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Nanometer-Scale Four-Point Probe Resistance Measurements of Individual Nanowires by Four-Tip STM

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Atomic Scale Interconnection Machines

Part of the book series: Advances in Atom and Single Molecule Machines ((AASMM))

Abstract

We present a review of our recent results about transport properties of nanowires measured by a four-tip scanning tunneling microscope (STM) installed with metal-coated carbon nanotube (CNT) tips. We first present our custom-made apparatus (with UNISOKU Co.) as well as CNT tips, and then some case studies with two different samples, Co-silicide nanowires self-assembled on Si(110) surface and Cu nanowires made by damascene processes used in LSI industry. It is shown that the four-tip STM with CNT tips is versatile and powerful for measuring the conductivity of individual nanostructures.

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References

  1. Kubo, O., Shingaya, Y., Nakayama, M., Aono, M., Nakayama, T.: Epitaxially grown WOx nanorod probes for sub-100 nm multiple-scanning-probe measurement. Appl. Phys. Lett. 88, 254101 (2006)

    Article  ADS  Google Scholar 

  2. Tsukamoto, S., Siu, B., Nakagiri, N.: Twin-probe scanning tunneling microcope. Rev. Sci. Instrum. 62, 1767 (1991)

    Article  ADS  Google Scholar 

  3. Okamoto, H., Chen, D. M.: An ultrahigh vacuum dual-tip scanning tunneling microscope operating at 4.2 K. Rev. Sci. Instr. 72, 4398 (2001)

    Google Scholar 

  4. Watanabe, H., Manabe, C., Shigematsu, T., Shimizu, M.: Single molecule DNA device measured with triple-probe atomic force microscope. Appl. Phys. Lett. 78, 2928 (2001); 79, 2462 (2001)

    Google Scholar 

  5. Lin, X., He, X.B., Yang, T.Z., Guo, W., Shi, D.X., Gao, H.-J., Ma, D.D.D., Lee, S.T., Liu, F., Xie, X.C.: Intrinsic current-voltage properties of nanowires with four-probe scanning tunneling microscopy: A conductance transition of ZnO nanowire. Appl. Phys. Lett. 89, 043103 (2006)

    Article  ADS  Google Scholar 

  6. Guise, O., Marbach, H., Yates Jr, J.T., Jung, M.-C., Levy, J.: Development and performance of the nanoworkbench: A four tip STM for conductivity measurements down to submicrometer scales. Rev. Sci. Instr. 76, 045107 (2005)

    Article  ADS  Google Scholar 

  7. Ishikawa, M., Yoshimura, M., Ueda, K.: Development of four-probe microscopy for electric conductivity measurement. Jpn. J. Appl. Phys. 44, 1502 (2005)

    Article  ADS  Google Scholar 

  8. Takami, K., Akai-Kasaya, M., Saito, A., Aono, M., Kuwahara, Y.: Construction of independently driven double-tip scanning tunneling microscope. Jpn. J. Appl. Phys. 44, L120 (2005)

    Article  ADS  Google Scholar 

  9. Grube, H., Harrison, B.C., Jia, J.F., Boland, J.J.: Stability, resolution, and tip–tip imaging by a dual-probe scanning tunneling microscope. Rev. Sci. Instr. 72, 4388 (2001)

    Article  ADS  Google Scholar 

  10. Bannani, A., Bobisch, C.A., Möller, R.: Local potentiometry using a multiprobe scanning tunneling microscope. Rev. Sci. Instrum. 79, 083704 (2008)

    Article  ADS  Google Scholar 

  11. Omicron Nano Technology GmbH (http://www.omicron.de/), MultiProbe, Inc (http://www.multiprobe.com/), Zyvex Co. (http://www.zyvex.com/)

  12. Shiraki, I., Tanabe, F., Hobara, R., Nagao, T., Hasegawa, S.: Independently driven four-tip probes for conductivity measurements in ultlahigh vacuum. Surf. Sci. 493, 633 (2001)

    Article  ADS  Google Scholar 

  13. Hasegawa, S., Shiraki, I., Tanabe, F., Hobara, R.: Transport at surface nanostructures measured by four-tip STM. Current Appl. Phys. 2, 465 (2002)

    Article  ADS  Google Scholar 

  14. Hobara, R., Nagamura, N., Hasegawa, S., Matsuda, I., Yamamoto, Y., Ishikawa, K., Nagamura, T.: Variable-temperature independently-driven four-tip scanning tunneling microscope. Rev. Sci. Inst. 78, 053705 (2007)

    Article  ADS  Google Scholar 

  15. Ikuno, T., Katayama, M., Kishida, M., Kamada, K., Murata, Y., Yasuda, T., Honda, S., Lee, J.-G., Mori, H., Oura, K.: Metal-coated carbon nanotube tip for scanning tunneling microscope. Jpn. J. Appl. Phys. 43, L644 (2004)

    Article  ADS  Google Scholar 

  16. Yoshimoto, S., Murata, Y., Hobara, R., Matsuda, I., Kishida, M., Konishi, H., Ikuno, T., Maeda, D., Yasuda, T., Honda, S., Okado, H., Oura, K., Katayama, M., Hasegawa, S.: Electrical characterization of metal-coated carbon-nanotube tips. Jpn. J. Appl. Phys. 44, L1563 (2005)

