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High-Resolution Electron Microscopy in Surface Science

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Part of the book series: Springer Series in Surface Sciences ((SSSUR,volume 5))

Abstract

A wide variety of diffraction, spectroscopy, and microscopy techniques are now available for the characterisation of surfaces, but only the microscopical methods, primarily using electrons, are able to provide direct real-space information about local inhomogeneities such as surface steps, terraces, domains, and defects. As a consequence of technical improvements, high-resolution electron microscopes in particular are nowadays capable of atomic imaging, and electron microscopists are already starting to utilise this capability in their studies of surfaces. Subnanometer surface detail can be resolved in the reflection imaging mode and atomic-scale features are visible in the transmission and profile imaging modes. The results already available indicate that these high-resolution electron microscopy (HREM) techniques should be indispensable to obtaining a detailed understanding of many surfaces and their macroscopic properties.

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References

  1. J.A. Venables: Ultramicroscopy 7, 82 (1981)

    Google Scholar 

  2. J.A. Venables, D.R. Batchelor, M. Hanbuchen, C.J. Harland, G.W. Jones: In press

    Google Scholar 

  3. J.M. Cowley: Diffraction Thy sics, 2nd Ed. (North-Holi and, Amsterdam 1981)

    Google Scholar 

  4. J.C.H. Spence: Experimental High Resolution Electron Microscopy (Clarendon, Oxford 1981)

    Google Scholar 

  5. D.J. Smith: Helv. Phys. Acta 56, 463 (1983)

    CAS  Google Scholar 

  6. G. Lehmpfuhl, Y. Uchida: Ultramicroscopy 4, 275 (1979)

    CAS  Google Scholar 

  7. M. Klaua, H. Bethge: Ultramicroscopy 11, 125 (1983)

    Google Scholar 

  8. K. Takayanagi, K. Kobayashi, Y. Kodaira, Y. Yokoyama, K. Yagi: In Proc. 7th Int. Conf. HVEM, ed. by R.M. Fisher, R. Gronsky, K. Westmacott (Lawrence Berkeley Laboratory, Berkeley 1983) p.47

    Google Scholar 

  9. D.F. Lynch: Acta Crystallogr., Sect. A27, 299 (1971)

    Google Scholar 

  10. D. Cherns: Philos. Mag. 30, 549 (1974)

    CAS  Google Scholar 

  11. J.C.H. Spence: “Developments in Electron Microscopy and Analysis”, Inst. Phys. Conf. Ser. 32, 257 (1975)

    Google Scholar 

  12. W. Krakow, D.G. Ast: Surf. Sci. 58, 485 (1976)

    CAS  Google Scholar 

  13. P. Goodman, A.F. Moodie: Acta Crystallogr., Sect. A30, 280 (1974)

    Google Scholar 

  14. W. Krakow: Ultramicroscopy 4, 55 (1979)

    CAS  Google Scholar 

  15. L.D. Marks, D.J. Smith: Nature (London) 303, 316 (1983)

    CAS  Google Scholar 

  16. K. Kambe, G. Lehmpfuhl: Optik (Stuttgart) 42, 187 (1975)

    CAS  Google Scholar 

  17. Tung Hsu, J.M. Cowley: Ultramicroscopy 11, 239 (1983)

    CAS  Google Scholar 

  18. Tung Hsu: Ultramicroscopy 11, 167 (1983)

    CAS  Google Scholar 

  19. Y. Uchida, G. Lehmpfuhl, J. Jager: Ultramicroscopy 15, 119 (1984)

    CAS  Google Scholar 

  20. D.J. Smith: J. Vac. Sci. Technol. B3, 1563 (1985)

    Google Scholar 

  21. K. Takayanagi, K. Yagi, K. Kobayashi, G. Honjo: J. Phys. E11, 441 (1978)

    Google Scholar 

  22. P. Atkin, K.C.A. Smith: In Electron Microscopy 1982, Vol.1 (Deutsche Gesellschaft für Elektronenmikroskopie e.V., Frankfurt 1982) p.525

