Abstract
Samples that are polycrystalline solids produced by some mechanical process frequently possess a non-random orientation of the crystallites due to deformation of the material during the forming operation. The resulting crystallite orientations (“texture”) can be more complex that those obtained from simple packing of powders. In the course of crystal structure analysis from powder diffraction data, changes in the Bragg intensities resulting from texture / preferred orientation can strongly degrade the quality of a Rietveld refinement or prevent a structure solution. Here, we consider models for describing texture in polycrystalline samples and examine their application to real world examples.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
References
March A (1932) Mathematische theorie der regelung nach korngestalt bei affiner deformation. Z Kristallogr 81:285–297
Dollase WA (1986) Correction of intensities for preferred orientation in powder diffractometry: application of the March model. J Appl Crystallogr 19:267–272
Bunge HJ (1993) Texture analysis in materials science. Cuviller Verlag, Gottingen
Von Dreele RB (1997) Quantitative texture analysis by Rietveld refinement. J Appl Crystallogr 30:517–525
Wenk HR (1991) Standard project for pole figure determination by neutron diffraction. J Appl Crystallogr 24:920–927
Acknowledgments
This work was supported by the US Department of Energy, Office of Basic Energy Sciences, Office of Science, under contract No. DE-AC-02-06CH11357.
Author information
Authors and Affiliations
Corresponding author
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2012 Springer Science+Business Media Dordrecht
About this paper
Cite this paper
Von Dreele, R.B. (2012). Texture – An Overview. In: Kolb, U., Shankland, K., Meshi, L., Avilov, A., David, W. (eds) Uniting Electron Crystallography and Powder Diffraction. NATO Science for Peace and Security Series B: Physics and Biophysics. Springer, Dordrecht. https://doi.org/10.1007/978-94-007-5580-2_22
Download citation
DOI: https://doi.org/10.1007/978-94-007-5580-2_22
Published:
Publisher Name: Springer, Dordrecht
Print ISBN: 978-94-007-5579-6
Online ISBN: 978-94-007-5580-2
eBook Packages: Physics and AstronomyPhysics and Astronomy (R0)