Skip to main content

Part of the book series: Springer Theses ((Springer Theses))

  • 847 Accesses

Abstract

In this chapter the data-evaluation procedures are discussed. Most of the data-evaluation steps are performed by programs written in an image processing soft-ware, PV-WAVE \({}^{\textregistered }\) [1]. Computer programing is highly required due to the large number of recorded patterns. Most computer programs run automatically after adjustment to the actual experimental conditions. In some programs the user have to define a Region Of Interest (ROI) on the first image and afterwards the program runs automatically.

Method consists entirely in the order and disposition of the objects towards which our mental vision must be directed if we would find out any truth. We shall comply with it exactly if we reduce involved and obscure propositions step by step to those that are simpler, and then starting with the intuitive apprehension of all those that are absolutely simple, attempt to ascend to the knowledge of all others by precisely similar steps.

...René Descartes.

This is a preview of subscription content, log in via an institution to check access.

Access this chapter

Chapter
USD 29.95
Price excludes VAT (USA)
  • Available as PDF
  • Read on any device
  • Instant download
  • Own it forever
eBook
USD 84.99
Price excludes VAT (USA)
  • Available as EPUB and PDF
  • Read on any device
  • Instant download
  • Own it forever
Softcover Book
USD 109.99
Price excludes VAT (USA)
  • Compact, lightweight edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info
Hardcover Book
USD 109.99
Price excludes VAT (USA)
  • Durable hardcover edition
  • Dispatched in 3 to 5 business days
  • Free shipping worldwide - see info

Tax calculation will be finalised at checkout

Purchases are for personal use only

Institutional subscriptions

Notes

  1. 1.

    All programs are freely available: http://www.chemie.uni-hamburg.de/tmc/stribeck/pv-wave/index_e.html.

  2. 2.

    See: http://plasma-gate.weizmann.ac.il/Grace/.

  3. 3.

    Where \(b\) indicates the width of a block in analogy with the notion of Strobl’s block structure [7, 8] observed during crystallization of polypropylene.

References

  1. VNI, PV-WAVE manuals, V 7.5, Houston, TX, USA (2007)

    Google Scholar 

  2. Denchev, Z., Dencheva, N., Funari, S.S., Motovilin, M., Schubert, T., Stribeck, N.: Nanostructure and mechanical properties studied during dynamical straining of microfibrillar reinforced HDPE/PA blends. J. Polym. Sci. Part B: Polym. Phys. 48, 237–250 (2010)

    Article  CAS  Google Scholar 

  3. Stribeck, N.: X-Ray Scattering of Soft Matter. Springer, Heidelberg (2007)

    Google Scholar 

  4. Stribeck, N., Nöchel, U.: A method for merging of USAXS and smeared SAXS patterns of fibers. J. Appl. Cryst. 41, 715–722 (2008)

    Article  CAS  Google Scholar 

  5. Stribeck, N.: Extraction of domain structure information from small-angle X-ray patterns of bulk materials. J. Appl. Cryst. 34, 496–503 (2001)

    Article  CAS  Google Scholar 

  6. Ruland, W.: The evaluation of the small-angle scattering of lamellar two-phase systems by means of interface distribution functions. Colloid Polym. Sci. 255, 417–427 (1977)

    Article  CAS  Google Scholar 

  7. Hugel, T., Strobl, G., Thomann, R.: Building lamellae from blocks: the pathway followed in the formation of crystallites of syndiotactic polypropylene. Acta Polym. 50, 214–217 (1999)

    Article  CAS  Google Scholar 

  8. Strobl, G.: Crystallization and melting of bulk polymers: new observations, conclusions and a thermodynamic scheme. Progr. Polym. Sci. 31, 398–442 (2006)

    Article  CAS  Google Scholar 

  9. Stribeck, N.: X-ray scattering for the monitoring of processes in polymer materials with fiber symmetry. J. Macromol. Sci. Part C: Polym. Rev. 50, 40–58 (2010)

    CAS  Google Scholar 

  10. Hall, E.L.: Computer Image Processing and Recognition. Academic Press, London (1980)

    Google Scholar 

  11. Humbert, S., Lame, O., Chenal, J.-M., Rochas, C., Vigier, G.: Small strain behavior of polyethylene: in situ SAXS measurements. J. Polym. Sci. Part B: Polym. Phys. 48, 1535–1542 (2010)

    Article  CAS  Google Scholar 

  12. Ran, S., Zong, X., Fang, D., Hsiao, B.S., Chu, B., Phillips, R.A.: Structural and morphological studies of isotactic polypropylene fibers during heat/draw deformation by in-situ synchrotron SAXS/WAXD. Macromolecules 34, 2569–2578 (2001)

    Article  CAS  Google Scholar 

  13. Jánosi, A.: Small-angle X-ray scattering from multiphase systems. Interpretation of the electron density fluctuation (Ger.). Monatsh. f. Chemie 114, 377–383 (1983)

    Article  Google Scholar 

  14. Glatter, O., Kratky, O. (eds.): Small Angle X-ray Scattering. Academic Press, London (1982)

    Google Scholar 

  15. Baltá-Calleja, F.J., Vonk, C.G.: X-Ray Scattering of Synthetic Polymers. Elsevier, Amsterdam (1989)

    Google Scholar 

Download references

Author information

Authors and Affiliations

Authors

Rights and permissions

Reprints and permissions

Copyright information

© 2013 Springer-Verlag Berlin Heidelberg

About this chapter

Cite this chapter

Zeinolebadi, A. (2013). Data Evaluation. In: In-situ Small-Angle X-ray Scattering Investigation of Transient Nanostructure of Multi-phase Polymer Materials Under Mechanical Deformation. Springer Theses. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-35413-7_3

Download citation

Publish with us

Policies and ethics