Skip to main content
SpringerLink
Log in

Extraction and Cleanup

  • Chapter
Analysis of Pesticides in Ground and Surface Water I

Part of the book series: Chemistry of Plant Protection ((PLANT PROTECTIO,volume 11))

Abstract

Within this chapter numerous techniques and procedures for extraction and cleanup of water samples containing pesticides are presented. These comprise several variations of both the liquid-liquid and the solid phase extraction procedures. Well-known techniques like adsorption chromatography and gel permeation chromatography have been shown to give satisfying results in the cleanup of surface water samples.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Log in via an institution
Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 84.99
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 109.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. Barceló D (1991) Analyst 116: 681

    Article  PubMed  Google Scholar 

  2. Onuska FI (1989) J High Resolut Cromatogr 12: 4

    Article  CAS  Google Scholar 

  3. Namiesnik J, Górecki T, Biziuk M (1990) Anal Chim Acta 237: 1

    Article  CAS  Google Scholar 

  4. Eadie BJ, Morehead NR, Landrum PF (1990) Chemosphere 20: 161

    Article  CAS  Google Scholar 

  5. Hadfield ST, Sadler JK, Bolygo E, Hill IR (1992) Pestic Sci 34: 207

    Article  CAS  Google Scholar 

  6. Sigleo AC, Means JC (1990) Rev Environ Contam Tox 112: 123

    Article  CAS  Google Scholar 

  7. Edgell KW, Jenkins EL, Lopez-Avila V, Longbottom JE (1991) J Assoc Off Anal Chem 74: 295

    PubMed  CAS  Google Scholar 

  8. Davì LM, Baldi M, Penazzi L, Liboni M (1992) Pestic Sci 35: 63

    Article  Google Scholar 

  9. Poole SK, Dean TA, Oudsema JW, Poole CF (1990) Anal Chim Acta 236: 3

    Article  CAS  Google Scholar 

  10. Lopez-Avila V, Wesselman R, Edgell K (1990) J Assoc Off Anal Chem 73: 276

    PubMed  CAS  Google Scholar 

  11. Hinckley DA, Bidleman TF (1989) Environ Sci Technol 23: 995

    Article  CAS  Google Scholar 

  12. Method 525.1 Determination of Organic Compounds in Drinking Water by Liquid-Solid Extraction and Capillary Column Gas Chromatography/Mass Spectrometry (Revision 2.2), Environmental Monitoring Systems Laboratory, Office of Research and Development, U.S. Environmental Protection Agency, Cincinnati, OH USA 45268. Available from: NTIS, 5285 Port Royal, Springfield, VA USA 22161

