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Investigations on the type of OH-Groups in Some Crystalline Silicates by High Resolution NMR-Spectroscopy in Solids

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Magnetic Resonance and Related Phenomena

Abstract

By the multiple-pulse method WAHUHA and the combination WAHUHA and magic-angle sample spinning the 1H chemical shift anisotropy∆S and its spatial average \( \bar G \) was measured for powders of calcium sodium hydrogen silicate (1), barium dL hydrogen silicate (2), dicalcium silicate hydrate A (3). dicalcium silicate hydrate B (4) and xonotlite (5). The values of ∆S and \( \bar G \) depend on the strength of the hydrogen bonding and are in qualitative agreement with the theoretical results of Ditchfield et al.

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References

  1. J.S. Waugh, L.M. Huber and U. Haeberlen, Phys. Rev. Letters 20 (1968), 180

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  2. H. Rosenberger, R. Zeiss and A.R. Grimmer, Z. Chem. 15 (1975) 162

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  3. H. Rosenberger and B. Schnabel, Wiss. Z. Friedr.-SchTTler-Univ. Jena, Math.-Naturw. Reihe 27 (1978), 257

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  4. R. Ditchfield, J. chem. Phys. 65 (1976), 3123

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  5. A.-R. Grimmer and H. Rosenberger, submitted to Z. Chemie

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  6. H. Rosenberger and A.-R. Grimmer, submitted to Z. Anorg. u. Allg. Chemie

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Author information

Authors and Affiliations

  1. Sektion Physik, Friedrich-Schiller-Universität, DDR-69-Jena, Max-Wien-Platz 1, Österreich

    H. Rosenberger, U. Haubenreißer & B. Schnabel

  2. Zentralinstitut für Anorganische Chemie, Akademie der Wissenschaften der DDR, DDR-1199-Berlin, Rudower Chaussee 5, Deutschland

    A.-R. Grimmer

Authors
  1. H. Rosenberger
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  2. A.-R. Grimmer
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  3. U. Haubenreißer
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  4. B. Schnabel
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Editor information

Editors and Affiliations

  1. Department of Physics, Institute of Cybernetics of the Academy of Sciences of the Estonian SSR, USSR

    E. Kundla , E. Lippmaa  & T. Saluvere ,  & 

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© 1979 Springer-Verlag Berlin Heidelberg

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Rosenberger, H., Grimmer, AR., Haubenreißer, U., Schnabel, B. (1979). Investigations on the type of OH-Groups in Some Crystalline Silicates by High Resolution NMR-Spectroscopy in Solids. In: Kundla, E., Lippmaa, E., Saluvere, T. (eds) Magnetic Resonance and Related Phenomena. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-81344-3_41

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  • DOI: https://doi.org/10.1007/978-3-642-81344-3_41

  • Publisher Name: Springer, Berlin, Heidelberg

  • Print ISBN: 978-3-642-81346-7

  • Online ISBN: 978-3-642-81344-3

  • eBook Packages: Springer Book Archive

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