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Effects of Rice Husk as a Precursor on Crystallization Kinetic of Glass Ceramics Derived from 45S5 Bioglass®

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Characterization and Development of Biosystems and Biomaterials

Part of the book series: Advanced Structured Materials ((STRUCTMAT,volume 29))

Abstract

The crystallization kinetic of glass ceramics derived from 45S5 Bioglass® made from rice husk ash was studied. In order to investigate and control the sintering process of these samples, the crystallization kinetic of the major phase was studied by differential scanning calorimetry (DSC) in the range of 700–800 °C and temperature-time-transformation (TTT) curves were established. Differential thermal analysis (DTA) was performed to investigate the thermal parameters of the prepared glasses. Phase evolution of the glass–ceramics sintered at temperatures ranging between 600 and 900 °C was investigated by Scanning electron microscope (SEM) and X-ray diffraction (XRD) techniques. All thermal parameters (the first glass transition temperature; T g1, the softening point; T s, the crystallization temperature; T c and the second glass transition temperature; T g2) of the prepared glass containing rice husk precursor were found to be lower than that of the controlled glass. It was found that the major crystalline phase in all sintered samples was Na2Ca2Si3O9.

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Acknowledgments

We would like to express their sincere gratitude to the Thailand Research Fund (TRF) and the Graduate School and Faculty of Science, Chiang Mai University, Thailand for their financial supports. We wish to thank the National Research University Project under Thailand’s Office of the Higher Education Commission for financial support.

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Authors and Affiliations

  1. Department of Physics and Materials Science, Chiang Mai University, Chiang Mai, 50200, Thailand

    Wilaiwan Leenakul, Sukum Eitssayeam, Gobwute Rujijangul & Kamonpan Pengpat

  2. Materials Science Research Center, Chiang Mai University, Chiang Mai, 50200, Thailand

    Wilaiwan Leenakul, Sukum Eitssayeam, Gobwute Rujijangul, Tawee Tunkasiri & Kamonpan Pengpat

  3. Department of Mathematics, Faculty of Science, Chiang Mai University, Chiang Mai, 50200, Thailand

    Natee Tongsiri

Authors
  1. Wilaiwan Leenakul
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  2. Sukum Eitssayeam
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  3. Gobwute Rujijangul
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  4. Tawee Tunkasiri
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  5. Natee Tongsiri
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  6. Kamonpan Pengpat
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Corresponding author

Correspondence to Kamonpan Pengpat .

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Editors and Affiliations

  1. , Faculty Biosciences and, University of Technology Malaysia - UTM, Block A, Building V01, Johor Bahru, 81310, Malaysia

    Andreas Öchsner

  2. , Department of Mechanical Engineering, University of Porto, Rua Dr. Roberto Frias, Porto, 4200-465, Portugal

    Lucas F. M. da Silva

  3. , Lehrstuhl für Technische Mechanik, Otto-von-Guericke-Universität Magdeburg, Universitätsplatz 2, Magdeburg, 39106, Germany

    Holm Altenbach

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Leenakul, W., Eitssayeam, S., Rujijangul, G., Tunkasiri, T., Tongsiri, N., Pengpat, K. (2013). Effects of Rice Husk as a Precursor on Crystallization Kinetic of Glass Ceramics Derived from 45S5 Bioglass®. In: Öchsner, A., da Silva, L., Altenbach, H. (eds) Characterization and Development of Biosystems and Biomaterials. Advanced Structured Materials, vol 29. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-31470-4_8

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