Skip to main content

Diffusion Structural Analysis in the Characterization of Inorganic Materials

  • Chapter
Characterization Techniques of Glasses and Ceramics
  • 555 Accesses

Abstract

The fundamentals of the emanation thermal analysis are described and sample preparation for different inert gas operations are considered and discussed. The mechanisms of releasing inert gases from solids are exposed in relation to the measurements of the diffusion of gases in solid samples. Thus, the applications to ceramics investigation, surface roughness and defects of powders are described. Applications for glasses, clay minerals and cements are discussed from our own experimental work. The corrosion on materials can be also investigated with this method.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 89.00
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 119.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 169.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. V. Balek, J. Tölgyessy: Emanation thermal analysis and other radiometric emanation methods, (Wilson and Wilson Eds., Comprehensive Analytical Chemistry, Part XIIC, Elsevier, Amsterdam, 1984 ).

    Google Scholar 

  2. V. Balek: Thermochim. Acta 22, 1 (1978).

    Article  Google Scholar 

  3. R.A. Levy, P.K. Gallagher: J. Electrochem. Soc. 132, 606 (1985).

    Google Scholar 

  4. P.A. Redhead: Vacuum, 21, 203 (1962).

    Article  Google Scholar 

  5. G. Carter, J.S. Colligon: Ion Bombardment of Solids, ( Heinemann, London, 1968 ).

    Google Scholar 

  6. M.D. Norgett, H.B. Lidiard: Philos. Mag. 18, 1193 (1968).

    Article  ADS  Google Scholar 

  7. R. Kelly, Hj. Matzke: J. Nucl. Mater. 17, 197 (1965); 20, 175 (1966).

    Google Scholar 

  8. J. Kríz, V. Balek: Thermochim. Acta 78, 377 (1984); 110, 245 (1987).

    Article  Google Scholar 

  9. S. Flügge, K.E. Zimens: Z. Phys. Chem., Abt. B. 42, 179 (1939).

    Google Scholar 

  10. O. Hahn: J. Chem. Soc. Suppl., S 259 (1949).

    Google Scholar 

  11. V. Balek: Cz. Patent No. 151172.

    Google Scholar 

  12. W.D. Emmerich, V. Balek: High Temp. High Press. 5, 67 (1973).

    Google Scholar 

  13. C. Jech, R. Kelly: Proc. Br. Ceram. Soc. 9. 359 (1976).

    Google Scholar 

  14. F.W. Felix, K. Meier: Phys. Status Solidi 32, 139 (1969).

    Article  Google Scholar 

  15. A.S. Ong, T.S. Elleman: J. Nucl. Mater. 42, 191 (1972).

    Article  ADS  Google Scholar 

  16. V. Balek: J. Mater. Sci. 5, 166 (1979).

    Article  ADS  Google Scholar 

  17. V. Balek: Farbe und Lack 85, 252 (1979).

    Google Scholar 

  18. J.A. Hedvall: Solid State Chemistry, (Elsevier, 1969 ).

    Google Scholar 

  19. V. Balek, Z. Malek, H.J. Pentinghaus: J. Sol-gel Sci. Technol. 2, 301 (1997).

    Article  Google Scholar 

  20. V. Balek, M. Vobotil, V. Baran: Nucl. Technol. 50, 53 (1980).

    Google Scholar 

  21. V. Balek, E. Klosovä, M. Murat, N. Almeida Camargo: Bull Am. Ceram. Soc. 75, 73 (1996).

    Google Scholar 

  22. V. Balek, H. Landsperskÿ, M. Vobor’il: Radiochem. Radioanal. Lett. 28, 289 (1977).

    Google Scholar 

  23. V. Balek, J. Fusek, O. Kríz, M. Leskelä, L. Niinistö, E. Nykänen, J. Rautanen, P. Soininen: J. Mater. Res. 9, 119 (1994).

    Article  ADS  Google Scholar 

  24. C. Quet, P. Bussiere: C.R. Acad. Sci., Ser. C 280, 859 (1976).

    Google Scholar 

  25. V. Balek: Sprechsaal 116, 978 (1983).

    Google Scholar 

  26. V. Balek: J. Mater. Sci. 17, 1269 (1982).

    Article  ADS  Google Scholar 

  27. V. Balek, J. Götz: Proc. 11th Int. Glass Congress, Prague, Vol. 3, pp. 35. ( J. Götz Ed., Prague, 1977 ).

    Google Scholar 

  28. S. Bordas, M. Clavaguera-Mora, V. Balek: Thermochim. Acta 93 283 (1985).166 V. Balek

    Google Scholar 

  29. V. Balek, Z. Malek, A. Clearfield: Surface reactivity of high level matrices characterized by radiometric emanation method (Proc. 7th Int. Conference on high level radioactive waste management, Las Vegas, Nevada, 1996 ) p. 474.

    Google Scholar 

  30. V. Balek, Z. Malek, A. Clearfield: Alteration of nuclear waste glasses characterized by radon emanation method, (Summary of an International Workshop “Glass as a waste form and vitrification technology”, held at NAS, Washington D.C., May 1996) (NRS Paper E. 58 ) p. 102.

    Google Scholar 

  31. W.D. Emmerich, V. Balek: High Temp.-High Pressures 5, 67 (1973).

    Google Scholar 

  32. V. Balek, J. Subrt: J. Pure Appl. Chem. 67, 1839 (1995).

    Article  Google Scholar 

  33. Z. Malek, V. Balek, D. Garfinkel-Schwekey, S. Yariv: J. Thermal Anal. 48, 83 (1997).

    Article  Google Scholar 

  34. V. Balek, M. Murat: Thermochim. Acta 282/283, 385 (1996).

    Google Scholar 

  35. V. Balek: Thermochim. Acta 72, 147 (1984).

    Article  Google Scholar 

  36. V. Balek, J. Dohndlek: J. Mater. Sci. 17, 2281 (1982).

    Article  ADS  Google Scholar 

  37. V. Balek, Z. Malek, B. Cdsenskÿ, D. Niznanskÿ, J. Subrt, E. Vecerníkovâ, H. Römich, M. Pilz: J. Sol-gel Sci Technol 8, 591 (1997).

    Google Scholar 

  38. V. Balek: J. Am. Ceram. Soc. 53, 540 (1970).

    Google Scholar 

  39. T. Ishii: Thermochim. Acta 88, 277 (1985); 93, 469 (1985); 109, 252 (1979).

    Google Scholar 

  40. V. Balek: J. Appl. Chem. (London) 20, 73 (1970).

    Article  Google Scholar 

  41. V. Balek: J. Therm. Anal. 12, 111 (1977).

    Google Scholar 

  42. V. Balek: Thermochim. Acta 110, 221 (1987).

    Article  Google Scholar 

  43. V. Balek: J. Thermal Anal. 35, 405 (1989).

    Article  ADS  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Editor information

Editors and Affiliations

Rights and permissions

Reprints and permissions

Copyright information

© 1999 Springer-Verlag Berlin Heidelberg

About this chapter

Cite this chapter

Balek, V. (1999). Diffusion Structural Analysis in the Characterization of Inorganic Materials. In: Rincon, J.M., Romero, M. (eds) Characterization Techniques of Glasses and Ceramics. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-03871-0_8

Download citation

  • DOI: https://doi.org/10.1007/978-3-662-03871-0_8

  • Publisher Name: Springer, Berlin, Heidelberg

  • Print ISBN: 978-3-642-08348-8

  • Online ISBN: 978-3-662-03871-0

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics