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Hydrothermal Preparation and Sintering of Fine Ceramic Powders

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Hydrothermal Reactions for Materials Science and Engineering

Abstract

Hydrothermal preparation is one of the methods to.make fine ceramic powders. There are: (1) hydrothermal oxidation, (2) hydrothermal precipitation, (3) hydrothermal synthesis, (4) hydrothermal decomposition, (5) hydrothermal crystallization, etc. Starting materials for hydrothermal oxidation is mainly metal. Reaction between metal and high temperature-high pressure solution occurs to form oxide. Therefore, starting materials for very fine powders are: (1) metal powders or chips, (2) gel, solutions, etc., (3) — oxides and solutions, (4) solids, and (5) hydrous material. This paper describes hydrothermal crystallization and oxidation. Fine powders of ZrO2, Al2O3, HfO2, and Al2O3–ZrO2 are described.

Sintered bodies are also able to get under hydrothermal conditions with reactions. Hydrothermal reaction sintered bodies of iron oxides, Cr 2 O 3, ZrO 2 and HfO 2 were obtained under 100 MPa above 1000°C with 1–5 µm grains.

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Authors and Affiliations

  1. Laboratory for Hydrothermal Syntheses, Research Laboratory of Engineering Materials, Tokyo Institute of Technology, 4259 Nagatsuta, Midori, Yokohama, 227, Japan

    Shigeyuki Sōmiya

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  1. Shigeyuki Sōmiya
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Editors and Affiliations

  1. The Nishi-Tokyo University, Japan

    Shigeyuki Sōmiya

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© 1989 Elsevier Science Publishers LTD

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Sōmiya, S. (1989). Hydrothermal Preparation and Sintering of Fine Ceramic Powders. In: Sōmiya, S. (eds) Hydrothermal Reactions for Materials Science and Engineering. Springer, Dordrecht. https://doi.org/10.1007/978-94-009-0743-0_8

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  • DOI: https://doi.org/10.1007/978-94-009-0743-0_8

  • Publisher Name: Springer, Dordrecht

  • Print ISBN: 978-94-010-6819-2

  • Online ISBN: 978-94-009-0743-0

  • eBook Packages: Springer Book Archive

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