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Sealing of Surface Micromachined Poly-SiGe Cavities

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Poly-SiGe for MEMS-above-CMOS Sensors

Part of the book series: Springer Series in Advanced Microelectronics ((MICROELECTR.,volume 44))

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Abstract

This chapter describes the sealing of polycrystalline SiGe (poly-SiGe) surface micromachined cavities for above-CMOS pressure sensor applications. Two different sealing techniques involving thin-film deposition are investigated: direct sealing and sealing by using an intermediate porous layer. The sealing materials studied include Si-oxide and aluminum. Both \(\mu \)c-SiGe and SiC are evaluated as porous layer. The maximum processing temperature is kept below \(460\,{^\circ }\)C to allow for the post-processing on top of standard CMOS. Section 5.1 gives a short overview about the most common sealing methods for pressure sensors and lists the main requirements the sealing layer needs to fulfill. Section 5.2 explains the fabrication process of the test structures. The measurement set up used to characterize the deflection of the sealed membranes deflection under different applied loads is introduced in Sect. 5.3. In Sect. 5.4 the theoretical analysis of the load-deflection behavior of square membranes is introduced, and with the help of finite element simulations a model adapted to our test structures is developed. Section 5.5 gives the results of the short- and long-term hermeticity tests performed on the sealed membranes. This section also describes the use of micro-venting holes drilled using Focus Ion Beam (FIB) in some of the sealed membranes to study the behavior of the diaphragms under 0-pressure-difference. This chapter ends with a conclusion (Sect. 5.6) listing the main aspects of the different sealing techniques studied and the reasons behind the selection of SACVD (Sub-Atmospheric Chemical Vapor Deposition) oxide as sealing layer for our pressure sensor.

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References

  1. K. Petersen, P.W. Barth, J. Poydock, J. Brown, J. Mallon, J. Bryaek, Silicon fusion bonding for pressure sensors, in Proceeding of the IEEE Solid-State Sensor and Actuator Workshop, Freemont (CA), 6–9 June 1988, pp. 144–147

    Google Scholar 

  2. H. Guckel, D.W. Burns, Planar processed polysilicon sealed cavities for pressure transducer arrays, in Proceeding of IEDM, 1984, pp. 223–225

    Google Scholar 

  3. C.H. Mastrangelo, R.S. Muller, S. Kumar, Microfabricated incandescent lamps. Appl. Opt. 30, 868–873 (1993)

    Article  ADS  Google Scholar 

  4. L. Lin, R.T. Howe, A.P. Pisano, Microelectromechanical filters for signal processing. J. Microelectromech. Syst. 7, 286–294 (1998)

    Article  Google Scholar 

  5. C. Liu, Y. Tai, Sealing of micromachined cavities using chemical vapor deposition methods: characterization and optimization. J. Microelectromech. Syst. 8, 135–145 (1999)

    Article  Google Scholar 

  6. M. Bartek, J.A. Foerster, R.F. Wolffenbuttel, Vacuum sealing of microcavities using metal evaporation. Sens. Actuators A , 61, 364–368 (1997)

    Google Scholar 

  7. B. Guo, L. Wen, P. Helin, G. Claes, A. Verbist, R. Van Hoof, B. Du Bois, J. De Coster, I. De Wolf, A. Hadi Shahar, Y. Li, H. Cui, M. Lux, G. Vereecke, H.A.C. Tilmans, L. Haspeslagh, S. Decoutere, H. Osman, R. Puers, S. Severi, A. Witvrouw, Above-IC generic poly-SiGe thin film wafer level packaging and MEM device technology: application to accelerometers, in Proceeding og the IEEE 24th International Conference on Micro Electro Mechanical Systems (MEMS), Mexico, 23–27 Jan 2011, p. 355

    Google Scholar 

  8. Y. Naito, P. Helin, K. Nakamura, J. De Coster, B. Guo, L. Haspeslagh, K. Onishi, H. A. C. Tilmans, High-Q torsional mode si triangular beam resonators encapsulated using SiGe thin film, 2010 IEEE International Electron Device Meeting (IEDM), pp. 7.1.1–7.1.4

    Google Scholar 

  9. M. Gromova, K. Baert, C. Van Hoof, A. Mehta, A. Witvrouw, The novel Use of low temperature hydrogenated microcrystalline silicon germanium (\(\upmu \)cSiGe:H) for MEMS applications. Microelectron. Eng. 76(1–4), 266–271 (2004)

    Google Scholar 

  10. G. Bryce, S. Severi, R. van Hoof, B. Guo, E. Kunnen, A. Witvrouw, S. Decoutere, Development, optimization and evaluation of a CF4 pre-treatment process to remove unwanted interfacial layers in stacks of CVD and PECVD polycrystalline Silicon-Germanium for MEMS applications. ECS Trans. 28, 79–90 (2010)

    Article  Google Scholar 

  11. G. Claes, Poly-silicon germanium thin-film package: study of structural features enabling CMOS-MEMS integration, Ph. D. thesis, Katholieke Universiteit Leuven, July, 2011

    Google Scholar 

  12. G.G. Stoney, The tension of thin metallic films deposited by electrolysis. Proc. Roy. Soc. Lond. A 82, 172–175 (1909)

