Abstract
The reaction-scheme is shown in Figure 16. The product was prepared according to the reported procedure [37]. 3-Bromothiophene (16.048 g, 98.41 mmol) is dissolved in 120 mL of freshly distilled n-hexane in a threeneck roundflask and cooled down to -55。C. 40 mL (100 mmol) of 2.5 M nbuthyllithium solution in hexane are added dropwise in about 15 minutes.
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© 2015 Springer Fachmedien Wiesbaden
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Weichselbaumer, M. (2015). Results and Discussion. In: Pyridine-functionalized Polymeric Catalysts for CO2-Reduction. BestMasters. Springer Spektrum, Wiesbaden. https://doi.org/10.1007/978-3-658-10358-3_3
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DOI: https://doi.org/10.1007/978-3-658-10358-3_3
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