    Google Scholar 

  13. House WA, Ziqing Ou (1992) Chemosphere 24: 819

    Article  CAS  Google Scholar 

  14. Foster GD, Foreman WT, Gates PM (1991) J Agric Food Chem 39: 1618

    Article  CAS  Google Scholar 

  15. Marvin CH, Brindle ID, Hall CD, Chiba M (1990) Anal Chem 62: 1495

    Article  CAS  Google Scholar 

  16. Borburgh HJ, Hammers WE (1992) Tox Environ Chem 35: 79

    Article  CAS  Google Scholar 

  17. Oppenhuizen ME, Cowell JE (1991) J Assoc Off Anal Chem 74: 317

    PubMed  CAS  Google Scholar 

  18. Wells DE, Kelly AG (1991) Mikrochim Acta (Wien) 111: 23

    Article  Google Scholar 

  19. Liska I, Krupcik J, Leclercq PA (1989) J High Resolut Cromatogr 12: 577

    Article  CAS  Google Scholar 

  20. Johnson WE, Fendinger NJ, Plimmer JR (1991) Anal Chem 63: 1510

    Article  PubMed  CAS  Google Scholar 

  21. Gauch R, Leuenberger U, Müller U (1989) Z Lebensm Unters Forsch 188: 36

    Article  PubMed  CAS  Google Scholar 

  22. Marvin CH, Brindle ID, Singh RP, Hall CD, Chiba M (1990) J Chromatogr 518: 242

    Article  CAS  Google Scholar 

  23. Simmons ND (1991) Brighton Crop Prot Conf — Weeds, Vol. 3, p1259

    Google Scholar 

  24. Landrum PF, Nihart SR, Eadie BJ, Gardner WS (1984) Environ Sci Technol 18: 187

    Article  PubMed  CAS  Google Scholar 

  25. Munch DJ, Graves RL, Maxey RA, Engel TM (1990) Environ Sci Technol 24: 1446

    Article  CAS  Google Scholar 

  26. Schuette SA, Smith RG, Holden LR, Graham JA (1990) Anal Chim Acta 236: 141

    Article  CAS  Google Scholar 

  27. Manes Vinuesa J, Molto Cortés JC, Igualada Canas C, Font Pérez G (1989) J Chromatogr 472: 365

    Article  Google Scholar 

  28. Reupert R, Plöger E, Brausen G (1990) Hewlett–Packard Publ no 12–5952–2229

    Google Scholar 

  29. Bolygó E, Atreya NC (1991) Fresenius J Anal Chem 339: 423

    Article  Google Scholar 

  30. Ahmad I (1983) J Environ Sci Health B18: 207

    Article  CAS  Google Scholar 

  31. Fielding M, Gibby S, Moore K (1991) In: Angeletti G, Björseth A (eds) Organic micropollutants in the aquatic environment: proceedings of the 6th European symposium, 1990. Kluwer, Dordrecht, p 142

    Chapter  Google Scholar 

  32. Von Böer G, Schlett C, Thier H-P (1990) Z Wasser-Abwasser-Forsch 23: 220

    Google Scholar 

  33. Akerblom M (1985) J Chromatogr 319: 427

    Article  PubMed  CAS  Google Scholar 

  34. Dedek W, Weil L, Feistel L (1992) Vom Wasser 78: 155

    CAS  Google Scholar 

  35. Leggett DC, Jenkins TF, Miyares PH (1990) Anal Chem 62: 1355

    Article  CAS  Google Scholar 

  36. Baumgarten D, Pfrang I (1989) GIT Fachz Lab 9: 815

    Google Scholar 

  37. Crepeau KL, Walker G, Winterlin W (1991) Bull Environ Contam Toxicol 46: 512

    Article  PubMed  CAS  Google Scholar 

  38. Di Corcia A, Marchetti M (1992) Environ Sci Technol 26: 66

    Article  Google Scholar 

  39. Andersson A, Ohlin B (1986) Vär Föda 38 Suppl 2: 79

    Google Scholar 

  40. Norris LA (1986) Weed Sci 34: 485

    CAS  Google Scholar 

  41. Weil L, Niessner R (1991) Nachr Chem Tech Lab 39: 1277

    Article  CAS  Google Scholar 

  42. Scharf J, Wiesiollek R, Bächmann K (1992) Fresenius J Anal Chem 342: 813

    Article  CAS  Google Scholar 

  43. Lee HB, Peart TE, Carron JM, Tse H (1991) J Assoc Off Anal Chem 74: 835

    CAS  Google Scholar 

  44. Vogelgesang J (1991) Fresenius J Anal Chem 340: 384

    Article  CAS  Google Scholar 

  45. Munch DJ, Frebis CP (1992) Environ Sci Technol 26: 921

    Article  CAS  Google Scholar 

  46. Durand G, Barceló D (1989) Tox Environ Chem 25: 1

    Article  CAS  Google Scholar 

  47. Baumgarten D, Pfrang I (1989) GIT Supplement 3: 80

    Google Scholar 

  48. Geissler A, Schöler HF (1991) Chemosphere 23: 1029

    Article  CAS  Google Scholar 

  49. Harrington-Fowler L (1991) American Laboratory August 1991: 39

    Google Scholar 

  50. Schoeler HF, Brodesser J (1988) In: Angeletti G, Björseth A (eds) Organic micropollutants in the aquatic environment: proceedings of the 5th European symposium, 1987. Kluwer, Dordrecht

