Organoiron Compounds, Part B

Mononuclear Compounds 11
  • Konrad Holzapfel
  • Wolfgang Petz
  • Christa Siebert (Maintal)
  • Bernd Wöbke
Part of the Gmelin Handbook of Inorganic Chemistry / Gmelin Handbuch der Anorganischen Chemie book series (GMELIN, volume F-e / A-C / B / 11)

Abstract

[C5H5Fe]+C6H5CO0- forms in solution by photolysis (λ=359 and 466 nm) of benzoylferrocene and an excess of water in (CH3)2S0, pyridine, or dimethylformamide. The 1H NMR spectrum of a C5D5N solution shows a C5H5 resonance at δ=3.8 ppm along with signals of C6H5C00- and cyclopentadiene. Characteristic IR absorptions indicate the presence of a carboxylate group. Admission of oxygen produces a purple solution (λmax=550 nm), which displays the ESR spectrum of high-spin FeIII. Benzoic acid was isolated after acidification [1].

Keywords

Carbonyl Pyrrole Thermolysis Hexadecane Dithiocarbamate 

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Copyright information

© Springer-Verlag Berlin Heidelberg 1982

Authors and Affiliations

  • Konrad Holzapfel
  • Wolfgang Petz
  • Christa Siebert (Maintal)
  • Bernd Wöbke

There are no affiliations available

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