Abstract
To 1,2-C2B9H13 in C6H6 is added an equimolar amount of Be(C2H5)2∙3.30(C2H5)2. C2H6 is evolved, and a white precipitate is formed in a small yield. The precipitate is separated by filtration, washed with C6H6, and dried at 50°C.
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References
Popp, G., Hawthorne, M. F. (J. Am. Chem. Soc. 90 [1968] 6553/4).
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Schmid, G., Boltsch, O., Boese, R. (Organometallics 6 [1987] 435/9).
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© 1987 Springer-Verlag Berlin Heidelberg
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Schmidbaur, H. (1987). Compounds with Ligands Bonded by Two or Three Carbon Atoms (Beryllocarbaboranes). In: Kubny, A., Mirbach, M., Krüerke, U., Slawisch, A. (eds) Be Organoberyllium Compounds. Gmelin Handbook of Inorganic Chemistry, vol B-e / 1 / 1. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-06024-7_3
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DOI: https://doi.org/10.1007/978-3-662-06024-7_3
Publisher Name: Springer, Berlin, Heidelberg
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