    Google Scholar 

  51. Färber H, Peldszus S, Schöler HF (1991) Vom Wasser 76: 13

    Google Scholar 

  52. Färber H, Schöler HF (1991) Vom Wasser 77: 249

    Google Scholar 

  53. Van Hoof F, Ackermans P, Wauters M (1991) In: Angeletti G, Björseth A (eds) Organic micropollutants in the aquatic environment: proceedings of the 6th European symposium, 1990. Kluwer, Dordrecht, p 315

    Chapter  Google Scholar 

  54. Dix KD, Fritz JS (1990) Anal Chim Acta 236: 43

    Article  CAS  Google Scholar 

  55. Hemmerling C, Risto C, Augustyniak B, Jenner K (1991) Die Nahrung 35: 711

    Article  PubMed  CAS  Google Scholar 

  56. Legrand MF, Costentin E, Bruchet A (1991) Environ Technol 12: 985

    Article  CAS  Google Scholar 

  57. Foster GD, Rogerson PF (1990) Int J Environ Anal Chem 41: 105

    Article  CAS  Google Scholar 

  58. Gregor DJ (1990) In: Kurtz DA (ed) Long range transport of pesticides. Lewis, Chelsea, p 373

    Google Scholar 

  59. Clement RE, Suter SA, Tosine HM (1989) Chemosphere 18: 133

    Article  Google Scholar 

  60. van der Hoff GR, Gort SM, Baumann RA, van Zoonen P, Brinkman UAT (1991) J High Resolut Cromatogr 14: 465

    Article  Google Scholar 

  61. Potter TL, Carpenter T, Putnam R, Reddy K, Clark JM (1991) J Agric Food Chem 39: 2184

    Article  CAS  Google Scholar 

  62. Goosens EC, Bunschoten RG, Engelen V, de Jong D, van den Berg JHM (1990) J High Resolut Cromatogr 13: 438

    Article  CAS  Google Scholar 

  63. Farran A, Cortina JL, De Pablo J, Barceló D (1990) Anal Chim Acta 234: 119

    Article  CAS  Google Scholar 

  64. van Zoonen P, Hogendoorn EA, van der Hoff GR, Baumann RA (1992) Trends Anal Chem 11: 11

    Article  Google Scholar 

  65. Wigfield YY, Lanouette M (1990) Anal Chim Acta 233: 311

    Article  CAS  Google Scholar 

  66. Pack DE (1967) In: Zweig G (ed) Analytical methods for pesticides, plant growth regulators and food additives, vol. 5. Academic Press, New York, p 397 and p 473

