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Estrazione con fluidi supercritici (SFE)

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Il campione per l’analisi chimica

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Riassunto

L’estrazione con fluidi supercritici, o supercritical fluid extraction (SFE), rappresenta una valida alternativa ai sistemi classici di estrazione con solvente e ad altre tecniche, come distillazione frazionata, estrazione in corrente di vapore e desorbimento termico.

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Bibliografia

  • Ali MY, Cole RB (2001) SFE-plus-C18 Lipid Cleanup and Selective Extraction Method for GC/MS Quantitation of Polycyclic Aromatic Hydrocarbons in Smoked Meat. Journal of Agricultural and Food Chemistry, 49(9): 4192–4198

    Article  CAS  Google Scholar 

  • Ali MY, Cole RB (2002) One-step SFE-plus-C(18) selective extraction of low-polarity compounds, with lipid removal, from smoked fish and bovine milk. Analytical Bioanalytical Chemistry, 374(5): 923–931

    Article  CAS  Google Scholar 

  • Andersen MR, King JW, Hawtorne SB (1990) Environmental matrices extracted by SPE. In: Lee ML, Markides KE (eds) Analytical supercritical fluid chromatography and extraction. Chromatographic Conferences, Provo, UT

    Google Scholar 

  • Andersen MR, Swanson JT, Porter NL, Richter BE (1989) Supercritical fluid extraction as a sample introductory method for chromatography. Journal of Chromatographic Science, 27(7): 371–377

    Article  CAS  Google Scholar 

  • Anyanwu EC, El-Saeid MH, Akpan AI, Saled MA (2003) Evaluation of the most current and effective methods in the analysis of chlorinated dioxins in ground beef. The Scientific World Journal, 3: 913–921

    Article  Google Scholar 

  • AOAC International (2002) Official Method of Analysis 41.1.69

    Google Scholar 

  • Arancibia V, Valderrama M, Rodriguez P et al (2003) Quantitative extraction of sulfonamides in meats by supercritical methanol-modified carbon dioxide: A foray into real-world sampling. Journal of Separation Science, 26(18): 1710–1716

    Article  CAS  Google Scholar 

  • Ashraf-Khorassani M, Ude M, Doane-Wedeman T et al (2002) Comparison of gravimetry and hydrolysis/derivatization/gas chromatography-mass spectrometry for quantitative analysis of fat from standard reference infant formula powder using supercritical fluid extraction. Journal of Agricultural and Food Chemistry, 50(7): 1822–1826

    Article  CAS  Google Scholar 

  • Barth MM, Zhou C, Kute KM, Rosenthal GA (1995) Determination of optimum conditions for supercritical fluid extraction of carotenoids from carrot (Daucus carota L.) tissue. Journal of Agricultural and Food Chemistry, 43(11): 2876–2878

    Article  CAS  Google Scholar 

  • Berche B, Henkel M, Kenna R (2009) Critical phenomena: 150 years since Cagniard de la Tour. Journal of Physical Studies, 13(3): 3001–3004

    Google Scholar 

  • Björklund E, Jàremo M, Mathiasson L (2000) Simultaneous determination of PCBs and triglycerides in a model fat sample using selective supercritical fluid extraction. Journal of Liquid Chromatography and Related Techniques, 23(15): 2337–2344

    Article  Google Scholar 

  • Björklund E, von Holst C, Anklam E (2002) Fast extraction, clean-up and detection methods for the rapid analysis and screening of seven indicator PCBs in food matrices. Trends in Analytical Chemistry, 21(1) 40–53

    Article  Google Scholar 

  • Boatto G, Nieddu M, Carta A et al (2003) Supercritical fluid extraction and GC detection of p,p1-DDE and PCB congeners in some samples of dying species from Sardinia. Fresenius Environmental Bulletin 12(5): 435–441

    CAS  Google Scholar 

  • Bøwadt S, Pelusio F, Montanarella L, Larsen B (1993) Trapping techniques in supercritical fluid extraction. Journal of Trace and Microprobe Techniques, 11(1–3): 117–131

    Google Scholar 

  • Cavalcanti RN, Meireles MAA (2012) Fundamentals of supercritical fluid extraction. In: Pawliszyn J (ed) Comprehensive sampling and sample preparation. Elsevier, Amsterdam