    Google Scholar 

  23. J.M. Cowley: Surf. Sci. 114, 587 (1982)

    CAS  Google Scholar 

  24. O.L. Krivanek, Y. Tanishiro, K. Takayanagi, K. Yagi: Ultramicroscopy 11, 215 (1983)

    CAS  Google Scholar 

  25. N.J. Long, A.K. Petford: Unpublished results

    Google Scholar 

  26. L.D. Marks, D.J. Smith: Surf. Sci. 143, 495 (1984)

    CAS  Google Scholar 

  27. D.J. Smith, L.A. Bursill: Ultramicroscopy 17, 387 (1985)

    CAS  Google Scholar 

  28. R.J. Wilson, P.M. Petroff: Rev. Sci. Instrum. 54, 1534 (1983)

    CAS  Google Scholar 

  29. G. Honjo, K. Yagi, K. Takayanagi, S. Nagakura, S. Katagiri, M. Kubozoe, I. Matsui: In Electron Microscopy 1980, Antwerp 1980, Vol.4, ed. by P. Brederoo, J. van Landuyt (Seventh European Congress on Electron Microscopy Foundation, Leiden 1980) p.22

    Google Scholar 

  30. A.F. Moodie, C.E. Warble: Philos. Mag. 16, 891 (1967)

    CAS  Google Scholar 

  31. A.F. Moodie, C.E. Warble: J. Cryst. Growth 10, 26 (1971)

    CAS  Google Scholar 

  32. G. Lehmpfuhl, Y. Uchida: In Proc. 37th Annu. Meet. EMSA, San Antonio 1979, ed. by G.W. Bailey (Claitors, Baton Rouge, LA 1979) p.208

    Google Scholar 

  33. G. Lehmpfuhl, Y. Uchida: Inst. Phys. Conf. Ser. 52, 393 (1980)

    Google Scholar 

  34. L.A. Bursill: Chem. Scr. 14, 83 (1978–1979)

    Google Scholar 

  35. S. Iijima: Ultramicroscopy 6, 41 (1981)

    CAS  Google Scholar 

  36. Y. Uchida, G. Lehmpfuhl, U. Klengler: In Electron Microscopy 1982, Vol.2 (Deutsche Gesellschaft fur Elektronenmikroskopie e.V., Frankfurt 1982) p.289

    Google Scholar 

  37. P. Petroff: Mat. Res. Soc. Symp. Proc. 31, 117 (1984)

    CAS  Google Scholar 

  38. S. Iijima: Optik (Stuttgart) 47, 437 (1977)

    CAS  Google Scholar 

  39. S. Iijima, Tung Hsu: In Proc. 38th Annu. Meet. EMSA, Reno 1980, ed. by G.W. Bailey (Claitors, Baton Rouge, LA 1980) p.376

    Google Scholar 

  40. W. Krakow, G. Trafas: In Proc 39th Annu. Meet. EMSA, Atlanta 1981, ed. by G.W. Bailey (Claitors, Baton Rouge, LA 1981) p.20

    Google Scholar 

  41. W. Krakow: Surf. Sci. Ill, 503 (1981)

    Google Scholar 

  42. W. Krakow: Thin Solid Films 93, 235 (1982)

    CAS  Google Scholar 

  43. G. Nihoul, K. Abdelmoula, J.J. Metois: Ultramicroscopy 12, 353 (1984)

    Google Scholar 

  44. G. Lehmpfuhl, K. Takayanagi: Ultramicroscopy 6, 195 (1981)

    CAS  Google Scholar 

  45. K. Takayanagi: Jpn. J. Appl, Phys. 22, L4 (1983)

    Google Scholar 

  46. K. Takayanagi, K. Yagi: Trans. Jpn. Inst. Met. 24, 337 (1983)

    CAS  Google Scholar 

  47. W. Krakow: Mat. Res. Soc. Symp. Proc. 31, 189 (1984)

    CAS  Google Scholar 

  48. W. Krakow: Surf. Sci. 140, 137 (1984)

    CAS  Google Scholar 

  49. J.M. Cowley, Z.C. Kang: Ultramicroscopy 11, 131 (1983)

    CAS  Google Scholar 

  50. C.E. Warble, J.M. Cowley: In Proc. 41st Annu. Meet. EMSA, Phoenix 1983, ed. by G.W. Bailey (San Francisco Press, San Francisco 1983) p.319

    Google Scholar 

  51. E.A. Lodge, J.M. Cowley: Ultramicroscopy 13, 213 (1984)

    Google Scholar 

  52. Y. Uchida, G. Lehmpfuhl, F. Fujimoto: In 4th Int. Conf. HVEM, Toulouse 1975, ed. by B. Jouffrey, P. Favard (Societe Francaise de Microscopie Electronique, Paris 1976) p.113