    Google Scholar 

  67. Di Corcia A, Marchetti M (1991) Anal Chem 63: 580

    Article  PubMed  Google Scholar 

  68. Coquart V, Hennion M-C (1991) J Chromatogr 553: 329

    Article  CAS  Google Scholar 

  69. Battista M, Di Corcia A, Marchetti M (1989) Anal Chem 61: 935

    Article  PubMed  CAS  Google Scholar 

  70. Di Corcia A, Marchetti M, Samperi R (1989) Anal Chem 61: 1363

    Article  Google Scholar 

  71. Hagenguth M, München (1992) personal communication

    Google Scholar 

  72. Hagen DF, Markel CG, Schmitt GA (1990) Anal Chim Acta 236: 157

    Article  CAS  Google Scholar 

  73. Brouwer ER, Lingeman H, Brinkman UAT (1990) Chromatographia 29: 415

    Article  CAS  Google Scholar 

  74. Brouwer ER, Van Iperen DJ, Liska I, Lingeman H, Brinkman UAT (1992) Int J Environ Anal Chem 47: 257

    Article  CAS  Google Scholar 

  75. Yoo LJ, Shen Y, Fitzsimmons S (1992) Proc Water Qual Technol Conf 1991, Pt 2, 913

    Google Scholar 

  76. Thoma JJ, Kraut A, George JE, Day RS (1992) Proc Water Qual Technol Conf 1991, Pt 2, p 851

    Google Scholar 

  77. Junk GA, Avery MJ, Richard JJ (1988) Anal Chem 60: 1347

    Article  CAS  Google Scholar 

  78. Molto JC, Picó Y, Font G, Manes J (1991) J Chromatogr 555: 137

    Article  PubMed  CAS  Google Scholar 

  79. Thier H-P, Zeumer H (eds) (1991) Rückstandsanalytik von Pflanzenschutzmitteln/DFG. VCH Verlagsgesellschaft, Weinheim

    Google Scholar 

  80. Dalbacke J, Dahlquist I, Persson C (1990) J Chromatogr 507: 381

    Article  PubMed  CAS  Google Scholar 

  81. Nash RG (1990) J Assoc Off Anal Chem 73: 438

    PubMed  CAS  Google Scholar 

  82. Mangani F, Crescentini G, Palma P, Bruner F (1988) J Chromatogr 452: 527

    Article  CAS  Google Scholar 

  83. Brooks MW, Jenkins J, Jimenez M, Quinn T, Clark JM (1989) Analyst 114: 405

    Article  PubMed  CAS  Google Scholar 

  84. Benfenati E, Tremolada P, Chiappetta L, Frassanito R, Bassi G, Di Toro N, Fanelli R, Stella G (1990) Chemosphere 21: 1411

    Article  CAS  Google Scholar 

  85. Junk GA, Richard JJ (1988) Anal Chem 60: 451

    Article  CAS  Google Scholar 

  86. Howard AL, Taylor LT (1992) J Chrom Sci 30: 374

    CAS  Google Scholar 

  87. Ho JS, Tang PH (1992) J Chrom Sci 30: 344

    CAS  Google Scholar 

  88. Alberti J, Willemsen H-G (1989) Forum Städte-Hygiene 40: 118

    CAS  Google Scholar 

  89. Seiber JN, Glotfelty DE, Lucas AD, McChesney MM, Sagebiel JC, Wehner TA (1990) Arch Environ Contam Toxicol 19: 583

    Article  PubMed  CAS  Google Scholar 

  90. Mattern GC, Louis JB, Rosen JD (1991) J Assoc Off Anal Chem 74: 982

    CAS  Google Scholar 

  91. Geerdink RB, Van Balkom CAA, Brouwer H-J (1989) J Chromatogr 481: 275

    Article  PubMed  CAS  Google Scholar 

  92. Subra P, Hennion M-C, Rosset R, Frei RW (1989) Intern J Environ Anal Chem 37: 45

    Article  CAS  Google Scholar 

  93. Subra P, Hennion M-C, Rosset R, Frei RW (1988) J Chromatogr 456: 121

    CAS  Google Scholar 

  94. Dedek W, Wenzel K-D, Luft F, Oberländer H, Mothes B (1987) Fresenius Z Anal Chem 328: 484

    Article  CAS  Google Scholar 

  95. Dedek W, Wenzel K-D, Oberländer H, Mothes B, Männig J (1991) Fresenius J Anal Chem 339: 201

    Article  CAS  Google Scholar 

  96. Ramsteiner KA (1989) J Chromatogr 465: 410

    Article  CAS  Google Scholar 

  97. Marvin CH, Brindle ID, Hall CD, Chiba M (1991) J Chromatogr 555: 147

    Article  PubMed  CAS  Google Scholar 

  98. Reupert R, Zube I, Plöger E (1992) LC-GC Intl 5 (6): 43

    Google Scholar 

  99. Liska I, Brouwer ER, Ostheimer AGL, Lingeman H, Brinkman UAT, Geerdink RB, Mulder WH (1992) Int J Environ Anal Chem 47: 267

