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Molybdate Hydrates with Subgroup 3 Metals

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Book cover Mo Molybdenum

Part of the book series: Gmelin Handbook of Inorganic Chemistry ((1039,volume M-o / A-B / B / 4))

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Abstract

During studies of the solubility of rare earth molybdates M2(MoO4)3 · n H2O with M = La to Er and Yb in weakly acidic aqueous MCI3 solutions the formation of soluble complexes [MMoO4]+ has been observed [1]. These complexes form in an initial reaction when an aqueous solution of ammonium paramolybdate is added to an aqueous MCI3 solution in the concentration range Mo: M<1.5 for M = La, Sm, Er, and Yb. With increasing paramolybdate concentrations the M2(MoO4)3·nH2O molybdates (see below) precipitate [2]. In basic medium the compounds M(OH)MoO4· n H2O are formed (p. 249) [3, 4]. The stability constants K, determined by conductivity measurements at pH 5.5 to 6.5, 25°C, and an ionic strength of 0.0012, are given in the following table (Std. Dev. = standard deviation) [1]:

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Authors and Affiliations

  1. Universität Göttingen, Germany

    Karl-Heinz Tytko

  2. Gmelin-Institut, Frankfurt am Main, Germany

    Wolf-Dietrich Fleischmann, Dieter Gras & Eberhard Warkentin

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  1. Karl-Heinz Tytko
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Hartmut Katscher Friedrich Schröder

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Tytko, KH., Fleischmann, WD., Gras, D., Warkentin, E. (1985). Molybdate Hydrates with Subgroup 3 Metals. In: Katscher, H., Schröder, F. (eds) Mo Molybdenum. Gmelin Handbook of Inorganic Chemistry, vol M-o / A-B / B / 4. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-07836-5_6

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