Abstract
Gold nano-electrode ensembles were synthesized within nanoporous polycarbonate membranes and coupled with screen printed substrates. A disposable and versatile electrochemical system for biosensing and bio analytical applications has been obtained. Scanning Electron Microscopy and Scanning Probe Microscopy techniques were used to characterize the membrane surface, the nanostructured surfaces and the resulting biosensing devices. Efficiency and response of nano-probes were tested with several enzymatic immobilizations on the sensitive surface. Herein, the model case of a glucose oxidase biosensor based on nanoelectrodes is taken into account, for further evaluations on the accuracy of the biosensor system.
Access this chapter
Tax calculation will be finalised at checkout
Purchases are for personal use only
References
Jirage KB, Hulteen JC, Martin CR (1999) Effect of thiol chemisorption on the transport properties of gold nanotubule membranes. Anal Chem 71(21):4913–4918
Gamero M, Pariente F, Lorenzo E, Alonso C (2010) Nanostructured rough gold electrodes for the development of lactate oxidase-based biosensors. Biosensors Bioelectronics 25(9):2038–2044
Codognoto L, Winter E, Doretto KM, Monteiro GB, Rath S (2010) Electroanalytical performance of self-assembled monolayer gold electrode for chloramphenicol determination. Microchimica Acta 169(3–4):345–351
Menon VP, Martin CR (1995) Fabrication and evaluation of nanoelectrode ensembles. Anal Chem 67(13):1920–1928
DeLeo M, Kuhn A, Ugo P (2007) 3D-ensembles of gold nanowires: preparation, characterization and electroanalytical peculiarities. Electroanalysis 19(2–3):227–236
Pereira FC, Moretto LM, De Leo M, Boldrin Zanoni MV, Ugo P (2006) Gold nanoelectrode ensembles for direct trace electroanalysis of iodide. Anal Chim Acta 575(1):16–24
Vastarella W, Maly J, Ilie M (2009) Integration between template based nanostructured surfaces and biosensors. In: Merkoçi A (ed) Biosensing using Nanomaterials. Wiley, Hoboken, pp 379–419
Ugo P, Moretto LM (2007) Metal deposition. In: Zoski CG (ed) Handbook of electrochemistry, Elsevier Science, Amsterdam, Chapter 16, Section 16.2, pp 678–709
Brunetti B, Ugo P, Moretto LM, Martin CR (2000) Electrochemistry of phenothiazine and methylviologen biosensor electron transfer mediators at nanoelectrode ensembles. J Electroanal Chem 491(1–2):166–174
Moretto LM, Pepe N, Ugo P (2004) Voltammetry of redox analytes at trace concentrations with nanoelectrode ensembles. Talanta 62(5):1055–1060
Vastarella W, Della Seta L, Masci A, Maly J, De Leo M, Moretto LM, Pilloton R (2007) Biosensors based on gold nanoelectrode ensembles and screen printed electrodes. Int J Environ Anal Chem 87(10–11):701–714
Lee HS, Salerno MB, Rittmann BE (2008) Thermodynamic evaluation on H2 production in glucose fermentation. Environ Sci Technol 42:2401–240
Author information
Authors and Affiliations
Corresponding author
Editor information
Editors and Affiliations
Rights and permissions
Copyright information
© 2011 Springer Science+Business Media B.V.
About this paper
Cite this paper
Della Seta, L., Montereali, M.R., Patriarca, C., Marone, A., Vastarella, W. (2011). Electrochemical and Morphological Investigation on Gold Bio-Nano-Electrodes. Preliminary Results. In: Neri, G., Donato, N., d'Amico, A., Di Natale, C. (eds) Sensors and Microsystems. Lecture Notes in Electrical Engineering, vol 91. Springer, Dordrecht. https://doi.org/10.1007/978-94-007-1324-6_18
Download citation
DOI: https://doi.org/10.1007/978-94-007-1324-6_18
Published:
Publisher Name: Springer, Dordrecht
Print ISBN: 978-94-007-1323-9
Online ISBN: 978-94-007-1324-6
eBook Packages: EngineeringEngineering (R0)