    Article  CAS  Google Scholar 

  100. Kwakman PJM, Vreuls JJ, Brinkman UAT, Ghijsen RT (1992) Chromatographia 34: 41

    Article  CAS  Google Scholar 

  101. Arthur CL, Potter DW, Buchholz KD, Motlagh S, Pawliszyn J (1992) LC-GC 5 (10): 8

    Google Scholar 

  102. Louch D, Motlagh S, Pawliszyn J (1992) Anal Chem 64: 1187

    Article  CAS  Google Scholar 

  103. DiGiano FA, Elliot D, Leith D (1988) Environ Sci Technol 22: 1365

    Article  CAS  Google Scholar 

  104. Kaiser RE, Rieder R (1989) J Chromatogr 477: 49

    Article  CAS  Google Scholar 

  105. LeBel GL, Williams DT, Griffith G, Benoit FM (1979) J Assoc Off Anal Chem 62: 241

    PubMed  CAS  Google Scholar 

  106. Green DR, Stull JK, Heesen TC (1986) Mar Pollut Bull 17: 324

    Article  CAS  Google Scholar 

  107. Ahnoff M, Josefsson B (1974) Anal Chem 46: 658

    Article  CAS  Google Scholar 

  108. Gómez-Belinchón JI, Grimalt JO, Albaigés J (1988) Environ Sci Technol 22: 677

    Article  Google Scholar 

  109. Strachan WMJ, Huneault H (1984) Environ Sci Technol 18: 127

    Article  PubMed  CAS  Google Scholar 

  110. Nilvé G, Audunsson G, Jönsson JA (1989) J Chromatogr 471: 151

    Article  Google Scholar 

  111. Nilvé G, Stebbins R (1991) Chromatographia 32: 269

    Article  Google Scholar 

  112. Nilvé G (1992) Sample pretreatment methods for determination of acidic herbicides in water, with special emphasis on supported liquid membranes Thesis, Lund University, Lund, Sweden

    Google Scholar 

  113. Mathiasson L, Nilvé G, Ulén B (1991) Intern J Environ Anal Chem 45: 117

    Article  CAS  Google Scholar 

  114. Thier H-P, Zeumer H (eds) (1987) Manual of pesticide residue analysis/DFG. VCH Verlagsgesellschaft, Weinheim

    Google Scholar 

  115. Reichert JK, Lochtman J, Huschens 0 (1991) Gewässerschutz, Wasser, Abwasser 125: 568

    Google Scholar 

  116. Gill R, Qua SC, Moffat AC (1983) J Chromatogr 255: 483

    Article  PubMed  CAS  Google Scholar 

  117. Akerblom M (1990) Bull Environ Contam Toxicol 45: 157

    Article  PubMed  CAS  Google Scholar 

  118. Debets AJJ, Hupe K-P, Kok WT, Brinkman UAT (1992) J Chromatogr 600: 163

    Article  CAS  Google Scholar 

  119. Hogendoorn EA, van Zoonen P, Brinkman UAT (1991) Chromatographia 31: 285

    Article  CAS  Google Scholar 

  120. Lopez-Avila V, Dodhiwala NS, Milanes J, Beckert WF (1989) J Assoc Off Anal Chem 72: 593

    CAS  Google Scholar 

  121. Specht W, Tillkes M (1985) Fresenius Z Anal Chem 322: 443

    Article  CAS  Google Scholar 

  122. de la Vigne U, Jänchen DE, Weber WH (1991) J Chromatogr 553: 489

    Article  PubMed  Google Scholar 

  123. Cubero Ferradal F, Rodriguez Procopio J, Hernandez Hernandez L (1992) Fresenius J Anal Chem 343: 382

    Article  Google Scholar 

  124. Seiber JN, McChesney MM, Kon R, Leavitt RA (1984) J Agric Food Chem 32: 678

    Article  CAS  Google Scholar 

  125. Hogendoorn EA, de Jong APJM, van Zoonen P, Brinkman UAT (1990) J Chromatogr 511: 243

    Article  CAS  Google Scholar 

  126. Hogendoorn EA, Brinkman UAT, van Zoonen P (1991) Poster presented at: 3rd Workshop on chemistry and fate of modern pesticides, 4–6 Sept 1991, Int Ass Env Anal Chem

