S-Phosphorus-Substituted Thiohydroxylamines and Derivatives

  • Norbert Baumann
  • Hans-Jürgen Fachmann
  • Reimund Jotter
  • Alfons Kubny
Part of the Gmelin Handbook of Inorganic and Organometallic Chemistry / Gmelin Handbuch der Anorganischen Chemie book series (GMELIN, volume S / S-N / 10 / a)

Abstract

The compounds listed in Table 70 were prepared by passing dry NH3 for 45 min (No. 3) or 1 h (Nos. 1, 2, 4 to 6) through a solution of the corresponding phosphorus-containing disulfides, R2P(X)SSP(X)R2, in dry C6H6 (Nos. 1 to 5) or in dry ether (No. 6). Liquid products (Nos. 1 to 3) were separated and purified by vacuum distillation and solid products (Nos. 5, 6) by recrystallization from hexane (compound No. 4 decomposed during distillation) [1]. The compound with R = 4-CIC6H4, X = S formed analogously, but was not isolated [2].

Keywords

Rubber Recrystallization Anhydride CCl4 Piperidine 

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Copyright information

© Springer-Verlag Berlin Heidelberg 1994

Authors and Affiliations

  • Norbert Baumann
  • Hans-Jürgen Fachmann
  • Reimund Jotter
  • Alfons Kubny
    • 1
  1. 1.Frankfurt am MainGermany

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