    Article  ADS  Google Scholar 

  13. R. Arghavani, Z. Yuan, N. Ingle, K-B Jung, M. Seamons, S. Venkataraman, V. Banthia, K. Lilja, P. Leon, G. Karunasiri, S. Yoon, and A. Mascarenhas, Stress management in Sub-90-nm transistor architecture. IEEE Trans. Electr. Devices, 51(10), 1740–1743 (2004)

    Google Scholar 

  14. A. Witvrouw, J. Proost, B. Deweerdt, Ph Roussel, K. Maex, Stress relaxation in Al-Si-Cu thin films and lines. Mat. Res. Soc. Symp. Proc. 356, 441–446 (1995)

    Article  Google Scholar 

  15. I. de Wolf, J. de Coster, O. Varela Pedreira, L. Haspeslagh, A. Witvrouw, Wafer level characterization and failure analysis of microsensors. Proc. IEEE Sens. 26–29, 144–147 (Oct. 2009)

    Google Scholar 

  16. O. Varela Pedreira, T. Lauwagie, J. de Coster, L. Haspeslagh, A. Witvrouw, I. de Wolf, High throughput measurement techniques for wafer level yield inspection of MEMS devices, in Proceeding of the SPIE 9th International Symposium LM, vol. 7155 715 50M-1–11, 2008

    Google Scholar 

  17. M. Zecchino, Characterazing MEMS devices through transparent media (2010), http://www.bruker-axs.com/

  18. O. Tabata, K. Kawahata, S. Sugiyama, I. Igarashi, Mechanical property measurements of thin films using load-deflection of composite rectangular membrane, in Proceeding of the MEMS 1989, pp. 152–156

    Google Scholar 

  19. M.G. Allen, M. Mehregany, R.T. Howe, S.D. Senturia, Microfabricated structures for the in situ measurement of residual stress, young’s modulus and ultimate strain of thin films. Appl. Phys. Lett. 51, 241–243 (1987)

    Article  ADS  Google Scholar 

  20. S.D. Senturia, Microsystems Design (Kluwer Academic Publisher, Norwell, 2000)

    Google Scholar 

  21. D. Maier-Schneider, J. Maibach, E. Obermeier, A new analytical solution for the load-deflection of square membranes. J. Microelectromech. Syst. 4, 238–241 (1995)

    Article  Google Scholar 

  22. D. Maier-Schneider, A. Köprülülü, S. Ballhausen Holm, E. Obermeier, Elastic properties and microstructure of LPCVD polysilicon films. J. Micromech. Microeng. 6, 436–446 (1996)

    Google Scholar 

  23. COMSOL multiphysics, www.comsol.com

  24. A. Partridge, A. E. Rice, T.W. Kenny, New thin film epitaxial polysilicon encapsulation for piezoresistive accelerometers, in Proceeding of the IEEE 14th International Conference on Micro Electro Mechanical Systems (MEMS), pp. 54–59, 2001

    Google Scholar 

  25. T. Kramer, O. Paul”, Postbuckled micromachined square membranes under differential pressure. J. Micromech. Microeng. 12, 475–478 (2002)

    Article  ADS  Google Scholar 

  26. X. Li, B. Bhushan, A review of nanoindentation continuous stiffness measurement technique and its applications. Mater. Character. 48, 11–36 (2002)

    Article  Google Scholar 

  27. M.A. Huff, A.D. Nikolich, M.A. Schmidt, Design of sealed cavity microstructures formed by silicon wafer bonding. J. Microelectromech. Syst. 2, 74–81 (1993)

    Article  Google Scholar 

  28. V. Ziebart, O. Paul, H. Baltes, Strongly buckled square micromachined membranes. J. Microelectromech. Syst. 4, 423–32 (1999)

    Article  Google Scholar 

  29. K. Fujino, Y. Nishimoto, N. Tokumasu, K. Maeda, Silicon dioxide deposition by atmospheric pressure and low-temperature CVD Using TEOS and Ozone. J. Electrochem. Soc. 137, 2883–2887 (1990)

    Article  Google Scholar 

  30. R. Legtenberg, H.A.C. Tilmans, Electrostatically driven vacuum-encapsulated polysilicon resonators Part I. Design and fabrication. Sens. Actuators A 45, 57–66 (1994)

    Article  Google Scholar 

  31. J.A. Voorthuyzen, K. Keskin, P. Bergveld, Investigations of the surface conductivity of silicon dioxide and methods to reduce it. Surf. Sci. 187, 201–211 (1987)

    Article  ADS  Google Scholar 

  32. B. Wang, S. Tanaka, B. Guo B, G. Vereecke, S. Severi, A. Witvrouw, M. Wevers, I. De Wolf, Outgassing studies of thin-films used for poly-SiGe based vacuum packaging of MEMS. Microelectron. Reliab. 51(9–11), 1878–1881 (2011)

    Google Scholar 

  33. Q. Li, H. Goosen, F. van Keulen, J. van Beek, G. Zhang, Assessment of testing methodologies for thin-film vacuum MEMS packages. Microsyst. Technol. 15, 161–168 (2009)

    Article  Google Scholar 

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Correspondence to Pilar González Ruiz .

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Ruiz, P.G., Meyer, K.D., Witvrouw, A. (2014). Sealing of Surface Micromachined Poly-SiGe Cavities. In: Poly-SiGe for MEMS-above-CMOS Sensors. Springer Series in Advanced Microelectronics, vol 44. Springer, Dordrecht. https://doi.org/10.1007/978-94-007-6799-7_5

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  • DOI: https://doi.org/10.1007/978-94-007-6799-7_5

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