Characterization of Metallic Catalysts by X-Ray and Electron Microscopy Techniques

  • G. Bergeret
Part of the Centre de Physique des Houches book series (LHWINTER, volume 6)

Abstract

This lecture is intended to describe briefly the X-ray and electron microscopy techniques and to give a survey of their application to the study of metallic catalysts.

Keywords

Nickel Graphite Silicate Platinum Zeolite 

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References

  1. [1]
    van Hardeveld R. and Hartog F., Surf. Sci. 15 (1969) 189–230.ADSCrossRefGoogle Scholar
  2. [2]
    Mackay A.L., Icta Crvst. 15 (1962) 916–918.Google Scholar
  3. [3]
    Gordon M.B., Ph. D. Thesis (3ep1e Cycle), Grenoble, France, 1978.Google Scholar
  4. [4]
    Rousset J.L.. Cadrot A.M., Cadete Santos Aires F.J., Renouprez A., Mélinon P., Perez A., Pellarin M., Vialle J.L. and Broyer M., J. Chem. Phys. 102 (1995) 8574–8585.Google Scholar
  5. [5]
    Bergeret G. and Gallezot P.. Particles Size and Dispersion Measurements. in “Handbook of Heterogeneous Catalysis”, G. Ertl. H. Knözinger and J. Weitkamp Eds. (VCH, Weinheim, to be published May 1997) Part A. Section 3. 1. 2.Google Scholar
  6. [6]
    Klug H.P. and Alexander L.E.. X-Ray Diffraction Procedures for Polycrystalline and Amorphous Materials, 2nd cd. (Wiley, New York. 1974 ).Google Scholar
  7. [7]
    Modern Powder Diffraction. D.L. Bish and J.E. Post Eds.. Reviews in Mineralogy, Vol. 20 ( Mineralogical Society of America, Washington DC. 1989 ).Google Scholar
  8. [8]
    Gallezot P, X-Ray Techniques in Catalysis, in “Catalysis, Science and Technology”, J.R. Anderson and M. Boudart Eds. ( Springer, Berlin. 1984 ) Vol. 5, pp. 221–273.Google Scholar
  9. [9]
    Bergeret G., X-Ray Powder Diffraction, in “Handbook of Heterogeneous Catalysis”, G. Ertl, H. Knözinger and J. Weitkamp Eds. (VCH, Weinheim, to be published May 1997) Part A, Section 3.1. 3. 1.Google Scholar
  10. [10]
    Powder Diffraction File (PDF), International Centre for Diffraction Data. 12 Campus Blvd, Newton Square, PA 19073–3273 USA, http://www.icdd.com.Google Scholar
  11. [11]
    Caussin P.. Nusinovici J. and Beard D.W., in “Advances in X-Ray Analysis”. C.S. Barrett. J.V. Gilfrich, R. Jenkins, T.C. Huang and P.K. Predecki Eds.. (Plenum, New York, 1989) Vol. 32, pp. 531–538; Diffrac-AT, Socabim. 9 bis Villa du Bel-Air, F75012 Paris.Google Scholar
  12. [12]
    Hardacre C., Rayment T. and Lambert R.M., J. Catal. 158 (1996) 102–108.CrossRefGoogle Scholar
  13. [13]
    Clausen B.S., Steffensen G., Fabius B., Villadsen J., Feidenhans L.R. and Topsoe H.. J. Catal. 132 (1991) 524–535.CrossRefGoogle Scholar
  14. [14]
    Faudon J.F., Senocq F., Bergeret G., Moraweck B., Clugnet G., Nicot C. and Renouprez A., J. Catal. 144 (1993) 460–471.CrossRefGoogle Scholar
  15. [15]
    Koningsberger D.C. and Prins R., X-Ray Absorption. Principles, Applications, Techniques of EXAFS, SEXAFS, and XANES ( Wiley, New York, 1988 ).Google Scholar
  16. [16]
    Teo B.K., EXAFS: Basic Principles and Data Analysis ( Springer, Berlin, 1986 ).CrossRefGoogle Scholar
