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Identification and Confirmatory Analysis Based on Capillary GC-Mass Spectrometry

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Analysis of Pesticides in Ground and Surface Water I

Part of the book series: Chemistry of Plant Protection ((PLANT PROTECTIO,volume 11))

Abstract

In this chapter, the application of GC/MS for the confirmation of results positively monitored with screening methods using less selective detectors is described. Furthermore, the screening for pesticides in water—ranging from ground and tap to surface and sewage water—with full scan as well as the target compound analysis applying selected ion monitoring (SIM) is reviewed. The chapter starts with a short description of the different types of mass spectrometric equipment with respect to their suitability for GC/MS coupling. State of the art pesticide multiresidue analysis in water is demonstrated with examples from different pesticide classes. Since the examples in this chapter were mainly produced by the authors group, a survey of recent publications was prepared and is presented in a preceding subchapter. Furthermore, a case story of the elucidation of an unknown contaminant in ground water samples is reported. Finally a software program is described enabling automatic screening of water samples for a multitude of pesticides by searching dedicated pesticide libraries with full scan acquisition

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Author information

Authors and Affiliations

  1. Institute of Food Chemistry, Technical University Berlin, D-13355, Berlin, Germany

    Hans-Jürgen Stan & Thomas Heberer

Authors
  1. Hans-Jürgen Stan
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  2. Thomas Heberer
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Editor information

Editors and Affiliations

  1. Technische Universität Berlin, Gustav-Meyer-Allee 25, D-13355, Berlin, Germany

    H.-J. Stan

  2. Trautenaustraße 8, D-10717, Berlin, Germany

    W. Ebing i.R.

  3. Institut für Phytopathologie, Universität Kiel, Hermann-Rodewald-Str. 9, D-24118, Kiel, Germany

    H. Börner

  4. FG Naturstoffe, Universität Potsdam, Stahnsdorfer Damm 81, D-14532, Kleinmachnow, Germany

    D. Martin

  5. Hoechst Schering AgrEvo GmbH, Postfach 27 06 54, D-13476, Berlin, Germany

    V. Sjut

  6. ZF — FWI, Bayer AG, Q 18, D-51368, Leverkusen, Bayerwerk, Germany

    J. Stetter

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© 1995 Springer-Verlag Berlin Heidelberg

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Stan, HJ., Heberer, T. (1995). Identification and Confirmatory Analysis Based on Capillary GC-Mass Spectrometry. In: Stan, HJ., Ebing i.R., W., Börner, H., Martin, D., Sjut, V., Stetter, J. (eds) Analysis of Pesticides in Ground and Surface Water I. Chemistry of Plant Protection, vol 11. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-03156-8_6

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  • DOI: https://doi.org/10.1007/978-3-662-03156-8_6

  • Publisher Name: Springer, Berlin, Heidelberg

  • Print ISBN: 978-3-662-03158-2

  • Online ISBN: 978-3-662-03156-8

  • eBook Packages: Springer Book Archive

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