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Gallium Triorganyls

  • Jean-Claude Maire
  • Ulrich Krüerke
  • Marlis Mirbach
  • Wolfgang Petz
  • Christa Siebert
Part of the Gmelin Handbook of Inorganic and Organometallic Chemistry - 8th edition book series (GMELIN, volume G-a / 1- / 1)

Abstract

The reaction of methyl Grignard reagents with gallium halides leads to the etherate Ga(CH3)3-O(C2H5)2 [1,2] which can be converted into solvent-free Ga(CH3)3 by heating in a higher boiling ether [22]. The preparation of solvent-free Ga(CH3)3 from GaCl3 and CH3MgI in O(C5H11-i)2 in a 68% yield has been claimed in [44]. The Grignard solution containing an excess of CH3I can also be electrolyzed using a Ga-pool anode and a Pt cathode to give Ga(CH3)3-O(C2H5)2 which is converted into Ga(CH3)3 by addition of O(C5H11-i)2, removal of ether under vacuum, and decomposition of Ga(CH3)3•O(C5H11-i)2 at 190°C [40]; see also [45].

Keywords

Raman Spectrum Nuclear Quadrupole Resonance Dalton Trans Stretch Force Constant Neat Liquid 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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Copyright information

© Springer-Verlag Berlin Heidelberg 1986

Authors and Affiliations

  • Jean-Claude Maire
    • 1
  • Ulrich Krüerke
  • Marlis Mirbach
  • Wolfgang Petz
  • Christa Siebert
  1. 1.Université d’Aix-MarseilleFrance

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