    Google Scholar 

  127. Akerblom M, Thorén L, Staffas A (1990) Vär Föda 42: 236

    Google Scholar 

  128. Durand G, Forteza R, Barceló D (1989) Chromatographia 28: 597

    Article  CAS  Google Scholar 

  129. Barceló D, Solé M, Durand G, Albaigés J (1991) Fresenius J Anal Chem 339: 676

    Article  Google Scholar 

  130. Murphy PG (1972) J Assoc Off Anal Chem 55: 1360

    PubMed  CAS  Google Scholar 

  131. Bernal JL, Del Nozal MJ, Jiménez JJ (1992) J Chromatogr 607: 303

    Article  CAS  Google Scholar 

  132. Bellar TA, Budde WL (1988) Anal Chem 60: 2076

    Article  CAS  Google Scholar 

  133. Ahmed AW, Mallet VN, Bertrand MJ (1989) J Assoc Off Anal Chem 72: 365

    PubMed  CAS  Google Scholar 

  134. Cotterill EG (1992) Pestic Sci 34: 291

    Article  CAS  Google Scholar 

  135. Åkerblom M (1990) Pesticide residue analysis with special reference to ion pairing techniques. Thesis, Swedish Univ of Agr Sci, Uppsala, Sweden

    Google Scholar 

  136. Bogus ER, Watschke TL, Mumma RO (1990) J Agric Food Chem 38: 142

    Article  CAS  Google Scholar 

Download references

Author information

Authors and Affiliations

  1. Department of Environmental Assessment, Swedish University of Agricultural Sciences, Box 7050, S-75007, Swedish

    Malin Åkerblom

Authors
  1. Malin Åkerblom
    View author publications

    You can also search for this author in PubMed Google Scholar

Editor information

Editors and Affiliations

  1. Technische Universität Berlin, Gustav-Meyer-Allee 25, D-13355, Berlin, Germany

    H.-J. Stan

  2. Trautenaustraße 8, D-10717, Berlin, Germany

    W. Ebing i.R.

  3. Institut für Phytopathologie, Universität Kiel, Hermann-Rodewald-Str. 9, D-24118, Kiel, Germany

    H. Börner

  4. FG Naturstoffe, Universität Potsdam, Stahnsdorfer Damm 81, D-14532, Kleinmachnow, Germany

    D. Martin

  5. Hoechst Schering AgrEvo GmbH, Postfach 27 06 54, D-13476, Berlin, Germany

    V. Sjut

  6. ZF — FWI, Bayer AG, Q 18, D-51368, Leverkusen, Bayerwerk, Germany

    J. Stetter

Rights and permissions

Reprints and permissions

Copyright information

© 1995 Springer-Verlag Berlin Heidelberg

About this chapter

Cite this chapter

Åkerblom, M. (1995). Extraction and Cleanup. In: Stan, HJ., Ebing i.R., W., Börner, H., Martin, D., Sjut, V., Stetter, J. (eds) Analysis of Pesticides in Ground and Surface Water I. Chemistry of Plant Protection, vol 11. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-662-03156-8_3

Download citation

  • DOI: https://doi.org/10.1007/978-3-662-03156-8_3

  • Publisher Name: Springer, Berlin, Heidelberg

  • Print ISBN: 978-3-662-03158-2

  • Online ISBN: 978-3-662-03156-8

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics

Search

Navigation