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Texture – An Overview

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Uniting Electron Crystallography and Powder Diffraction

Abstract

Samples that are polycrystalline solids produced by some mechanical process frequently possess a non-random orientation of the crystallites due to deformation of the material during the forming operation. The resulting crystallite orientations (“texture”) can be more complex that those obtained from simple packing of powders. In the course of crystal structure analysis from powder diffraction data, changes in the Bragg intensities resulting from texture / preferred orientation can strongly degrade the quality of a Rietveld refinement or prevent a structure solution. Here, we consider models for describing texture in polycrystalline samples and examine their application to real world examples.

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References

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Acknowledgments

This work was supported by the US Department of Energy, Office of Basic Energy Sciences, Office of Science, under contract No. DE-AC-02-06CH11357.

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Correspondence to Robert B. Von Dreele .

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© 2012 Springer Science+Business Media Dordrecht

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Von Dreele, R.B. (2012). Texture – An Overview. In: Kolb, U., Shankland, K., Meshi, L., Avilov, A., David, W. (eds) Uniting Electron Crystallography and Powder Diffraction. NATO Science for Peace and Security Series B: Physics and Biophysics. Springer, Dordrecht. https://doi.org/10.1007/978-94-007-5580-2_22

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  • DOI: https://doi.org/10.1007/978-94-007-5580-2_22

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  • Publisher Name: Springer, Dordrecht

  • Print ISBN: 978-94-007-5579-6

  • Online ISBN: 978-94-007-5580-2

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