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Experimental and ZAF Correction Aspects of Carbon Analysis in Steels: Application to the Carburization of Irradiated Uranium-Plutonium Carbide Fuel Pin Claddings

  • H. Kleykamp
Part of the Mikrochimica Acta book series (MIKROCHIMICA, volume 10)

Abstract

The quantitative carbon analysis in steels by electron probe microanalysis (EPMA) has been on debate for more than one decade when the ZAF correction procedure was extended to the light element analysis with material data becoming available at that time. The conditions for a reliable analysis are a hydrocarbon low vacuum in the electron optical column of the instrument, a qualified sample preparation, selected standards similar in composition to the target and a well-developed ZAF correction computer programme.

Keywords

Carbon Analysis Mass Attenuation Coefficient Backscatter Coefficient Turbomolecular Pump Carbide Fuel 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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References

  1. 1.
    H. Kleykamp, Reaktortagung Düsseldorf 1976, proc. symp., p. 542.Google Scholar
  2. 2.
    H. Kleykamp, in Advanced LMFBR Fuels, Tucson/Ariz. 1977, proc. symp., p. 166.Google Scholar
  3. 3.
    H. Kleykamp, Reaktortagung Hannover 1978, proc. symp., p. 660.Google Scholar
  4. 4.
    M. Champigny, D. Gauvain, L. Meny, and J. Ruste, J. Microsc. Spectrosc. Electron. 4, 137 (1979).Google Scholar
  5. 5.
    R. Cytermann, M. Perrot, and J. Rouault, in Int. Conf. on Post-irradiation Examination, Lake District/UK 1980, proc. symp., p. 161.Google Scholar
  6. 6.
    R. Cytermann, M. Perrot, and N. Vignesoult, J. Microsc. Spectrosc. Electron. 6, 611 (1981).Google Scholar
  7. 7.
    J. Ruste, M. Bouchacourt, and F. Thevenot, J. Less-Common Met. 59, 131 (1978).CrossRefGoogle Scholar
  8. 8.
    W. Weisweiler, Mikrochim. Acta [Wien], Suppl. IV, 1970, 17.Google Scholar
  9. 9.
    S. Baumgartl, A.R. Büchner, K. Dreyer, P. Schwaab, H. Stender, and H. Vetters, Arch. Eisenhüttenwes. 50, 85 (1979).Google Scholar
  10. 10.
    K.F.J. Heinrich, Mikrochim. Acta [Wien], Suppl. IV, 1970, 253.Google Scholar
  11. 11.
    K.F.J. Heinrich, H. Yakowitz, Mikrochim. Acta [Wien] 1970, 123.Google Scholar
  12. 12.
    S.J.B. Reed, in 8th Int. Conf. on X-Ray Optics and Microanal., Boston 1977, proc. symp., p. 25A.Google Scholar
  13. 13.
    G. Love and V.D. Scott, in 9th Int. Conf. on X-Ray Optics and Microanal., Den Haag 1980, proc. symp., vol. 3, p. 146.Google Scholar
  14. 14.
    A. Boekestein, A.M. Stadhouders, A.L.H. Stols, G.M. Roomans, and E. Peters, in 10th Int. Conf. on Electron Microsc., Hamburg 1982, proc. symp., vol. 1, p. 667.Google Scholar
  15. 15.
    H. Hantsche and G. Kempf, Beitr. elektronenmikrosk. Direktabb. Oberfl. 15, 99 (1982).Google Scholar
  16. 16.
    P.M. Thomas, Report AERE-R 4593 (1964).Google Scholar
  17. 17.
    J. Philibert and R. Tixier, J. Phys. D 1, 685 (1968).CrossRefGoogle Scholar
  18. 18.
    M. J. Berger and S. M. Seltzer, in Publ. 1133, Ntl. Acad. of Sciences, Washington/D.C. 1964, p. 205.Google Scholar
  19. 19.
    P. Duncumb, P.K. Shields-Mason, and C. da Casa, in 5th Int. Congr. on X-Ray Optics and Microanal., Tübingen 1968, proc. symp., p. 146.Google Scholar
  20. 20.
    J. Ruste, in 8th Int. Conf. on X-Ray Optics and Microanal., Boston 1977, proc. symp., p. 35A.Google Scholar
  21. 21.
    W. Weisweiler, Arch. Eisenhüttenwes. 49, 555 (1978).Google Scholar
  22. 22.
    J.W. Colby, Adv. in X-Ray Anal. 11, 287 (1968).CrossRefGoogle Scholar
  23. 23.
    W. Bambynek, B. Crasemann, R.W. Fink, H.U. Freund, H. Mark, C.D. Swift, R.E. Price, and P. V. Rao, Rev. Mod. Phys. 44, 716 (1972).CrossRefGoogle Scholar
  24. 24.
    B.L. Henke and E.S. Ebisu, in Adv. in X-Ray Anal. 17, 150 (1974).CrossRefGoogle Scholar
  25. 25.
    J. Philibert, in 5th Int. Congr. on X-Ray Optics and Microanal., Tübingen 1968, proc. symp., p. 114.Google Scholar
  26. 26.
    O. Brümmer, Mikroanalyse mit Elektronen-und Ionensonden, 2nd ed. Leipzig: 1980. p.98.Google Scholar
  27. 27.
    W.C. Leslie, The Physical Metallurgy of Steels. New York: 1981.Google Scholar

Copyright information

© Springer-Verlag Wien 1983

Authors and Affiliations

  • H. Kleykamp
    • 1
  1. 1.Institut für Material- und FestkörperforschungKernforschungszentrum KarlsruheKarlsruheFederal Republic of Germany

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