Chem. Soc. (A), 1967, 1478.

    Google Scholar 

  81. S. W. Marshall, J. A. Nelson, and R. M. Wilenzick, Comm. Assoc. Computing Machinery, 1965, 8, 313.

    Google Scholar 

  82. G. M. Bancroft, A. G. Maddock, W. K. Ong, R. H. Prince, and A. J. Stone, J. Chem. Soc. (A), 1967, 1966.

    Google Scholar 

  83. D. B. Owen, ‘Handbook of Statistical Tables’, Pergamon Press, 1962.

    Google Scholar 

  84. A. Gavron, D. Kedem, and T. Rothem, Nuclear Instr. Methods, 1968, 61, 213.

    Article  Google Scholar 

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© 1971 T. C. Gibb and N. N. Greenwood

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Greenwood, N.N., Gibb, T.C. (1971). Experimental Techniques. In: Mössbauer Spectroscopy. Springer, Dordrecht. https://doi.org/10.1007/978-94-009-5697-1_2

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  • DOI: https://doi.org/10.1007/978-94-009-5697-1_2

  • Publisher Name: Springer, Dordrecht

  • Print ISBN: 978-94-009-5699-5

  • Online ISBN: 978-94-009-5697-1

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