    Article  ADS  Google Scholar 

  17. Konishi, H., Murata, Y., Wongwiriyapan, W., Kishida, M., Tomita, K., Motoyoshi, K., Honda, S., Katayama, M., Yoshimoto, S., Kubo, K., Hobara, R., Matsuda, I., Ha-segawa, S., Yoshimura, M., Lee, J.-G., Mori, H.: High-yield synthesis of conductive carbon nanotube tips for multiprobe scanning tunneling microscope. Rev. Sci. Instr. 78, 013703 (2007)

    Article  ADS  Google Scholar 

  18. Kanagawa, T., Hobara, R., Matsuda, I., Tanikawa, T., Natori, A., Hasegawa, S.: Anisotropy in conductance of a quasi-one-dimensional metallic surface state measured by square micro-four-point probe method. Phys. Rev. Lett. 91, 036805 (2003)

    Article  ADS  Google Scholar 

  19. Shingaya, Y., et al.: Carbon nanotube tip for scanning tunneling microscopy. Phys. B 323, 153 (2002)

    Article  ADS  Google Scholar 

  20. Ishikawa, M., et al.: Simultaneous measurement of topography and contact current by contact mode atomic force microscopy with carbon nanotube probe. Jpn. J. Appl. Phys. 41, 4908 (2002)

    Article  ADS  Google Scholar 

  21. Ueda, K., Yoshimura, M., Nagamura, T.: A fabrication method tips for scanning probe microscopes and its apparatus, Japan Patent 2004, No. 3557589

    Google Scholar 

  22. Tang, J., Gao, B., Geng, H., Velev, O.D., Qin, L.-C., Zhou, O.: Assembly of ID nanostructures into sub-micrometer diameter fibrils with controlled and variable length by dielectrophoresis. Adv. Mater. 15, 1352 (2003)

    Article  Google Scholar 

  23. Yoshimoto, S., Murata, Y., Hobara, R., Matsuda, I., Kishida, M., Konishi, H., Ikuno, T., Maeda, D., Yasuda, T., Honda, S., Okado, H., Oura, K., Katayama, M., Hasegawa, S.: Four-point probe resistance measurements using ptIr-coated carbon nanotube tips. Nano Lett. 7, 956 (2007)

    Article  ADS  Google Scholar 

  24. Murata, Y., Yoshimoto, S., Kishida, M., Maeda, D., Yasuda, T., Ikuno, T., Honda, S., Okado, H., Hobara, R., Matsuda, I., Hasegawa, S., Oura, K., Katayama, M.: Exploiting metal coating of carbon nanotubes for scanning tunneling microscopy probes. Jpn. J. Appl. Phys. 44, 5336 (2005)

    Article  ADS  Google Scholar 

  25. He, Z., Smith, D.J., Bennett, P.A.: Endotaxial silicide nanowires. Phys. Rev. Lett. 93, 256102 (2004)

    Article  ADS  Google Scholar 

  26. Okino, H., Matsuda, I., Hobara, R., Hosomura, Y., Hasegawa, S., Bennett, P.A.: In situ resistance measurements of epitaxial cobalt silicide nanowires on Si(110). Appl. Phys. Lett. 86, 233108 (2005)

    Article  ADS  Google Scholar 

  27. Hensel, J.C., Tung, R.T., Poate, J.M., Unterwald, F.C.: Specular boundary scattering and electrical transport in single-crystal thin films of CoSi2. Phys. Rev. Lett. 54, 1840 (1985)

    Article  ADS  Google Scholar 

  28. Allen, P.B., Schulz, W.W.: Bloch-Boltzmann analysis of electron transport in intermetallic compounds — ReO3, BaPbO3, CoSi2, and Pd2Si. Phys. Rev. B 47, 14434 (1993)

    Article  Google Scholar 

  29. Kitaoka, Y., Tono, T., Yoshimoto, S., Hirahara, T., Hasegawa, S., Ohba, T.: Direct detection of grain boundary scattering in damascene Cu wires by nanometer-scale four-point probe resistance measurements. Appl. Phys. Lett. 95, 052110 (2009)

    Article  ADS  Google Scholar 

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Acknowledgments

The present work was done in collaboration with UNISOKU Co., Ltd. in construction of the four-tip STM and Prof. M. Katayama in fabricating CNT tips. It was fully supported by the SENTAN Program of the Japan Science and Technology Agency (JST), and also by Grants-in-Aid for Scientific Research and A3 Foresight Program from the Japanese Society for the Promotion of Science (JSPS).

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Correspondence to S. Hasegawa .

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© 2012 Springer-Verlag Berlin Heidelberg

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Hasegawa, S., Hirahara, T., Kitaoka, Y., Yoshimoto, S., Tono, T., Ohba, T. (2012). Nanometer-Scale Four-Point Probe Resistance Measurements of Individual Nanowires by Four-Tip STM. In: Joachim, C. (eds) Atomic Scale Interconnection Machines. Advances in Atom and Single Molecule Machines. Springer, Berlin, Heidelberg. https://doi.org/10.1007/978-3-642-28172-3_12

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  • DOI: https://doi.org/10.1007/978-3-642-28172-3_12

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  • Publisher Name: Springer, Berlin, Heidelberg

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  • Online ISBN: 978-3-642-28172-3

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