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A New Method in Preparation of Monodisperse Particles

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Part of the book series: NATO ASI Series ((ASHT,volume 12))

Abstract

It seems needless to say that monodispersed particles perfectly controlled in size, shape and internal structure are the ultimate goals of general advanced materials such as electromagnetic devices, modern ceramics, catalysts, photosensitive materials, medicines, pigments, cosmetics, etc., since the properties of these materials decisively depend on their size, shape and structure. However, when we try to produce monodispersed particles as ideal materials on industrial scale, we have to be confronted with essential problems of their exceedingly low productivity or high costs, because most of them have been prepared in extremely dilute systems (mostly of the order of 10-3 – 10-2 mole dm-3) to avoid the tremendous coagulation or need costly metal alkoxides as starting materials. In addition, when we employ the sol-gel process for the preparation of amorphous metal oxides starting from metal alkoxides, we usually suffer from a problem of its rather poor reproducibility. Still more difficult issue is the perfect control of their mean size, shape and internal structure, and it is hardly achieved in most monodispersed systems. Thus, it has appeared almost impossible in principle to realize the dream of producing monodispersed particles from ordinary metal salts in highly condensed systems, not to mention the precise control of the above properties.

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References

  1. Sugimoto, T. and Sakata, K. (1992) Preparation of monodisperse pseudocubic α- Fe2O3 particles from condensed ferric hydroxide gel, J. Colloid Interface Sci. 152, 587–590.

    Article  CAS  Google Scholar 

  2. Sugimoto, T., Sakata, K., and Muramatsu, A. (1993) Formation mechanism of monodisperse pseudocubic α- Fe2O3 particles from condensed ferric hydroxide gel, J. Colloid Interface Sci. 159, 372–382.

    Article  CAS  Google Scholar 

  3. Sugimoto, T., Khan, M. M., and Muramatsu, A. (1993) Preparation of monodisperse peanut-type α- Fe2O3 particles from condensed ferric hydroxide gel, Colloids Surf. A 70, 167–169.

    Article  CAS  Google Scholar 

  4. Sugimoto, T., Khan, M. M., Muramatsu, A., and Itoh, H. (1993) Formation mechanism of monodisperse peanut-type α- Fe2O3 particles from condensed ferric hydroxide gel, Colloids Surf. A 79, 233–247.

    Article  CAS  Google Scholar 

  5. Sugimoto, T. (1987) Preparation of monodispersed colloidal particles, Adv. Colloid Interface Sci. 28, 65–108.

    Article  CAS  Google Scholar 

  6. Itoh, H., Mochida, T., and Sugimoto, T. (1992) Formation mechanism of monodisperse ellipsoidal hematite particles by gel-sol method, Proc. 64th Annual Meeting Chem. Soc. Japan, Niigata, vol. 1, pp. 110.

    Google Scholar 

  7. Itoh, H., Mochida, T., and Sugimoto, T. (1993) Effect of added organic compounds on the morphology of hematite colloid prepared by gel-sol method, Proc. 65th Annual Meeting Chem. Soc. Japan, Tokyo, vol. 1, pp. 305.

    Google Scholar 

  8. Sugimoto, T., Muramatsu, A., Sakata, K., and Shindo, D. (1993) Characterization of hematite particles of different shapes, J. Colloid Interface Sci. 158, 420–428.

    Article  CAS  Google Scholar 

  9. Sugimoto, T., Waki, S., and Itoh, H. (1995) Preparation of monodisperse platelet-type hematite particles by gel-sol method, Proc. 69th Annual Meeting Chem. Soc. Japan, Kyoto, I, pp. 254.

    Google Scholar 

  10. Sugimoto, T., Ndei, M. K., and Itoh, H. (1993) Shape and structure control of monodisperse ellipsoidal α- Fe2O3 particles by gel-sol method, Proc. 65th Annual Meeting Chem. Soc. Japan, Tokyo, vol. 1, pp. 305.

    Google Scholar 

  11. Sugimoto, T., Sakata, K., and Itoh, H. (1993) Shape and structure control of monodisperse spindle-type hematite particles by gel-sol method, Proc. 46th Symp. Colloid Interface Chem., Tokyo, pp. 306–307.

    Google Scholar 

  12. Shindo, D., Aita, S., Park, G., and Sugimoto, T. (1993) High-voltage high-resolution electron microscopy of monodispersed pseudocubic and peanut-type hematite particles, Mater. Trans., JIM 34, 1226–1228.

    CAS  Google Scholar 

  13. Shindo, D., Park, G., Waseda, Y., and Sugimoto, T. (1994) Internal structure analysis of monodispersed peanut-type hematite particles produced by the gel-sol method, J. Colloid Interface Sci. 168, 478–484.

    Article  CAS  Google Scholar 

  14. Shindo, D., Park, G., Waseda, Y., and Sugimoto, T. (1994) Internal structure analysis of monodispersed peanut-type hematite particles produced by the gel-sol method, J. Colloid Interface Sci. 168, 478–484.

    Article  CAS  Google Scholar 

  15. Sugimoto, T. and Sakata, K. (1994) Shape and internal structure control of monodispersed hematite particles by gel-sol method, Proc. 47th Symp. Colloid Interface Chen., Okayama, pp. 240–241.

    Google Scholar 

  16. Shindo, D., Lee, B., Waseda, Y., Muramatsu, A., and Sugimoto, T. (1993) Crystallography of platelet-type hematite particles by electron microscopy, Mater. Trans, JIM 34, 580–585.

    CAS  Google Scholar 

  17. Sugimoto, T., Dirige, E. G., and Muramatsu, A. (1994) Synthesis of uniform cadmium sulfide (CdS) particles from a condensed cadmium hydroxide suspension, Proc. 47th Symp. Colloid Interface Chem., Okayama, pp. 236–237.

    Google Scholar 

  18. Sugimoto, T, Dirige, E. G., and Muramatsu, A. (in press) Synthesis of uniform CdS particles from condensed Cd(OH) 2 suspension, J. Colloid Interface Sci.

    Google Scholar 

  19. Sugimoto, T, Dirige, E. G., and Muramatsu, A. (in press) Formation mechanism of uniform CdS particles from condensed Cd(OH) 2 suspension, J. Colloid Interface Sci.

    Google Scholar 

  20. Muramatsu, A. and Sugimoto, T. (1994) New synthetic method of spherical uniform Cu2O particles with highly condensed CuO sol as a source of Cu, Proc. 47th Symp. Colloid Interface Chem., Okayama, pp. 238–239.

    Google Scholar 

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© 1996 Kluwer Academic Publishers

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Sugimoto, T. (1996). A New Method in Preparation of Monodisperse Particles. In: Pelizzetti, E. (eds) Fine Particles Science and Technology. NATO ASI Series, vol 12. Springer, Dordrecht. https://doi.org/10.1007/978-94-009-0259-6_5

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  • DOI: https://doi.org/10.1007/978-94-009-0259-6_5

  • Publisher Name: Springer, Dordrecht

  • Print ISBN: 978-0-7923-4047-8

  • Online ISBN: 978-94-009-0259-6

  • eBook Packages: Springer Book Archive

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