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Real-Time Neutron Powder Diffraction

  • Chapter
Chemical Crystallography with Pulsed Neutrons and Synchroton X-rays

Part of the book series: NATO ASI Series ((ASIC,volume 221))

Abstract

The use of a high-flux neutron source together with large curved one-dimensional position sensitive detectors (PSD’s) allows a complete powder diffraction pattem to be recorded simultaneously on a time scale of a few minutes or less so that transient phenomena such as chemical reactions in the solid state or first-order phase transitions can now be studied in real-time. Such measurements provide direct information on the progress of a reaction (kinetic law), but may also shed light on the transformations of structure and/or morphology which occur in the reactants during the course of a reaction. The instrumental parameters relevant to the design of time-dependent experiments are discussed. The applications are illustrated by four kinds of experiments: kinetic studies, thermodiffractometry, texture and stroboscopic measurements.

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Author information

Authors and Affiliations

  1. Institut Laue Langevin, 156X 38042, Grenoble, France

    J. Pannetier

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  1. J. Pannetier
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Editor information

Editors and Affiliations

  1. Centro de Quimica Estrutural, Instituto Superior Técnico, Lisboa, Portugal

    Maria Arménia Carrondo

  2. Department of Crystallography, University of Pittsburgh, Pennsylvania, USA

    George A. Jeffrey

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© 1988 D. Reidel Publishing Company

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Pannetier, J. (1988). Real-Time Neutron Powder Diffraction. In: Carrondo, M.A., Jeffrey, G.A. (eds) Chemical Crystallography with Pulsed Neutrons and Synchroton X-rays. NATO ASI Series, vol 221. Springer, Dordrecht. https://doi.org/10.1007/978-94-009-4027-7_14

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  • DOI: https://doi.org/10.1007/978-94-009-4027-7_14

  • Publisher Name: Springer, Dordrecht

  • Print ISBN: 978-94-010-8287-7

  • Online ISBN: 978-94-009-4027-7

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