Skip to main content
  • 153 Accesses

Abstract

In the following sections the basic multipulse NMR techniques used in the exercises are introduced. The emphasis, however, is not on the physical description and explanation of the pulse sequences, but on the practical evaluation of the spectra and their importance in structural elucidation.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 74.99
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Preview

Unable to display preview. Download preview PDF.

Unable to display preview. Download preview PDF.

References

  1. Ernst RR, Bodenhausen G, Wokaun A (1986; 2nd ed. 1987) Principles of Nuclear Magnetic Resonance in One and Two Dimensions. Oxford University Press, Oxford.

    Google Scholar 

  2. Kessler H, Gehrke M, Griesinger C (1988) Angew Chem 100: 507;

    Article  CAS  Google Scholar 

  3. Kessler H, Gehrke M, Griesinger C (1988) Angew Chem Int Ed Engl 27: 490.

    Article  Google Scholar 

  4. 1. Günther H (1983) NMR-Spektroskopie, 2nd ed. Thieme, Stuttgart, p 264;

    Google Scholar 

  5. 1a Günther H (1983) NMR Spectroscopy — An Introduction. Wiley, Chichester, p 282.

    Google Scholar 

  6. Barrett MW, Farrant RD, Kirk DN, Mersh JD, Sanders JKM, Duax WL (1982) J Chem Soc Perkin Trans 2:105.

    Google Scholar 

  7. Schneider H-J, Buchheit U, Becker N, Schmidt G, Siehl U (1985) J Am Chem Soc 107:7027.

    Article  CAS  Google Scholar 

  8. Duddeck H, Rosenbaum D, Elgamal MHA, Fayez MBE (1986) Magn Reson Chem 24:999.

    Article  CAS  Google Scholar 

  9. Croasmun WR, Carlson RMK (1987) Two-Dimensional NMR Spectroscopy, Applications for Chemists and Biochemists. VCH Publishers, New York, p 387.

    Google Scholar 

  10. Noggle JH, Schirmer RE (1971) The Nuclear Overhauser Effect. Academic Press, New York.

    Google Scholar 

  11. For modern multipulse 1H broadband decoupling methods see Shaka AJ, Keeler J (1987) Prog NMR Spectrosc 19:47.

    Article  CAS  Google Scholar 

  12. Kalinowski H-O, Berger S, Braun S (1984) 13C-NMR-Spektroskopie. Thieme, Stuttgart, p 46.

    Google Scholar 

  13. Günther H (1973) NMR spectroscopy — an introduction. Wiley, Chichester, p 310, 359.

    Google Scholar 

  14. Benn R, Günther H (1983) Angew Chem 95: 381

    Article  CAS  Google Scholar 

  15. 4.a Benn R, Günther H (1983) Angew Chem Int Ed Engl 22: 350;

    Article  Google Scholar 

  16. 4.b Benn R, Günther H Sanders JKM, Hunter BK (1987) Modem NMR spectroscopy — a guide for chemists. Oxford University Press, Oxford, p 69.

    Google Scholar 

  17. Bendall MR, Doddrell DM, Pegg DT, Hull WE (1983) High resolution multipulse NMR spectrum editing and DEPT. Bruker brochure; Derome AE (1987) Modern NMR techniques for chemistry research. Pergamon Press, Oxford, p 143.