    Google Scholar 

  • Cavalcanti RN, Navarro-Díaz HJ, Santos DT et al (2012) Supercritical carbon dioxide extraction of polyphenols from pomegranate (Punica granatum L.) leaves: chemical composition, economic evaluation and chemometric approach. Journal of Food Research, 1(3): 282–294

    Article  CAS  Google Scholar 

  • Chafer A, Pascual-Martí MC, Salvador A, Berna A (2005) Supercritical fluid extraction and HPLC determination of relevant polyphenolic compounds in grape skin. Journal of Separation Science, 28(16): 2050–2056

    Article  CAS  Google Scholar 

  • Combs MT, Boyd S, Ashraf-Hhorassani M, Taylor LT (1997) Quantitative recovery of sulfonamides from chicken liver, beef liver, and egg yolk via modified supercritical carbon dioxide. Journal of Agricultural and Food Chemistry, 45(5): 1779–1783

    Article  CAS  Google Scholar 

  • Döker O, Salgin U, Yildiz N et al (2010) Extraction of sesame seed oil using supercritical CO2 and mathematical modeling. Journal of Food Engineering, 97(3): 360–366

    Article  Google Scholar 

  • EPA — Environmental protection Agency (1996) Supercritical fluid extraction of polynuclear aromatic hydrocarbons, EPA method 3561 http://www.epa.gov/osw/hazard/testmethods/sw846/pdfs/3561.pdf

    Google Scholar 

  • EPA — Environmental protection Agency (1996) Supercritical fluid extraction of total hydrocarbons, E PA method 3560 http://www.epa.gov/osw/hazard/testmethods/sw846/pdfs/3560.pdf

    Google Scholar 

  • Fiddler W, Pensabene JW (1996) Supercritical fluid extraction of volatile N-nitrosamines in fried bacon and its drippings: method comparison. Journal of AOAC International, 79(4): 895–901

    CAS  Google Scholar 

  • García-Rodríguez D, Carro-Díaz AM, Lorenzo-Ferreira RA (2008) Supercritical fluid extraction of polyhalogenated pollutants from aquaculture and marine environmental samples: A review. Journal of Separation Science, 31(8): 1333–1345

    Article  Google Scholar 

  • Hartonen K (2010) Novel accelerated extraction techniques. In: Jestoi M, Jàrvenpàà E, Peltonen K (eds) First dice your dill — new methods and techniques in sample handling. University of Turku, Turku

    Google Scholar 

  • Hopper ML, King JW, Johnson JH et al (1995) Multivessel supercritical fluid extraction of food items in Total Diet Study. Journal of AOAC International, 78(4): 1072–1079

    CAS  Google Scholar 

  • Horvatovich P, Miesch M, Hasselmann C, Marchioni E (2000) Supercritical fluid extraction of hydrocarbons and 2-alkylcyclobutanones for the detection of irradiated foodstuffs. Journal of Chromatography A, 897(1–2): 259–268

    Article  CAS  Google Scholar 

  • Hüsers N, Kleiböhmer W (1995) Studies on trapping efficiencies of various collection devices for offline supercritical fluid extraction. Journal of Chromatography A, 697(1–2): 107–114

    Article  Google Scholar 

  • King JW, Zhang Z (2002) Derivatization reactions of carbamate pesticides in supercritical carbon dioxide. Analytical Bioanalytical Chemistry, 374(1): 88–92

    Article  CAS  Google Scholar 

  • Lage Yusty MA, Cortizo Daviña JL (2005) Supercritical fluid extraction and high-performance liquid chromatography-fluorescence detection method for polycyclic aromatic hydrocarbons investigation in vegetable oil. Food Control, 16(1): 59–64

    Article  CAS  Google Scholar 

  • Larráyoz P, Carbonell M, Ibáñez F et al (1999) Optimization of indirect parameters which affect the extractability of volatile arima compounds from Idiazábal cheese using analytical supercritical fluid extractions (SFE). Food Chemistry, 64(1): 123–127

    Article  Google Scholar 

  • Lehotay SJ, Ibrahim MA (1995) Supercritical-fluid extraction and gas-chromatography ion-trap mass-spectrometry of pentachloronitrobenzene pesticides in vegetables. Journal of AOAC International, 78(2): 445–452

