Abstract
Gas chromatography-mass spectrometry (GC-MS) is one of the most valuable analytical techniques for the separation and identification of low-molecular weight fragments such as are found in product mixtures after the application of chemical degradation methods to lignin (Chap. 6) and in spent pulping liquors (Gierer and Petterson 1977, Gierer and Lindeberg 1980) and bleaching effluents (Lindström and Nordin 1976, Lindström and Österberg 1980, 1984).
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References
Adamson DW, Kenner J (1937) Improved preparation of aliphatic diazo-compounds, and certain of their properties. J Chem Soc 1551–1556
Beynon JH, Saunders RA, Williams AE (1968) The mass spectra of organic molecules. Elsevier, Amsterdam, 352–394
Budzikiewicz H, Djerassi C, Williams DH (1967) Mass spectrometry of organic compounds. Holden-Day, San Francisco, 9–27
Dougherty RC, Dalton J, Biros FJ (1972) Negative chemical ionization mass spectra of polycyclic chlorinated insecticides. Org Mass Spectrom 6: 1171–1181
Eistert B, Regitz M, Schwall H (1968) Methoden zur Herstellung und Umwandlung von aliphatischen Diazoverbindungen. In: Müller E, Bayer O, Meerwein H, Ziegler K (eds) Methoden der organischen Chemie (Houben-Weyl) 4. Aufl., Band X/4 Stickstoff- Verbindungen I, Teil 4, George Thieme, Stuttgart, 554–557
Gierer J, Lindeberg O (1980) Reactions of lignin during sulfate pulping. Part XIX. Isolation and identification of new dimers from a spent sulfate liquor. Acta Chem Scand B 34: 161–172
Gierer J, Petterson I (1977) Study on the condensation of lignins in alkaline media (2). Formation of stilbene and aryicoumaran structures through neighboring group participation reactions. Can J Chem 55: 593–599
Harrison A (1983) Chemical ionization mass spectrometry. CRC Press, Boca Raton, 22–45
Hunt DF, Stafford GC, Crow FW, Russell JW (1976) Pulsed positive negative ion chemical ionization mass spectrometry. Anal Chem 48: 2098–2105
Lapierre C, Monties B, Rolando C (1985) Thioacidolysis of lignin: comparison with acidolysis. J Wood Chem Technol 5: 277–292
Lindström K, Nordin J (1976) Gas chromatography-mass spectrometry of chlorophenols in spent bleach liquors. J Chromatogr 128: 13–26
Lindström K, Österberg F (1980) Synthesis, X-ray structure determination, and formation of 3,4,5-trichloroguaiacol occurring in kraft pulp spent liquors. Can J Chem 58: 815–822
Lindström K, Österberg F (1984) Characterization of the high-molecular-mass chlorinated matter in spent bleach liquor (SBL). Part 1. Alkaline SBL. Holzforschung 38: 201–212
Munson MSB, Field FH (1966a) Chemical ionization mass spectrometry I. General introduction. J Am Chem Soc 88: 2621–2630
Munson MSB, Field FH (1966b) Chemical ionization mass spectrometry II. Esters. J Am Chem Soc 88: 4337–4345
Odham G, Stenhagen E (1972) Fatty acids. In: Waller GR (ed) Biochemical applications of mass spectrometry. Wiley-Interscience, New York, 211–228
Schultz TP, Chen C-L, Goldstein IS, Scaringelli FP (1981) Analysis of lignin hydrogenation products by gas chromatography. J Chromatogr Sci 19: 235–239
Tai D-S, Terazawa M, Chen C-L, Chang H-m (1990a) Lignin biodégradation products from birch wood decayed by Phanerochaete chrysosporium. Part 1. Fractionation of methanol-extractive and characterization of ether-insoluble low-molecular weight fractions. Holzforschung 44: 185–190
Tai D-S, Terazawa M, Chen C-L, Chang H-m (1990b) Lignin biodégradation products from birch wood decayed by Phanerochaete chrysosporium. Part 2. The constituent of ether-soluble low-molecular weight fractions. Holzforschung 44: 257–262
Tai D-S, Chen C-L, Gratzl JS (1990c) Chemistry of delignification during kraft pulping of bamboos. J Wood Chem Technol 10: 75–99
Vogel A (1978) A textbook of practical organic chemistry, 4th edn, Longmans, London, 289–291
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Chen, CL. (1992). Gas Chromatography-Mass Spectrometry (GS-MS). In: Lin, S.Y., Dence, C.W. (eds) Methods in Lignin Chemistry. Springer Series in Wood Science. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-74065-7_38
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DOI: https://doi.org/10.1007/978-3-642-74065-7_38
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