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Chemische Strukturaufklärung

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Stoffliche Nutzung von Braunkohle

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Zusammenfassung

Die Charakterisierung der Energierohstoffe auf molekularer Ebene und in Bezug auf mineralische Bestandteile erfolgte in drei Schwerpunkten. Zum ersten sind konventionelle Methoden der Infrarot- und NMR-Spektroskopie für die Beschreibung von Kohlestrukturgruppen weiterentwickelt worden. Für die Analyse höher molekularer organischer Verbindungen bis hin zur Charakterisierung von Makromolekülen in Kohlen und Biomasse ist erstmalig die ultra-hochaufgelöste Fourier-Transform-Ionenzyklotron-Resonanz Massenspektrometrie (FT-ICR-MS) eingesetzt worden. Im dritten Schwerpunkt der chemischen Strukturaufklärung stand die Multielementanalytik aller prozessrelevanten mineralischen Bestandteile im Fokus. Hierzu wurde die elektrothermische Verdampfung in Kombination mit der Plasma-Atomemissionsspektrometrie (ETV-ICP OES) weiterentwickelt.

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Authors and Affiliations

  1. Institut für Analytische Chemie, TU Bergakademie Freiberg, Leipziger Str. 29, 09599, Freiberg, Deutschland

    Mirjam Schmidt

  2. Institut für Analytische Chemie, TU Bergakademie Freiberg, Leipziger Str. 29, 09599, Freiberg, Deutschland

    Daniela Vogt

  3. Institut für Analytische Chemie, TU Bergakademie Freiberg, Leipziger Str. 29, 09599, Freiberg, Deutschland

    Thomas Vogt

  4. Institut für Analytische Chemie, TU Bergakademie Freiberg, Leipziger Str. 29, 09599, Freiberg, Deutschland

    Matthias Otto

  5. Institut für Analytische Chemie, TU Bergakademie Freiberg, Leipziger Str. 29, 09599, Freiberg, Deutschland

    Bianca Wolf

  6. Institut für Analytische Chemie, TU Bergakademie Freiberg, Leipziger Str. 29, 09599, Freiberg, Deutschland

    Marika Rönnefahrt

  7. Institut für Analytische Chemie, TU Bergakademie Freiberg, Leipziger Str. 29, 09599, Freiberg, Deutschland

    Jan Zuber

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  1. Mirjam Schmidt
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  2. Daniela Vogt
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  4. Matthias Otto
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Correspondence to Mirjam Schmidt , Daniela Vogt or Bianca Wolf .

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Editors and Affiliations

  1. Inst. für Energieverfahrenstechnik und Chemieingenieurwesen, TU Bergakademie Freiberg, Freiberg, Germany

    Steffen Krzack

  2. Inst. für Energieverfahrenstechnik und Chemieingenieurwesen, TU Bergakademie Freiberg, Freiberg, Germany

    Heiner Gutte

  3. Inst. für Energieverfahrenstechnik und Chemieingenieurwesen, TU Bergakademie Freiberg, Freiberg, Germany

    Bernd Meyer

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Schmidt, M. et al. (2018). Chemische Strukturaufklärung. In: Krzack, S., Gutte, H., Meyer, B. (eds) Stoffliche Nutzung von Braunkohle. Springer Vieweg, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-46251-5_9

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