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S-Phosphorus-Substituted Thiohydroxylamines and Derivatives

  • Norbert Baumann
  • Hans-Jürgen Fachmann
  • Reimund Jotter
  • Alfons Kubny
Part of the Gmelin Handbook of Inorganic and Organometallic Chemistry / Gmelin Handbuch der Anorganischen Chemie book series (GMELIN, volume S / S-N / 10 / a)

Abstract

The compounds listed in Table 70 were prepared by passing dry NH3 for 45 min (No. 3) or 1 h (Nos. 1, 2, 4 to 6) through a solution of the corresponding phosphorus-containing disulfides, R2P(X)SSP(X)R2, in dry C6H6 (Nos. 1 to 5) or in dry ether (No. 6). Liquid products (Nos. 1 to 3) were separated and purified by vacuum distillation and solid products (Nos. 5, 6) by recrystallization from hexane (compound No. 4 decomposed during distillation) [1]. The compound with R = 4-CIC6H4, X = S formed analogously, but was not isolated [2].

Keywords

Petroleum Ether Title Compound Equimolar Amount Maleic Anhydride Equimolar Mixture 
These keywords were added by machine and not by the authors. This process is experimental and the keywords may be updated as the learning algorithm improves.

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Copyright information

© Springer-Verlag Berlin Heidelberg 1994

Authors and Affiliations

  • Norbert Baumann
  • Hans-Jürgen Fachmann
  • Reimund Jotter
  • Alfons Kubny
    • 1
  1. 1.Frankfurt am MainGermany

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