    Google Scholar 

  53. P.J.F. Levitt, A. Howie: J. Microsc. (Oxford) 116, 89 (1979)

    CAS  Google Scholar 

  54. K. Yagi, K. Takayanagai, K. Kobayashi, N. Osakabe, Y. Tanishiro, G. Honjo: Surf. Sci. 86, 174 (1979)

    CAS  Google Scholar 

  55. C.J. Roussouw, S.E. Donnelly, D.F. Lynch: Ultramicroscopy 16, 41 (1985)

    Google Scholar 

  56. K. Takayanagi: J. Microsc. (Oxford) 136, 287 (1984)

    CAS  Google Scholar 

  57. J.C. Heyraud, J.J. Metois: Surf. Sci. 100, 519 (1980)

    CAS  Google Scholar 

  58. Y. Tanishiro, H. Kanamori, K. Takayanagi, K. Yagi, G. Honjo: Surf. Sci. 111, 395 (1981)

    CAS  Google Scholar 

  59. D. Cherns, F.J. Minter, R.S. Nelson: Nucl. Instrum. Methods 136, 369 (1976)

    Google Scholar 

  60. D. Cherns: Philos. Mag. 36, 1429 (1977)

    CAS  Google Scholar 

  61. K. Takayanagi: Surf. Sci. 104, 527 (1981)

    CAS  Google Scholar 

  62. K. Takayanagi, H. Kanamori, Y. Tanishiro, K. Yagi: Acta Crystallogr., Sect. A37, C-300 (1981)

    Google Scholar 

  63. K. Takayanagi: Ultramicroscopy 8, 145 (1982)

    CAS  Google Scholar 

  64. K. Takayanagi, Y. Tanishiro, M. Takahashi, S. Takahashi: J. Vac. Sci. Technol. A3, 1502 (1985)

    Google Scholar 

  65. P. Petroff, R.J. Wilson: Phys. Rev. Lett. 51, 199 (1983)

    CAS  Google Scholar 

  66. J.W. Menter: J. Photogr. Sci. 1, 12 (1953)

    Google Scholar 

  67. P.E. Hojlund-Nielsen, J.M. Cowley: Surf. Sci. 54, 340 (1976)

    Google Scholar 

  68. J.D. Landry, G.G. Hembree, P.E. Hojlund-Neilsen, J.M. Cowley: In Scanning Electron Microscopy/1976, ed. by O. Johari (11TRI, Chicago 1976) p.239

    Google Scholar 

  69. T. Hsu, J.M. Cowley: In The Structure of Surfaces, ed. by M.A. Van Hove, S.Y. Tong, Springer Ser. Surf. Sci., Vol.2 (Springer, Berlin, Heidelberg 1985) p.55

    Google Scholar 

  70. Z.C. Kang: J. Micr. Spectr. Electron. 7, 33 (1982)

    CAS  Google Scholar 

  71. Tung Hsu, S. Iijima: Electron Microscopy 1982, Vol.1 (Deutsche Gesellschaft für Elektronenmikroskopie e.V., Frankfurt 1982) p.301

    Google Scholar 

  72. Y. Uchida, J. Jager, G. Lehmpfuhl: Ultramicroscopy 13, 325 (1984)

    CAS  Google Scholar 

  73. S. Iijima, Tung Hsu: Electron Microscopy 1982, Vol.l (Deutsche Gesellschaft für Elektronenmikroskopie e.V., Frankfurt 1982) p.293

