Gallium Triorganyls

  • Jean-Claude Maire
  • Ulrich Krüerke
  • Marlis Mirbach
  • Wolfgang Petz
  • Christa Siebert
Part of the Gmelin Handbook of Inorganic and Organometallic Chemistry - 8th edition book series (GMELIN, volume G-a / 1- / 1)

Abstract

The reaction of methyl Grignard reagents with gallium halides leads to the etherate Ga(CH3)3-O(C2H5)2 [1,2] which can be converted into solvent-free Ga(CH3)3 by heating in a higher boiling ether [22]. The preparation of solvent-free Ga(CH3)3 from GaCl3 and CH3MgI in O(C5H11-i)2 in a 68% yield has been claimed in [44]. The Grignard solution containing an excess of CH3I can also be electrolyzed using a Ga-pool anode and a Pt cathode to give Ga(CH3)3-O(C2H5)2 which is converted into Ga(CH3)3 by addition of O(C5H11-i)2, removal of ether under vacuum, and decomposition of Ga(CH3)3•O(C5H11-i)2 at 190°C [40]; see also [45].

Keywords

Vinyl Diamine Biphenyl Pentane ZnSe 

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Copyright information

© Springer-Verlag Berlin Heidelberg 1986

Authors and Affiliations

  • Jean-Claude Maire
    • 1
  • Ulrich Krüerke
  • Marlis Mirbach
  • Wolfgang Petz
  • Christa Siebert
  1. 1.Université d’Aix-MarseilleFrance

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