  17. [17]
    Moraweck B., X-Ray Absorption Spectroscopy: EXAFS and XANES, in “Catalyst Characterization: Physical Techniques for Solid Materials”. B. Imelik and J.C. Védrine Eds. ( Plenum, New York, 1994 ) pp. 377–416.Google Scholar
  18. [18]
    Lagarde P, Murata F., Vlaic G., Freund E., Dexpert H. and Bournonville P., J. Catal. 84 (1983) 333–343.CrossRefGoogle Scholar
  19. Berdala J., Freund E. and Lynch J.P., J. J’hys. Fr. Coll 272 (1986) 265–268.Google Scholar
  20. Berdala J., Freund E. and Lynch J.P., J. J’hys. Fr. Coll 272 (1986) 269–272.Google Scholar
  21. Bazin D., Dexpert D.. Lagarde P. and Bournonville P., J. Catal. 110 (1988) 209–215.CrossRefGoogle Scholar
  22. [19]
    Sinfelt J.H.. Via G.H. and Lytle F.W., J. Chem. Phys. 72 (1980) 4832–4844.ADSCrossRefGoogle Scholar
  23. [20]
    Sinfelt J.H., Via G.H. and Lytle F.W., Applications of EXAFS in Catalysis. Structure of Bimetallic Cluster catalysts. Catal. Rev.-Sei. Eng. 26 (1984) 81140.Google Scholar
  24. [21]
    Prins R. and Koningsberger D.C., in ref [15], pp. 358–363.Google Scholar
  25. [22]
    Niemantsverdriet J.W., Spectroscopy in Catalysis: an Introduction ( VCH, Weinheim, 1995 ), pp. 150–164.Google Scholar
  26. [23]
    Hlil E.K., Baudoing-Savois R., Moraweck B. and Renouprez A.J., J. Phys. Chem. 100 (1996) 3102–3107.CrossRefGoogle Scholar
  27. [24]
    Howie A., The Study of Supported Catalysts by Transmission Electron Microscopy, in “Characterizationj of Catalysts”, J.M. Thomas and R.M. Lambert Eds. ( Wiley, Chichester, 1980 ) pp. 89–104.Google Scholar
  28. [25]
    Baird T.. Characterization of Catalysts by Electron Microscopy_ in “ A Specialist Periodical Report” Catalysis, Vol. 5 ( Royal Society of Chemistry. London, 1982 ) pp. 172–219.Google Scholar
  29. [26]
    Sanders J.V., The Electron Microscopy of Catalysts, in “Catalysis, Science and Technology”. J.R. Anderson and M. Boudait Eds. Vol. 7 ( Springer. Berlin, 1985 ) pp. 51–158.Google Scholar
  30. [27]
    Gallezot P. and Leclercq C.. Characterization of Catalysts by Conventional and Analytical Electron Microscopy, in “Catalyst Characterization: Physical Techniques for Solid Materials”, B. Imelik and J.C. Védrine Eds. ( Plenum. New York 1994 ) pp. 509–558.Google Scholar
  31. [28]
    Gallezot P, Leclercq C., Mutin I., Nicot C. and Richard D., J. Alrcrosc. Spectrosc. Electron. 10 (1985) 479–484.Google Scholar
  32. [29]
    Gallezot P, Leclercq C., Barbier J. and Marecot P., J. Cato!. 116 (1989) 164–170.CrossRefGoogle Scholar
  33. [30]
    Colliex C., Lefèvre E. and Tencé in “Electron Microscopy and Analysis 1993, Proc. of the Institute of Physics. Electron Microscopy and Analysis Group Conference, Liverpool, 1993”, A.J. Craven Ed., Institute of Physics Conference Series Number 138, Institute of Physics Publishing, Bristol 1993. pp. 25–30.Google Scholar

Copyright information

© Springer-Verlag Berlin Heidelberg 1997

Authors and Affiliations

  • G. Bergeret
    • 1
  1. 1.Institut de Recherches sur la CatalyseCNRSVilleurbanne cedexFrance

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