    Google Scholar 

  74. T. Hsu, S. Iijima, J.M. Cowley: Surf. Sci. 137, 551 (1984)

    CAS  Google Scholar 

  75. N. Yamamoto, J.C.H. Spence: Thin Solid Films 104, 43 (1983)

    CAS  Google Scholar 

  76. N. Yamamoto, S. Muto: Jpn. J. Appl. Phys. 23, 2804 (1984)

    Google Scholar 

  77. B.C. Coonan, K.-H. Kuesters, C.B. Carter, Tung Hsu, G. Wicks: Philos. Mag. A50, 849 (1984)

    Google Scholar 

  78. Tung Hsu: J. Vac. Sci. Technol. B4, 1035 (1985)

    Google Scholar 

  79. J.M. Cowley: Ultramicroscopy 7, 181 (1981)

    CAS  Google Scholar 

  80. N. Osakabe, Y. Tanishiro, K. Yagi, G. Honjo: Surf. Sci. 97, 393 (1980)

    CAS  Google Scholar 

  81. N. Osakabe, Y. Tanishiro, K. Yagi, G. Honjo: Surf. Sci. 102, 424 (1981)

    CAS  Google Scholar 

  82. Y. Tanishiro, K. Takayanagi, K. Yagi: Ultramicroscopy 11, 95 (1983)

    CAS  Google Scholar 

  83. N. Osakabe, Y. Tanishiro, K. Yagi, G. Honjo: Surf. Sci. 109, 353 (1981)

    CAS  Google Scholar 

  84. Y. Tanishiro, K. Takayanagi, K. Kobayashi, K. Yagi: Acta Crystallogr. Ser. A37, C-300 (1981)

    Google Scholar 

  85. N. Shimizu, Y. Tanishiro, K. Kobayashi, K. Takayanagi, K. Yagi: Ultramicroscopy 18, 453 (1985)

    CAS  Google Scholar 

  86. K. Yagi, K. Kobayashi, Y. Tanishiro, K. Takayanagi: Thin Solid Films 126, 95 (1985)

    CAS  Google Scholar 

  87. Tung Hsu: In 3rd Asian-Pacific Conf. E.M., Singapore 1984, ed. by Chung Mui Fatt (Applied Research Corporation, Singapore 1984), p.242

    Google Scholar 

  88. R. Sinclair, T. Yamashita, F.A. Ponce: Nature (London) 290, 386 (1981)

    CAS  Google Scholar 

  89. D.J. Smith, L.D. Marks: Proc. 7th Int. Conf. HVEM, Berkeley 1983, ed. by R.M. Fisher, R. Gronsky, K. Westmacott (Lawrence Berkeley Laboratory, Berkeley 1983) p.53

    Google Scholar 

  90. L.D. Marks: Phys. Rev. Lett. 51, 1000 (1983)

    CAS  Google Scholar 

  91. L.D. Marks: Surf. Sci. 139, 281 (1984)

    CAS  Google Scholar 

  92. D.J. Smith, L.D. Marks: Ultramicroscopy 16, 101 (1985)

    CAS  Google Scholar 

  93. L.D. Marks, D.J. Smith: Surf. Sci. 157, L367 (1985)

    CAS  Google Scholar 

  94. D.J. Smith, L.D. Marks: Mat. Res. Soc. Symp. Proc. 41, 129 (1985)

    CAS  Google Scholar 

  95. D.J. Smith, L.D. Marks: Surf. Sci., in press

    Google Scholar 

  96. L.R. Wallenberg, J.-O. Bovin, G. Schmid: Surf. Sci. 156, 256 (1985)

    CAS  Google Scholar 

  97. S. Iijima, T. Ichihashi: Jpn. J. Appl. Phys. 24, L125 (1985)

    Google Scholar 

  98. J.-O. Bovin, L.R. Wallenberg, D.J. Smith: Nature (London) 317, 49 (1985)

    Google Scholar 

  99. L.R. Wallenberg, D.J. Smith, J.-O. Bovin: Naturwissenschaften 72, 539 (1985)

    CAS  Google Scholar 

  100. K. Yagi: In 3rd Asian-Pacific Conf. E.M., Singapore 1984, ed. by Chung Mui Fatt (Applied Research Corporation, Singapore 1984) p.232

    Google Scholar 

  101. Yokoyana et ai.: To be published

    Google Scholar 

  102. S. Iijima: Jpn. J. Appl. Phys. 23, L347 (1984)

    Google Scholar 

  103. S. Iijima, S. Ichikawa: J. Catal. 94, 313 (1985)

    CAS  Google Scholar 

  104. N.A. Briscoe, J.L. Hutchinson: Inst. Phys. Conf. Ser. 68, 249 (1984)

    CAS  Google Scholar 

  105. J.L. Hutchison, N.A. Briscoe: Ultramicroscopy 18, 435 (1985)

    CAS  Google Scholar 

  106. C.E. Warble: Ultramicroscopy 15, 301 (1984)

    CAS  Google Scholar 

  107. C.E. Warble: J. Mater. Sci., in press

    Google Scholar 

  108. D.J. Smith, L.A. Bursill, L.D. Marks, Peng Ju Lin: In Proc. 43rd Annu. Meet. EMSA, Louisville 1985, ed. by G.W. Bailey (San Francisco Press, San Francisco 1985) p.256