    CAS  Google Scholar 

  • Lehotay SJ, Valverde-García A (1997) Evaluation of different solid-phase traps for automated collection and clean-up in the analysis of multiple pesticides in fruits and vegetables after supercritical fluid extraction. Journal of Chromatography A, 765(1): 69–84

    Article  CAS  Google Scholar 

  • López M, Arce L, Garrido J et al (2004) Selective extraction of astaxanthin from crustaceans by use of supercritical carbon dioxide. Talanta, 64(3): 726–731

    Article  Google Scholar 

  • Mendiola JA, Herrero M, Cifuentes A, Ibañez E (2007) Use of compressed fluids for sample preparation: Food applications. Journal of Chromatography A, 1152(1–2): 234–246

    Article  CAS  Google Scholar 

  • Morales MT, Berry AJ, McIntyre PS, Aparicio R (1998) Tentative analysis of virgin olive oil aroma by supercritical fluid extraction-high resolution gas chromatography-mass spectrometry. Journal of Chromatography A, 819(1–2) 267–275

    Article  CAS  Google Scholar 

  • O’Keeffe MJ, O’Keeffe MO, Glennon JD (1999) Supercritical fluid extraction (SFE) as a multi-residue extraction procedure for beta-agonists in bovine liver tissue. Analyst, 124(9): 1355–1360

    Article  Google Scholar 

  • Palenzuela B, Rodríguez-Amaro R, Rios A, Valcárcel M (2002) Screening of polyphenols in grape marc by on-line supercritical fluid extraction — Amperometric detection with a PVC-graphite composite electrode. Electroanalysis, 14 (19–20): 1427–1432

    Article  CAS  Google Scholar 

  • Pourmortazavi SM, Hajimirsadeghi SS (2007) Supercritical fluid extraction in plant essentials and volatile oil analysis. Journal of Chromatography A, 1163(1–2): 2–24

    Article  CAS  Google Scholar 

  • Stolker AA, Zoontjes PW, van Ginkel LA (1998) The use of supercritical fluid extraction for the determination of steroids in animal tissues. Analyst, 123(12): 2671–2676

    Article  CAS  Google Scholar 

  • Sun M, Temelli F (2006) Supercritical carbon dioxide extraction of carotenoids from carrot using canola oil as a continuous co-solvent. Journal of Supercritical Fluids, 37: 397–408

    Article  CAS  Google Scholar 

  • Taylor SL, King JW, Richard JL, Greer JI (1993) Analytical-scale supercritical fluid extraction of aflatoxin B1 from field-inoculated corn. Journal of Agricultural and Food Chemistry, 41(6): 910–913

    Article  CAS  Google Scholar 

  • Taylor SL, King JW, Richard JL, Greer JI (1997) Supercritical fluid extraction of aflatoxin M1 from beef liver. Journal of Food Protection, 60(6): 698–700

    CAS  Google Scholar 

  • Turner C, King JW, Mathiasson L (2001) Supercritical fluid extraction and chromatography for fat-soluble vitamin analysis. Journal of Chromatogrophy A, 936: 215–237

    Article  CAS  Google Scholar 

  • Turner C, Sparr Eskilsson C, Björklund E (2002) Collection in analytical-scale supercritical fluid extraction. Journal of Chromatography A, 947: 1–22

    Article  CAS  Google Scholar 

  • Vasapollo G, Longo L, Rescio L, Ciurlia L (2004) Innovative supercritical CO2 extraction of lycopene from tomato in the presence of vegetable oil as cosolvent. Journal of Supercritical Fluids, 29: 87–96

    Article  CAS  Google Scholar 

  • Xie QL, Markides KE, Lee ML (1989) Supercritical fluid extraction-supercritical fluid chromatography with fraction collection for sensitive analytes. Journal of Chromatographic Science, 27(7): 365–370

    Article  CAS  Google Scholar 

  • Xu L, Zhan X, Chen R et al (2011) Recent advances on supercritical fluid extraction of essential oils. African Journal of Pharmacy and Pharmacology, 5(9): 1196–1211

    Article  CAS  Google Scholar 

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Moret, S., Conte, L.S. (2014). Estrazione con fluidi supercritici (SFE). In: Il campione per l’analisi chimica. Food. Springer, Milano. https://doi.org/10.1007/978-88-470-5738-8_2

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