    Google Scholar 

  18. Bax A (1984) J Magn Reson 57: 314.

    Article  CAS  Google Scholar 

  19. Von Philipsbom W (1971) Angew Chem 83: 470;

    Google Scholar 

  20. Von Philipsbom W (1971) Angew Chem Int Ed Engl 10: 472.

    Article  Google Scholar 

  21. Noggle JH, Schirmer RE (1971) The Nuclear Overhauser Effect. Academic Press, New York.

    Google Scholar 

  22. Günther H (1973) NMR spectroscopy — an introduction. Wiley, Chichester, p 299.

    Google Scholar 

  23. Kalinowski H-O, Berger S, Braun S (1984) 13C-NMR-Spektroskopie. Thieme, Stuttgart, pp 44, 566.

    Google Scholar 

  24. Ried W, Urlass G (1953) Chem Ber 86: 1101; Snatzke G, Malik F, Duddeck H (1987)(to be published).

    Article  CAS  Google Scholar 

  25. Martin ML, Martin GJ, Delpuech J-J (1980) Practical NMR spectroscopy. Heyden, London, p 222;

    Google Scholar 

  26. Derome AE (1987) Modern NMR techniques for chemistry research. Pergamon Press, Oxford, p 130.

    Google Scholar 

  27. Ernst RR, Bodenhausen G, Wokaun A (1986; 2nd ed. 1987) Principles of nuclear magnetic resonance in one and two dimensions. Oxford University Press, p 516.

    Google Scholar 

  28. Berm R, Günther H (1983)Angew Chem 95: 381

    Google Scholar 

  29. Berm R, Günther H (1983)Angew Chem Int Ed Engl 22: 350.

    Article  Google Scholar 

  30. Derome AE (1987) Modern NMR techniques for chemistry research. Pergamon Press, Oxford.

    Google Scholar 

  31. Sanders JKM, Hunter BK (1987) Modern NMR spectroscopy — a guide for chemists. Oxford University Press, Oxford.

    Google Scholar 

  32. Duddeck H, Kaiser M (1985) Spectrochim Acta 41A: 913.

    CAS  Google Scholar 

  33. Ernst RR, Bodenhausen G, Wokaun A (1986; 2nd ed. 1987) Principles of nuclear magnetic resonance in one and two dimensions. Oxford University Press, Oxford, p 434.

    Google Scholar 

  34. Benn R, Günther H (1983) Angew Chem 95:381;

    Article  CAS  Google Scholar 

  35. Benn R, Günther H (1983) Angew Chem Int Ed Engl 22:350.

    Article  Google Scholar 

  36. Derome AE (1987) Modern NMR techniques for chemistry research. Pergamon Press, Oxford.

    Google Scholar 

  37. Sanders JKM, Hunter BK (1987) Modern NMR spectroscopy — a guide for chemists. Oxford University Press, Oxford.

    Google Scholar 

  38. Günther H (1973) NMR spectroscopy — an introduction. Pergamon Press.

    Google Scholar 

  39. Duddeck H (1983) Tetrahedron 39:1365.

    Article  CAS  Google Scholar 

  40. Ernst RR, Bodenhausen G, Wokaun A (1986; 2nd ed 1987) Principles of nuclear magnetic resonance in one and two dimensions. Oxford University Press, Oxford, p 479.

    Google Scholar 

  41. Kessler H, Griesinger C, Zarbock J, Looslie HR (1984) J Magn Reson 57: 331.

    Article  CAS  Google Scholar 

  42. Breitmaier E, Voelter W (3rd ed 1987) 13C NMR spectroscopy. Verlag Chemie, Weinheim, New York.

    Google Scholar 

  43. Benn R, Günther H (1983) Angew Chem 95: 381;

    Article  CAS  Google Scholar 

  44. Benn R, Günther H (1983) Angew Chem Int Ed Engl 22: 350.

    Article  Google Scholar 

  45. Derome A E (1987) Modern NMR Techniques for Chemistry Research. Pergamon Press, Oxford, p 234.

    Google Scholar 

  46. Buddrus J, Bauer H (1987) Angew Chem 99: 642;

    Article  CAS  Google Scholar 

  47. Buddrus J, Bauer H (1987) Angew Chem Int Ed Engl 26: 625.

    Article  Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

Copyright information

© 1989 Dr. Dietrich Steinkopff Verlag GmbH & Co. KG, Darmstadt

About this chapter

Cite this chapter

Duddeck, H., Dietrich, W. (1989). Methodology. In: Structure Elucidation by Modern NMR. Steinkopff. https://doi.org/10.1007/978-3-642-97781-7_2

Download citation

  • DOI: https://doi.org/10.1007/978-3-642-97781-7_2

  • Publisher Name: Steinkopff

  • Print ISBN: 978-3-7985-0787-6

  • Online ISBN: 978-3-642-97781-7

  • eBook Packages: Springer Book Archive

Publish with us

Policies and ethics