    Google Scholar 

  109. L.D. Marks, A.K. Petford, M. O’Keeffe: In Proc. 43rd Annu. Meet. EMSA, Louisville 1985, ed. by G.W. Bailey (San Francisco Press, San Francisco 1985) p.266

    Google Scholar 

  110. J.P. Langmore, M.S. Isaacson, A.V. Crewe: In Proc. 32nd Annu. Meet. EMSA, St. Louis 1974, ed. by G.W. Bailey (Claitors, Baton Rouge, LA 1974) p.378

    Google Scholar 

  111. M.S. Isaacson, J. Langmore, N.W. Parker, D. Kopf, M. Utlaut: Ultramicroscopy 1, 359 (1976)

    CAS  Google Scholar 

  112. M.S. Isaacson, D. Kopf, M. Utlaut, N.W. Parker, A.V. Crewe: Proc. Nat. Acad. Sci. U.S.A. 14, 1802 (1977)

    Google Scholar 

  113. J.S. Wall, J.F. Hainfield, J.W. Bittner: Ultramicroscopy 3, 81 (1978)

    CAS  Google Scholar 

  114. S. Iijima: Paper presented at Arizona State University Centennial Conference on HREM (Scottsdale, January 1985)

    Google Scholar 

  115. J.-O. Bovin, L.R. Wallenberg: Paper presented at Arizona State University Centennial Conference on HREM (Scottsdale, January 1985)

    Google Scholar 

  116. W. Krakow: Inst. Phys. Conf. Ser. 61, 365 (1982)

    CAS  Google Scholar 

  117. J.C.H. Spence: Ultramicroscopy 11, 117 (1983)

    CAS  Google Scholar 

  118. G.J. Wood, O.L. Krivanek: Proc. 43rd Annu. Meet. EMSA, Louisville, 1985, ed. by G.W. Bailey (San Francisco Press, San Francisco 1985) p. 262

    Google Scholar 

  119. H. Shuman: Ultramicroscopy 2, 361 (1977)

    CAS  Google Scholar 

  120. J.M. Cowley, Lianmao Peng: Ultramicroscopy 16, 59 (1985)

    CAS  Google Scholar 

  121. A. Howie: Inst. Phys. Conf. Ser. 61, 419 (1982)

    CAS  Google Scholar 

  122. A. Howie: In Quantitative Electron Microscopy, ed. by J.N. Chapman, A.J. Craven (Scottish Universities Summer Schools in Physics, Edinburgh 1984) pp.37–43

    Google Scholar 

  123. J.M. Cowley: Mat. Res. Soc. Symp. Proc. 31, 177 (1984)

    CAS  Google Scholar 

  124. D.J. Smith: Contem. Physics, in press

    Google Scholar 

  125. Tung Hsu, J.M. Cowley: Mat. Res. Soc. Symp. Proc. 41, 121 (1985)

    CAS  Google Scholar 

  126. Tung Hsu: Norelco Rep. 31, 1 (1984)

    Google Scholar 

  127. K. Yagi: In 38th Annu. Meet. EMSA, Reno 1980, ed. by G.W. Bailey (Claitors, Baton Rouge, LA 1980) p.290

    Google Scholar 

  128. K. Yagi, K. Takayanagi, G. Honjo: Crystals, Growth, Properties and Applications 7, 47 (1982)

    CAS  Google Scholar 

  129. J.M. Cowley: In Scanning Electron Microscopy/1982, ed. by O. Johari, Vol.1 (SEM Inc., Chicago 1982) p.51

    Google Scholar 

  130. J.M. Cowley: ACS Symp. Ser. 353, 248 (1984)

    Google Scholar 

  131. M.J.Yacaman, K. Heinemann, H. Poppa: In Chemistry and Physics of Solid Surfaces, Vol.III, ed. by R. Vanselow, W. England (CRC, Boca Raton, FL 1982) p.109

    Google Scholar 

  132. M.J. Yacaman: In Chemistry and Physics of Solid Surfaces, ed. by R. Vanselow, R. Howe, Springer Ser. Chem. Phys., Vol.35 (Springer, Berlin, Heidelberg 1984) p.183

    Google Scholar 

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Smith, D.J. (1986). High-Resolution Electron Microscopy in Surface Science. In: Vanselow, R., Howe, R. (eds) Chemistry and Physics of Solid Surfaces VI. Springer Series in Surface Sciences, vol 5. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-82727-3_15

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